Understanding two-pulse phase-modulated decoupling in solid-state NMR

Journal of Chemical Physics

Volumn 130, Issue 11, 2009, Pages

  Scholz, Ingo ^a   Hodgkinson, Paul ^b   Meier, Beat H ^a   Ernst, Matthias ^a  

^a ETH ZURICH   (Switzerland)

^b DURHAM UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHASE MODULATION; RESONANCE; SPIN DYNAMICS;

ANALYTICAL EXPRESSIONS; CONTINUOUS WAVES; DECOUPLING TECHNIQUES; EFFECTIVE HAMILTONIANS; EXPERIMENTAL PARAMETERS; FLOQUET; FLOQUET APPROACHES; HETERONUCLEAR; HOMONUCLEAR; LIMITING FACTORS; LINE-WIDTHS; MAGIC-ANGLE SPINNINGS; ORGANIC SOLIDS; PHASE CHANGES; PULSE PHASE; RADIO FREQUENCIES; RESIDUAL COUPLINGS; RESONANCE CONDITIONS; SOLID-STATE NMR; SPIN DIFFUSIONS; SPIN SYSTEMS;

LINEWIDTH;

EID: 63149118012     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.3086936     Document Type: Article

References (48)

1. M. Ernst, J. Magn. Reson. JMARF3 1090-7807 10.1016/S1090-7807(03)00074-0 162, 1 (2003).
2. P. Hodgkinson, Prog. Nucl. Magn. Reson. Spectrosc. PNMRAT 0079-6505 10.1016/j.pnmrs.2005.04.002 46, 197 (2005).
3. M. Mehring, Principles of High Resolution NMR in Solids, 2nd ed. (Springer, Berlin, 1983).
4. I. J. Shannon, K. D. M. Harris, and S. Arumugan, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/0009-2614(92)85999-Q 196, 588 (1992).
5. M. Ernst, H. Zimmermann, and B. H. Meier, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(99)01423-2 317, 581 (2000).
6. G. Sinning, M. Mehring, and A. Pines, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/0009-2614(76)85325-0 43, 382 (1976).
7. M. Mehring and G. Sinning, Phys. Rev. B PRBMDO 0163-1829 10.1103/PhysRevB.15.2519 15, 2519 (1977).
8. A. E. Bennett, C. M. Rienstra, M. Auger, K. V. Lakshmi, and R. G. Griffin, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.470372 103, 6951 (1995).
9. Z. H. Gan and R. R. Ernst, Solid State Nucl. Magn. Reson. SSNRE4 0926-2040 10.1016/S0926-2040(96)01294-5 8, 153 (1997).
10. Y. L. Yu and B. M. Fung, J. Magn. Reson. JMARF3 1090-7807 10.1006/jmre.1997.1322 130, 317 (1998).
11. B. M. Fung, A. K. Khitrin, and K. Ermolaev, J. Magn. Reson. JMARF3 1090-7807 10.1006/jmre.1999.1896 142, 97 (2000).
12. A. Khitrin and B. M. Fung, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.480805 112, 2392 (2000).
13. K. Takegoshi, J. Mizokami, and T. Terao, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(01)00525-5 341, 540 (2001).
14. G. Gerbaud, F. Ziarelli, and S. Caldarelli, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(03)01056-X 377, 1 (2003).
15. G. De Pape, B. Elena, and L. Emsley, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.1773155 121, 3165 (2004).
16. R. S. Thakur, N. D. Kurur, and P. K. Madhu, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/j.cplett.2006.06.007 426, 459 (2006).
17. G. De Pape, P. Hodgkinson, and L. Emsley, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(03)00966-7 376, 259 (2003).
18. M. Ed́n and M. H. Levitt, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.479410 111, 1511 (1999).
19. J. Leppert, O. Ohlenschläger, M. Görlach, and R. Ramachandran, J. Biomol. NMR JBNME9 0925-2738 10.1023/B:JNMR.0000032614.79833.3d 29, 319 (2004).
20. G. De Pape, A. Lesage, and L. Emsley, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.1595088 119, 4833 (2003).
21. G. De Pape, D. Sakellariou, P. Hodgkinson, S. Hediger, and L. Emsley, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(02)01808-0 368, 511 (2003).
22. P. Tekely, P. Palmas, and D. Canet, J. Magn. Reson., Ser. A JMRAE2 1064-1858 10.1006/jmra.1994.1059 107, 129 (1994).
23. A. Detken, E. H. Hardy, M. Ernst, and B. H. Meier, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(02)00335-4 356, 298 (2002).
24. M. Ernst, A. Samoson, and B. H. Meier, Chem. Phys. Lett. CHPLBC 0009-2614 348, 293 (2001).
25. M. Ernst, A. Samoson, and B. H. Meier, J. Magn. Reson. JMARF3 1090-7807 10.1016/S1090-7807(03)00155-1 163, 332 (2003).
26. M. Ernst, M. A. Meier, T. Tuherm, A. Samoson, and B. H. Meier, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja0494510 126, 4764 (2004).
27. M. Kotecha, N. P. Wickramasinghe, and Y. Ishii, Magn. Reson. Chem. MRCHEG 0749-1581 10.1002/mrc.2151 45, S221 (2007).
28. X. Filip, C. Tripon, and C. Filip, J. Magn. Reson. JMARF3 1090-7807 176, 239 (2005).
29. G. De Pape, N. Giraud, A. Lesage, P. Hodgkinson, A. Böckmann, and L. Emsley, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja037213j 125, 13938 (2003).
30. U. Haeberlen, High Resolution NMR in Solids: Selective Averaging (Academic, New York, 1976).
31. M. Ernst, S. Bush, A. C. Kolbert, and A. Pines, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.472224 105, 3387 (1996).
32. A. Khitrin, T. Fujiwara, and H. Akutsu, J. Magn. Reson. JMARF3 1090-7807 10.1016/S1090-7807(02)00173-8 162, 46 (2003).
33. M. Carravetta, M. Ed́n, X. Zhao, A. Brinkmann, and M. H. Levitt, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(00)00340-7 321, 205 (2000).
34. M. Baldus, T. O. Levante, and B. H. Meier, Z. Naturforsch., A: Phys. Sci. ZNASEI 0932-0784 49a, 80 (1994).
35. E. Vinogradov, P. K. Madhu, and S. Vega, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(00)01006-X 329, 207 (2000).
36. E. Vinogradov, P. K. Madhu, and S. Vega, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.1408287 115, 8983 (2001).
37. R. Ramesh and M. S. Krishnan, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.1354147 114, 5967 (2001).
38. M. Ernst, A. Samoson, and B. H. Meier, J. Phys. Chem. JPCHAX 0022-3654 123, 064102 (2005).
39. J. R. Sachleben, J. Gaba, and L. Emsley, Solid State Nucl. Magn. Reson. SSNRE4 0926-2040 10.1016/j.ssnmr.2005.09.009 29, 30 (2006).
40. R. Ramachandran, V. S. Bajaj, and R. G. Griffin, J. Chem. Phys. JCPSA6 0021-9606 122, 164503 (2005).
41. M. Ernst, H. Geen, and B. H. Meier, Solid State Nucl. Magn. Reson. SSNRE4 0926-2040 10.1016/j.ssnmr.2005.08.004 29, 2 (2006).
42. M. Leskes, R. S. Thakur, P. K. Madhu, N. D. Kurur, and S. Vega, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.2746039 127, 024501 (2007).
43. I. Scholz, B. H. Meier, and M. Ernst, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.2800319 127, 204504 (2007).
44. P. Hodgkinson, PNMRSIM, a general simulation program for large problems in solid-state NMR. Available from: http://www.durham.ac.uk/paul.hodgkinson/ pNMRsim/ (2008).
45. V. E. Zorin, M. Ernst, S. P. Brown, and P. Hodgkinson, J. Magn. Reson. JMARF3 1090-7807 192, 183 (2008).
46. H. J. Reich, M. Jautelat, M. T. Messe, F. J. Weigert, and J. D. Roberts, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja01054a037 91, 7445 (1969).
47. B. Birdsall, N. J. M. Birdsall, and J. Feeney, J. Chem. Soc., Chem. Commun. JCCCAT 0022-4936 1972, 316 (1972).
48. G. De Pape, M. J. Bayro, J. Lewandowski, and R. G. Griffin, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja0550430 128, 1776 (2006).