Determination of hydrogen content in geological samples using elastic recoil detection analysis (ERDA)

Geochimica et Cosmochimica Acta

Volumn 73, Issue 11, 2009, Pages 3311-3322

  Bureau, Hélène ^a,b   Raepsaet, Caroline ^b   Khodja, Hicham ^b   Carraro, Anna ^c   Aubaud, Cyril ^d  

^a UNIVERSITÉ PIERRE ET MARIE CURIE   (France)

^b DIF   (France)

^c Dipartimento di Geoscienze   (Italy)

^d INSTITUT DE PHYSIQUE DU GLOBE DE PARIS   (France)

Author keywords

[No Author keywords available]

Indexed keywords

BACKSCATTER; DETECTION METHOD; FTIR SPECTROSCOPY; HYDROGEN ISOTOPE; MAPPING METHOD; MASS SPECTROMETRY; MELT INCLUSION; TRACE ELEMENT;

ATLANTIC ISLANDS; ATLANTIC OCEAN; CARIBBEAN ISLANDS; EURASIA; EUROPE; GUADELOUPE; ITALY; LEEWARD ISLANDS [LESSER ANTILLES]; LESSER ANTILLES; LIPARI ISLANDS; MESSINA [SICILY]; SICILY; SOUTHERN EUROPE; STROMBOLI;

EID: 65449125789     PISSN: 00167037     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.gca.2009.03.009     Document Type: Article

References (60)

1. Arredondo E.H., and Rossman G.R. Feasibility of determining the quantitative OH content of garnets with Raman spectroscopy. Am. Miner. 87 (2002) 307-311
2. Aubaud C., Withers A., Hirschmann M.M., Guan Y., Leshin L.A., Mackwell S.J., and Bell D.R. Intercalibration of FTIR and SIMS for hydrogen measurements in glasses and nominally anhydrous minerals. Am. Miner. 92 (2007) 811-828
3. Aubaud C., Bureau H., Raepsaet C., Khodja H., Hirschmann M.M., Withers A.C., and Bell D.R. Calibration of the infrared molar absorption coefficients for H in olivine, clinopyroxene and rhyolitic glass by elastic recoil detection analysis (2009). Chem. Geol. 260 (2009) 286-294
4. Barbour J.C., and Doyle B.L. Elastic recoil detection: ERD (or forward recoil spectrometry FRES). In: Tesmer J.R., et al. (Ed). Handbook of Modern Ion Beam Analysis (1995), Materials Research Society 83-138
5. Bartholomew R.F., Butler B.L., Hoover H.L., and Wu C.K. Infrared spectra of a water-containing glass. J. Am. Ceramic Soc. 63 (1980) 481-485
6. 8 (M = Li, Na, K): an interlaboratory study. Chem. Geol. 128 (1996) 41-63
7. 2O in silicate glasses using confocal microRaman spectroscopy. Chem. Geol. 229 (2006) 96-112
8. Bell D.R., and Rossman G.R. Water in the earth's mantle; the role of nominally anhydrous minerals. Science 255 (1992) 1391-1397
9. Bell D.R., Ihinger P.D., and Rossman G.R. Quantitative analysis of trace OH in garnet and pyroxenes. Am. Miner. 80 (1995) 465-474
10. Bell D. R., Rossman G. R., Maldener J., Endisch D. and Rauch F. (2003) Hydroxide in olivine: a quantitative determination of the absolute amount and calibration of the IR spectrum. J. Geophys. Res. 108 B2. doi:10.1029/2001JB000679.
11. Beran A. and Libowitzky E. (2006) Water in natural minerals II: olivine, garnet and accessory minerals. In Water in nominally anhydrous minerals. Reviews in Mineralogy and Geochemistry, vol 62, (eds. H. Keppler and J. R. Smith). pp. 177-191.
12. Berger P., Gallien J.P., Khodja H., Daudin L., Berger M.H., and Sayier A. Nuclear microprobe local hydrogen measurements in HTPC. Solid State Ionics 177 (2006) 1655-1658
13. Bolfan-Casanova N., Keppler H., and Rubie D. Water partitioning between nominally anhydrous minerals in the MgO-SiO2-H2O system up to 24 GPa: implications for the distribution of water in Earth's mantle. Earth Planet. Sci. Lett. 182 (2000) 209-221
14. Bureau H., Trocellier P., Shaw C., Khodja H., Bolfan-Casanova N., and Demouchy S. Determination of the concentration of water dissolved in glasses and minerals using nuclear microprobe. Nucl. Instrum. Methods Phys. Res. B 210 (2003) 449-454
15. Carraro A., and Visonà D. Mantle xenoliths in Triassic camptonite dykes of the Predazzo Area (Dolomites, Northern Italy): petrography, mineral chemistry and geothermobarometry. Eur. J. Mineral 15 (2003) 103-115
16. Carraro A., Carli C., Visonà D. and Boscardin M. (2005) I noduli di peridotite a spinello nel filone basaltico di Valle di Fondi (Altopiano di Asiago, Vicenza): microstrutture, composizione e geotermometria. Studi e Ricerche - Associazione Amici del Museo - Museo Civico "G. Zannato" - Montecchio Maggiore (Vicenza), 12, 37-41.
17. Carraro A., Visonà D., Bettin S. and Boscardin M. (2006) Noduli ultramafici e megacristalli nelle lave basaltiche di Salbeghi (Marosticano, Vicenza). Studi e Ricerche - Associazione Amici del Museo - Museo Civico "G. Zannato" - Montecchio Maggiore (Vicenza), 13, 35-42.
18. Carraro A., Bureau H., Visonà D., Raepsaet C., Fuchs Y. and Khodja H., (2007a) Hydrogen concentration in mantle xenoliths from the Veneto Volcanic Province (NE Italy). Goldschmidt. Conference Cologne 19-24 August 2007, Germany.
19. Carraro A., Visonà D., Nimis P. and Boscardin M. (2007b) I granati delle Fosse di Novale (Vicenza). Studi e Ricerche - Associazione Amici del Museo - Museo Civico "G. Zannato" - Montecchio Maggiore (Vicenza), 14, 77-80.
20. Chabiron A., Pironon J., and Massare D. Characterization of water in synthetic rhyolitic glasses and natural melt inclusions by Raman spectroscopic study. Contrib. Miner. Petrol. 146 (2004) 485-492
21. Cohen B.L., Fink C.L., and Degnan J.H. Nondestructive analysis for trace amounts of hydrogen. J. Appl. Phys. 43 (1972) 19-25
22. Daudin L., Khodja H., and Gallien J.P. Development of "position-charge-time" tagged spectrometry for ion beam microanalysis. Nucl. Instrum. Methods B 210 (2003) 153-158
23. Deloule E., Paillat O., Pichavant M., and Scaillet B. Ion microprobe determination of water in silicate glassest methods and applications. Chem. Geol. 125 (1995) 19-28
24. Demouchy S., Jacobsen S.D., Gaillard F., and Stern C.R. Rapid magma ascent by water diffusion profiles in mantle olivine. Geology 34 (2006) 429-432
25. 2O contents of silicic volcanic glasses. Am. Mine. 80 (1995) 319-328
26. Di Muro A., Villemant B., Montagnac G., Scaillet B., and Reynart B. Quantification of water content and speciation in natural silicic glasses (phonolite, dacite, rhyolite) by confocal microRaman spectrometry. Geochim. et Cosmochim. Acta 70 (2006) 2868-2884
27. Dixon J.E., Stolper E.M., and Holloway J.R. An experimental study of water and carbon dioxide solubilities in mid-ocean ridge basaltic liquids. Part I: Calibration and solubility models. J. Petro. 36 (1995) 1607-1631
28. Endish D., Sturm H., and Rauch F. Nuclear reaction analysis of hydrogen at levels below 10 at ppm. Nucl. Instrum. Methods Phys. Res. B 84 (1994) 380-392
29. Furuno K., Komatsubara T., Sasa K., Oshima H., Yamato Y., Ishii S., Kimura H., and Kurosawa M. Measurement of hydrogen concentration in thick mineral or rock samples. Nucl. Instrum. Methods Phys. Res. B 210 (2003) 459-463
30. Hauri E., Wang J., Dixon J.E., King P.L., Mandeville C., and Newman S. SIMS analysis of volatiles in silicate glasses 1. Calibration, matrix effects and comparison with FTIR. Chem. Geol. 183 (2002) 99-114
31. Ingrin J., and Skogby H. Hydrogen in nomainally anhydrous uppermantle minerals:Concentration levels and implications. Eur. J. Mineral 12 (2000) 543-570
32. Jagielski J., Gentils A., Thomé L., Nowicki L., Garrido F., and Klaumünzer S. Channeling study of the damage induced in zirconia irradiated with high-energy heavy ions. Nucl. Instrum. Methods B 219-220 (2004) 626-630
33. Khodja H., Berthoumieux E., Daudin L., and Gallien J.P. The Pierre Süe Laboratory nuclear microprobe as a multi-disciplinary analysis tool. Nucl. Instrum. Methods B 181 (2001) 83-86
34. Koga K., Hauri E., Hirschmann M. and Bell D., (2003) Hydrogen concentration analyses using SIMS and FTIR: comparison and calibration for nominally anhydrous minerals. Geochem., Geophys., Geosyst., 4. doi:10.1029/2002GC00378.
35. Kohn S.C. and Grant K.J. (2006) The partitioning of water between nominally anhydrous minerals and silicate melts. In Water in nominally anhydrous minerals. Reviews in Mineralogy and Geochemistry, vol. 62, (eds. H. Keppler and J. R. Smith). pp. 231-241.
36. Kovacs I., Hermann J., O'Neill H.St.C., Gerald J.F., Sambridge M., and Horvath G. Quantitative absorbance spectroscopy with unpolarized light: Part II. Experimental evaluation and development of a protocol for quantitative analysis of mineral IR spectra. Am. Miner. 93 (2008) 765-778
37. Libowitzky E., Beran A., (2006) The structure of hydrous species in nominally anhydrous minerals: information from polarized IR spectroscopy. In Water in nominally anhydrous minerals. Reviews in Mineralogy and Geochemistry, vol 62, (eds. H. Keppler and J. R. Smith). pp. 29-52.
38. Libowitzky E., and Rossman G.R. An IR absorption calibration for water in minerals. Am. Miner. 82 (1997) 1111-1115
39. Maxwell J.A., Campbell J.L., and Teesdale W.J. The Guelph PIXE software package. Nucl. Instrum. Methods Phys. Res. B 43 (1989) 218-230
40. Mayer M. (1999) SIMNRA a simulation program for the analysis of NRA, RBS,and ERDA, In Proceedings of the 15th International Conference on the Application of Accelerators in Research and Industry. (eds. J. L. Duggan and I. L. Morgan), American Institute of Physics Conference Proceedings, 475, p. 541.
41. Mercier M., Di Muro A., Giordano D., Métrich N., Lesne P., Pichavant M., Scaillet B., Clocchiatti R., and Montagnac G. Influence of glass polymerisation and oxidation on micro-Raman water analysis in alumino-silicate glasses. Geochim. et Cosmochim. Acta 73 (2009) 197-217
42. Mosbah M., Tirira J., Clocchiatti R., Gosset J., and Massiot P. Hydrogen microdetermination in geological materials using elastic recoil detection analysis (ERDA). Nucl. Instrum. Methods Phys. Res. B 49 (1990) 340-344
43. Mosbah M., Clocchiatti R., Métrich N., Piccot D., Rio S., and Tirira J. The characterization of glass inclusions through nuclear microprobe. Nucl. Instrum. Methods Phys. Res. B 104 (1995) 271-275
44. Newman S., Stolper E.M., and Epstein S. Measurement of water in rhyolitic glasses: calibration of an infrared spectroscopic technique. Am. Miner. 71 (1986) 1527-1541
45. Ohtani E. Water in the mantle. Elements 1 (2005) 25-30
46. Paterson M. The determination of hydroxyl by infrared absorption in quartz silicate glasses and similar materials. Bull. Miner. 105 (1982) 20-29
47. Raepsaet C., Bureau H., Khodja H., Aubaud C., and Carraro A. μ-ERDA developments in order to improve the water content determination in hydrous and nominally anhydrous mantle phases. Nucl. Instrum. Methods Phys. Res. B 266 (2008) 1333-1337
48. Reichart P., Dollinger G., Bergmaier A., Datzmann G., Hauptner A., and Körner H.-J. Sensitive 3D hydrogen mcroscopy by proton-proton scattering. Nucl. Instrum. Methods Phys. Res. B 197 (2002) 134-149
49. Rossman G. R. (2006) Analytical methods for measuring water in nominally anhydrous minerals, In Water in nominally anhydrous minerals. Reviews in Mineralogy and Geochemistry, vol 62, (eds. H. Keppler and J. R. Smith). pp. 1-28.
50. Sambridge M., Gerald J.F., Kovacs I., O'Neill H.St.C., and Hermann J. Quantitative absorbance spectroscopy with unpolarized light: Part I. Physical and mathematical development. Am. Miner. 93 (2008) 751-764
51. Shao L., Wang Y.Q., Nastasi M., and Mayer J.W. A technique to study lattice location of light elements in silicon by channelling elastic recoil detection analysis. Nucl. Instrum. Methods Phys. Res. B 249 (2006) 230-233
52. Sie S.H., Suter G.F., Chekhmir A., and Green T.H. Microbeam recoil detection for the study of hydration of minerals. Nucl. Instrum. Methods Phys. Res. B 104 (1995) 261-265
53. Skogby, H. (2006) In Water in Natural Mantle Minerals I: Pyroxenes. Reviews in Mineralogy and Geochemistry, MSA, 62, (eds. H. Keppler and J. R. Smith). pp. 155-167.
54. 2O storage and recycling in the mantle. Earth Planet. Sci. Lett. 137 (1995) 45-55
55. Stolper E.M. Water in silicate glasses: an infrared spectroscopic study. Contrib. Miner. Petro. 81 (1982) 1-17
56. Sweeney R.J., Prozesky V.M., and Springhorn K.A. Use of the elastic recoil detection analysis (ERDA) microbeam technique for the quantitative determination of hydrogen in materials and hydrogen partitioning between olivine and melt at high pressures. Geochim et Cosmochim. Acta 61 (1997) 101-113
57. Thomas R. Determination of the water contents of granite melt inclusions by confocal laser Raman microprobe spectroscopy. Am. Miner. 85 (2000) 868-872
58. Visonà D., Caironi V., Carraro A., Dallai L., Fioretti A.M., and Fanning M. Zircon megacrysts from the basalts of the Venetian Volcanic Province (NE Italy). U-Pb age, oxygen isotope and REE. Lithos 94 (2007) 168-180
59. Wegden M., Kristiansson P., Pastuovic Z., Skogby H., Auzelyte V., Elfman M., Malmqvist K.G., Nilsson C., Pallon J., and Shariff A. Hydrogen analysis by p-p scattering in geological material. Nucl. Instrum. Methods Phys. Res. B 219-220 (2004) 550-554
60. Wegdén M., Kristiansson P., Skogby H., Auzelyte V., Elfman M., Malmqvist K.G., Nilsson C., Pallon J., and Shariff A. Hydrogen depth profiling by p-p scattering in nominally anhydrous minerals. Nucl. Instrum. Methods Phys. Res. B 231 (2005) 524-529