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64549111524
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note
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Operating conditions: Column Phenomenex Luna (C18, 150 × 4.6 mm, 5 μm); Solvent system: gradient elution, 0-10 min, acetonitrile:water (1:1); 10-35 min, acetonitrile:water (70:30); 36-40 min, acetonitrile:water (1:1).
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