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Bis-urea 2 did not form nanotubes at room temperature in any solvent tested: in chloroform, 2 forms the same filaments as 1 (Table 1); in dodecane, 2 is not soluble.
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Bis-urea 2 did not form nanotubes at room temperature in any solvent tested: in chloroform, 2 forms the same filaments as 1 (Table 1); in dodecane, 2 is not soluble.
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Up to now, our efforts to find a direct spectroscopic signature of the encapsulated solvent have been unsuccessful, because of the very broad NMR signal for bis-ureas 1 and 2 in nonpolar solvents.
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Up to now, our efforts to find a direct spectroscopic signature of the encapsulated solvent have been unsuccessful, because of the very broad NMR signal for bis-ureas 1 and 2 in nonpolar solvents.
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46
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For the rheological characterization of solutions of bis-urea 1: Ducouret, G.; Chassenieux, C.; Martins, S.; Lequeux, F.; Bouteiller, L. J. Colloid Interface Sci., 2007, 310, 624-629.
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