Practical assessment of frictional heating effects and thermostat design on the performance of conventional (3 μm and 5 μm) columns in reversed-phase high-performance liquid chromatography

Journal of Chromatography A

Volumn 1216, Issue 18, 2009, Pages 3961-3969

  Fallas, Morgane M ^a   Hadley, Mark R ^b   McCalley, David V ^a  

^a UNIVERSITY OF THE WEST OF ENGLAND   (United Kingdom)

^b ASTRAZENECA   (United Kingdom)

Author keywords

Column efficiency; Frictional heating; HPLC; Retention

Indexed keywords

AIR HEATERS; AXIAL TEMPERATURE GRADIENTS; COLUMN EFFICIENCY; DEAD VOLUMES; FRICTIONAL HEATING; HEATING EFFECTS; HEATING SYSTEMS; HPLC; INTERNAL DIAMETERS; MOBILE-PHASE VELOCITIES; OVEN TEMPERATURES; PRACTICAL INVESTIGATIONS; RADIAL TEMPERATURE GRADIENTS; RETENTION; REVERSED-PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHIES; WATER BATHS;

AIR PREHEATERS; CHROMATOGRAPHIC ANALYSIS; FRICTION; HEATING EQUIPMENT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; PARTICLE SIZE; PLASMAS; TEMPERATURE SENSORS; THERMAL EFFECTS; THERMAL GRADIENTS; THERMOSTATS; TOLUENE;

HEATING;

TOLUENE;

ANALYTIC METHOD; ARTICLE; BATH; FLOW RATE; FRICTION; HEATING; PARTICLE SIZE; PRIORITY JOURNAL; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; THERMOREGULATION;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; EQUIPMENT DESIGN; PARTICLE SIZE; RESINS, SYNTHETIC; TEMPERATURE;

EID: 63649105157     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.03.007     Document Type: Article

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