Method performance and multi-laboratory assessment of a normal phase high pressure liquid chromatography-fluorescence detection method for the quantitation of flavanols and procyanidins in cocoa and chocolate containing samples

Journal of Chromatography A

Volumn 1216, Issue 24, 2009, Pages 4831-4840

  Robbins, Rebecca J ^a   Leonczak, Jadwiga ^a   Johnson, J Christopher ^a   Li, Julia ^a   Kwik Uribe, Catherine ^a   Prior, Ronald L ^b   Gu, Liwei ^c  

^a MARS INC   (United States)

^b U S DEPARTMENT OF AGRICULTURE   (United States)

^c UNIVERSITY OF FLORIDA   (United States)

Author keywords

Chocolate; Cocoa; Diol; Flavanols; FLD; HPLC; Multi laboratory validation; NIST; Procyanidins; Quantitative

Indexed keywords

CHOCOLATE; COCOA; DIOL; FLAVANOLS; FLD; HPLC; MULTI-LABORATORY VALIDATION; NIST; PROCYANIDINS; QUANTITATIVE;

BEVERAGES; CHROMATOGRAPHIC ANALYSIS; DISCRIMINANT ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LABORATORIES; PHASE SEPARATION; SEMICONDUCTOR SWITCHES;

HIGH PRESSURE LIQUID CHROMATOGRAPHY;

FLAVANOL DERIVATIVE; PROCYANIDIN DERIVATIVE;

ARTICLE; CACAO; CHEMICAL STRUCTURE; FLUORESCENCE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LABORATORY TEST; PRIORITY JOURNAL;

ANTIOXIDANTS; CACAO; CANDY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FLAVONOLS; FLUORESCENCE; FOOD ANALYSIS; PROANTHOCYANIDINS;

THEOBROMA CACAO;

EID: 65549101812     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.04.006     Document Type: Article

References (30)

1. Heiss C., Kleinbongard P., Dejam A., Perre S., Schroeter H., Sies H., and Kelm M. J. Am. Coll. Card 46 (2005) 1276
2. Rein D., Paglieroni T.G., Wun T., Pearson D.A., Schmitz H.H., Gosselin R., and Keen C.L. Am. J. Clin. Nutr. 72 (2000) 30
3. Fisher N.D., Hughes M., Gerhard-Herman M., and Hollenberg N.K. J. Hypertens. 21 (2003) 2281
4. Prior R.L., and Gu L. Phytochemistry 66 (2005) 2264
5. Schroeter H., Heiss C., Balzer J., Kleinbongard P., Keen C.L., Hollenberg N.K., Sies H., Kwik-Uribe C., Schmitz H.H., and Kelm M. Proc. Natl. Acad. Sci. 103 (2006) 1024-1029
6. Engler M.B., Engler M.M., Chen C.Y., Malloy M.J., Browne A., Chui E.Y., Kwak H.-K., Milbury P., Paul S.M., Blumberg J., and Mietus-Snyder M.L. J. Am. Coll. Nutr. 23 (2004) 197
7. Porter L.J. In: Harborne J.B. (Ed). The Flavanoids (1988), Chapman and Hall Ltd., New York p. 23
8. Santos-Buelga C., and Williamson G. In: Santos-Buelga C., and Williamson G. (Eds). Methods in Polyphenol Analysis (2003), The Royal Society of Chemistry, Cambridge p. 267
9. Waterhouse A.L., Ignelzi S., and Shirley J.R. Am. J. Enol. Vitic. 51 (2000) 383
10. Rigaud J., Escribano-Bailon M.T., Prieur C., Souquet J.M., and Cheynier V.J. J. Chromatogr. A 654 (1993) 179
11. Lazarus S.A., Adamson G.E., Hammerstone J.F., and Schmitz H.H. J. Agric. Food Chem. 47 (1999) 3693
12. Hammerstone J.F., Lazarus A.S., Mitchell A.E., Rucker R.B., and Schmitz H.H. J. Agric. Food Chem. 47 (1999) 490
13. Gu L., Kelm M., Hammerstone J.F., Beecher G., Cunningham D., Vannozzi S., and Prior R.L. J. Agric. Food Chem. 50 (2002) 4852
14. Rein D., Lotito S., Fraga C.G., Schmitz H.H., and Keen C.L. J. Nutr. 130 (2000) 2120S
15. Engler M.B., Engler M.M., Chen C.Y., Malloy M.J., Browne A., Chiu E.Y., Kwak H.K., Milbury P., Paul S.M., Blumberg J., and Mietus-Snyder M.L. J. Am. Coll. Nutr. 23 (2004) 197
16. Kelm M.A., Johnson J.C., Robbins R.J., Hammerstone J.F., and Schmitz H.H. J. Agric. Food Chem. 54 (2006) 1571
17. Adamson G.E., Lazarus S.A., Mitchell A.E., Prior R.L., Cao G., Jacobs P.H., Kremers B.G., Hammerstone J.F., Rucker R., Ritter K.A., and Schimtz H.H. J. Agric. Food Chem. 47 (1999) 4184
18. Gu L., Hager A., Robbins R.J., and Prior R.L. FASEB 22 (2008) 5
19. Gu L., Kelm M.A., Hammerstone J.F., Beecher G., Holden J., Haytowitz D., and Prior R.L. J. Agric. Food Chem. 51 (2003) 7513
20. Snyder L.R., Glajch J.L., and Kirkland J.J. Practical HPLC Method Development (1988), John Wiley & Sons
21. Snyder L.R. J. Chromatogr. Sci. 16 (1978) 223
22. Snyder L.R., and Kirkland J.J. Introduction to Modern Liquid Chromatography (1979), Wiley-Interscience
23. http://www.aoac.org/dietsupp6/Dietary-Supplement-web-site/slv_guidelines.pdf.
24. Lazarus S.A., Hammerstone J.F., Adamson G.E., and Schmitz H.H. In: Abelson J.N., and Simon M.I. (Eds). Methods in Enzymology (2001), Academic Press, Berkeley, California p. 46
25. Krech J.H., and Rose-Pehrsson S.L. Appl. Spec. 50 (1996) 1528
26. Saha S.K., and Dogra S.K. J. Lumin. 75 (1997) 117
27. Mattice W.L. In: Hemingway R.W., and Laks P.E. (Eds). Plant Polyphenols (1992), Plenum Press, New York p. 447
28. Counet C., and Collin S. J Agric. Food Chem. 51 (2003) 6816
29. Bittner S. Amino Acids 30 (2006) 205
30. Gu L., House S., Wu E.X., Ou B., and Prior R.L. J Agric. Food Chem. 54 (2006) 4057