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7
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46449090883
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For detailed mechanistic studies of the role of additives, see:
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For detailed mechanistic studies of the role of additives, see:. Flowers R.A. Synlett (2008) 1427-1439
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Flowers, R.A.1
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9
-
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0346422364
-
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For an elegant example of the use of alcohol proton donors in directing the reaction pathway, see:
-
For an elegant example of the use of alcohol proton donors in directing the reaction pathway, see:. Hutton T.K., Muir K.W., and Procter D.J. Org. Lett. 5 (2003) 4811-4814
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3042835365
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11
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0000728528
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3 SnH/AIBN/Δ conditions, see:
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3 SnH/AIBN/Δ conditions, see:. Enholm E.J., and Kinter K.S. J. Org. Chem. 60 (1995) 4850-4855
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33845691976
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For α-tethered bis-cyclohexenones, see:
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For α-tethered bis-cyclohexenones, see:. Handy S.T., and Omune D. Tetrahedron 63 (2007) 1366-1371
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Handy, S.T.1
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14
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17444396764
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16
-
-
65549132173
-
-
note
-
f = 0.17 (40% EtOAc in petrol). Spectroscopic characterisation of compounds 9-11, 13, 14b, 19, 20a/b and 21a/b is provided as Supplementary data.
-
-
-
-
17
-
-
65549095216
-
-
note
-
13C NMR spectroscopy, IR and high resolution mass spectrometry.
-
-
-
-
18
-
-
65549096493
-
-
note
-
-1, Z = 28. These data are from an isotropic refinement of sub-publication quality. The coordinates are available in CIF format as Supplementary data.
-
-
-
-
19
-
-
0033515504
-
-
An oligomeric samarium species is probable, and expected from a radical-radical 5-exo-trig homodimerisation. Only for the purpose of clarity, monomeric samarium(III) chelation control is shown:
-
An oligomeric samarium species is probable, and expected from a radical-radical 5-exo-trig homodimerisation. Only for the purpose of clarity, monomeric samarium(III) chelation control is shown:. Keck G.E., Wager C.A., Sell T., and Wager T.T. J. Org. Chem. 64 (1999) 2172-2173
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Keck, G.E.1
Wager, C.A.2
Sell, T.3
Wager, T.T.4
-
20
-
-
65549083162
-
-
note
-
Spectroscopic characterization of compounds 17a/b and 18 is provided as Supplementary data.
-
-
-
-
21
-
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0000912721
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Mattay J., Banning A., Bischof E.W., Heidbreder A., and Runsink J. Chem. Ber. 125 (1992) 2119-2127
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Mattay, J.1
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24
-
-
65549125632
-
-
note
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3).
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