Effect of seeds on the dry-gel synthesis and catalytic performance of titanosilicalite-1

Kuei Suan Jen Hsueh Pao/ Journal of the Chinese Ceramic Society

Volumn 37, Issue 3, 2009, Pages 453-457

  Zhang, Haijiao ^a,b   Liu, Yueming ^a   Jiao, Zheng ^b   Nguyen, Manhtai ^b   Wu, Peng ^a   He, Mingyuan ^a  

^a EAST CHINA NORMAL UNIVERSITY   (China)

^b SHANGHAI UNIVERSITY   (China)

Author keywords

Catalytic performance; Dry gel conversion; Seed; Synthesis; Titanosilicalite 1 zeolite

Indexed keywords

GELATION; GELS; SCANNING ELECTRON MICROSCOPY; SILICA; SYNTHESIS (CHEMICAL); TITANIUM; ZEOLITES;

CATALYTIC PERFORMANCE; COOPERATIVE EFFECTS; CRYSTAL SEEDS; CRYSTAL SIZES; CRYSTALLINITY; DRY-GEL CONVERSION; DRY-GEL CONVERSION METHODS; FUMED SILICAS; GEL SYNTHESIS; HIGH ACTIVITIES; LOW COSTS; MOLE RATIOS; PHYSICAL AND CHEMICAL PROPERTIES; SCANNING ELECTRON MICROSCOPES; SYNERGISTIC EFFECTS; SYNTHESIS; TETRABUTYLORTHOTITANATE; TETRAPROPYLAMMONIUM HYDROXIDES; TITANIUM SOURCES; TITANOSILICALITE-1 ZEOLITE; X- RAY DIFFRACTIONS;

CATALYST ACTIVITY;

EID: 63749120545     PISSN: 04545648     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (17)

1. TAMASSO M, PEREGO G, NOTARI B. Preparation of porous crystalline synthetic material comprised of silicon and titanium oxide[P]. US Patent, 4410501, 1983.
2. THANGARAJ A, EAPEN M J, SIVASANKER S, et al. Studies on the synthesis of titanium silicalite TS-1[J]. Zeolites, 1992, 12(8): 943-950.
3. LI Mingfeng, GUO Xinwen, WANG Xiangsheng. Chin J Catal (in Chinese), 1997, 18(4): 269-270.
4. GUO Xinwen, LI Gang, WANG Xiangsheng. J Dilian Univ Tech (in Chinese), 1998, 38(3): 359-362.
5. TUEL A. Crystallization of titanium silicalite-1 (TS-1) from gels containing[J]. Zeolites, 1996, 16(2/3): 108-117.
6. LI Gang, GUO Xinwen, WANG Xiangsheng, et al. Synthesis of titanium silicalites in different template systems and their catalytic performance[J]. Appl Catal A, 1999, 185(1): 11-18.
7. 2 solids: Influence of the synthesis variables[J]. Appl Catal, A: General, 1995, 124(2): 391-408.
8. WANG Liqin, WANG Xiangsheng, GUO Xinwen. Chin J Catal (in Chinese), 2003, 24(2): 132-136.
9. ZHANG Haijiao, LIU Yueming, WU Haihong, et al. Hydrothermal synthesis of hexamethyleneimine-templated TS-1 titanosilicate supported by active seeds[J]. Chem. Lett, 2006, 35(11): 1276-1277.
10. XU W Y, DONG J, LI J, WU F. A novel method for the preparation of zeolite ZSM-5[J]. J Chem Soc, Chem Commun, 1990, 10: 755-756.
11. MASAHIKO MATSUKATA, NORIKAZU NISHIYAMA, KOREKAZU UEYAMA. Crystallization of FER and MFI zeolites by a vapor-phase transport method[J]. Micro Mater, 1996, 7: 109-117.
12. PENG Wu, TAKAYUKI MIYAJI, LIU Yueming, et al. Synthesis of Ti-MWW by a dry-gel conversion method[J]. Catal Today, 2005, 99: 233-240.
13. TATSUMI T, JAPPAR N. Properties of Ti-beta zeolites synthesized by a dry gel conversion method and hydrothermal method[J]. J Phys Chem B, 1998, 102(37): 7126-7131.
14. ZHANG Xiaoming, DING Yong, PENG Zhiguang, et al. A preparation method of titanium silicalite zeolite[P]. CN Patent 1327947, 2001.
15. JIE Jia, WU Baolin, ZHOU Jicheng. Fine Chem Inter (in Chinese), 2001, 31(2): 18-21.
16. XU Ruren, PAN Wenqin. Inorganic Synthesis and Preparative Chemistry (in Chinese). Beijing: Higher Education Press, 2002: 429-430.
17. XIA Q H, TATSUMI T. Crystallization kinetics of nanosized Tiβ zeolites with high oxidation activity by a dry-gel conversion technique[J]. Mater Chem Phys, 2005, 89: 89-98.