Quantitative determination of the 1,3-butadiene urinary metabolite 1,2-dihydroxybutyl mercapturic acid by high-performance liquid chromatography/tandem mass spectrometry using polynomial calibration curves

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 877, Issue 13, 2009, Pages 1388-1393

  Carrieri, Mariella ^a   Bartolucci, Giovanni Battista ^a   Livieri, Monica ^a   Paci, Enrico ^b   Pigini, Daniela ^b   Sisto, Renata ^b   Corsetti, Federica ^b   Tranfo, Giovanna ^b  

^a UNIVERSITY OF PADOVA   (Italy)

^b ISPESL   (Italy)

Author keywords

1,3 Butadiene; Biological monitoring; DHBMA; HPLC MS MS; Method validation; Occupational exposure; Polynomial regression

Indexed keywords

1,3-BUTADIENE; BIOLOGICAL MONITORING; DHBMA; HPLC-MS/MS; METHOD VALIDATION; OCCUPATIONAL EXPOSURE; POLYNOMIAL REGRESSION;

ACIDS; CALIBRATION; EXTRACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLISM; METABOLITES; POLYNOMIAL APPROXIMATION; SYNTHETIC RUBBER;

BUTADIENE;

1,2 DIHYDROXYBUTYLMERCAPTURIC ACID; 1,3 BUTADIENE; ACETYLCYSTEINE DERIVATIVE; UNCLASSIFIED DRUG;

ACCURACY; ANALYTIC METHOD; ARTICLE; CALIBRATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; METABOLITE; NORMAL HUMAN; POLYNOMIAL CALIBRATION CURVE; PRIORITY JOURNAL; QUANTITATIVE ASSAY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; URINALYSIS; URINE LEVEL; VALIDATION PROCESS;

ACETYLCYSTEINE; BUTADIENES; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; QUALITY CONTROL; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; TANDEM MASS SPECTROMETRY; UNCERTAINTY;

EID: 64149115109     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2009.02.005     Document Type: Article

References (33)

1. Brunnemann K.D., Kagan M.R., Cox J.E., and Hoffman D. Carcinogenesis 11 (1990) 1863
2. Himmelstein M.W., Acquavella J.F., Recio L., Mendisky M.A., and Bond J.A. Crit. Rev. Toxicol. 27 (1997) 1
3. Natusch D.F.S., and Tomkins B.A. Anal. Chem. 50 (1978) 1429
4. International Agency for Research on Cancer. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans: 1,3-Butadiene (1992), World Health Organization, Lyon
5. Löfroth G., Burton R.M., Forehand L., Hammond S.K., Seila R.L., Zweidinger R.B., and Lewtas J. Environ. Sci. Technol. 23 (1989) 610
6. International Agency for Research on Cancer. Re-evaluation of Some Organic Chemicals, Hydrazine and Hydrogen Peroxide. Monographs on the Evaluation of the Carcinogenic Risk of Chemicals to Humans (1999), World Health Organization, Lyon
7. K. Phillips, A.M. McKenna, D.A. Howard, M.C. Bentley, J.N. Cook, Le Collane della Fondazione Salvatore Maugeri, Pavia, 1997, p. 33.
8. Owen P., Glaister J., Gaunt I., and Pullinger D. Am. Ind. Hyg. Assoc. J. 48 (1987) 407
9. Melnick R.L., Huff J., Chou B.J., and Miller R.A. Cancer. Res. 50 (1990) 6592
10. Santos-Burgoa C., Matanoski G., Zeger S., and Schwartz L. Am. J. Epidemiol. 136 (1992) 843
11. Cochrane J.E., and Skopek T.R. Carcinogenesis 15 (1994) 713
12. Cochrane J.E., and Skopek T.R. Carcinogenesis 15 (1994) 719
13. Cheng H., Sathiakumar N., Graff J., Matthews R., and Delzell E. Chem. Biol. Interact. 166 (2007) 15
14. ACGIH. Threshold Limit Values and Biological Exposure Indices (2008), ACGIH, Cincinnati, OH
15. USEPA. An SAB Report: Review of the Health Risk Assessment of 1,3-Butadiene (1998), Science Advisory Board, Washington, DC
16. NIOSH. Recommendations for Occupational Safety and Health. Compendium of Policy Document and Statements (1992), NIOSH, Cincinnati, OH
17. Deutsche Forschungsgemeinschaft. MAK-und BAT-Werte-Liste 2008, Senatskommission zur Prüfung gesundheitsschädlicher Arbeitsstoffe (2008), Wiley/VCH, Weinheim
18. Csanady G., Guengerich F., and Bond J. Carcinogenesis 13 (1992) 1142
19. Thornton-Manning J.R., Dahl A.R., Bechtold W.E., Griffith Jr. W.C., and Henderson R.F. Carcinogenesis 16 (1995) 1723
20. van Sittert N.J., Megens H.J., Watson W.P., and Boogaard P.J. Toxicol. Sci. 56 (2000) 189
21. Boogaard P.J., van Sittert N.J., and Megens H.J. Chem. Biol. Interact. 135-136 (2001) 695
22. Sabourin P.J., Burka L.T., Bechtold W.E., Dahl A.R., Hoover M.D., Chang I.Y., and Henderson R.F. Carcinogenesis 13 (1992) 1633
23. Bechtold W.E., Strunk M.R., Chang I.Y., Ward J.B., and Henderson R.F. Toxicol. Appl. Pharmacol. 127 (1994) 44
24. Sapkota A., Halden R.U., Dominici F., Groopman J.D., and Buckley T.J. Chem. Biol. Interact. 160 (2006) 70
25. Urban M., Gilch G., and Schepers G. J. Chromatogr. B 796 (2003) 131
26. McDonald J.D., Bechtold W.E., Krone J.R., Blackwell W.B., Kracko D.A., and Henderson R.F. J. Anal. Toxicol. 28 (2004) 168
27. Matuszewski B.K., Constanzer M.L., and Chavez-Eng C.M. Anal. Chem. 75 (2003) 3019
28. The International Conference on Harmonization. Validation of Analytical Procedure: Methodology (Q 2B) (1996), Food and Drug Administration, USA
29. Picò Y., Farrè M., Soler C., and Barcelò D. J. Chromatogr. A 1176 (2007) 123
30. Fayed A.S., Shehata M.A., Ashour A., Hassan N.Y., and Weshahy S.A. J. Pharm. Biomed. Anal. 5 (2007) 407
31. Sakamoto Y., Ishiguro M., and Kitagawa G. Akaike Information Criterion Statistics (1986), D. Reidel Publishing Company, Tokyo
32. EURACHEM/CITAC Guide CG4 Quantifying Uncertainty in Analytical Measurement, EURACHEM, 2000.
33. Fustinoni S., Perbellini L., Soleo L., Manno M., and Foà V. Toxicol. Lett. 149 (2004) 353