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Volumn 37, Issue 12, 2008, Pages 1216-1217

Abrupt spin transitions and LIESST effects observed in Fe II spin-crossover complexes with extended π-conjugated schiff-base ligands having N 4O 2 donor sets

(8) Kuroda Sowa, Takayoshi a Yu, Zhong a Senzaki, Yuka a Sugimoto, Kunihisa b,d Maekawa, Masahiko a Munakata, Megumu a Hayami, Shinya c,e Maeda, Yonezo c

a KINKI UNIVERSITY (Japan)

b RIGAKU CORPORATION (Japan)

c KYUSHU UNIVERSITY (Japan)

d JAPAN SYNCHROTRON RADIATION RESEARCH INSTITUTE (Japan)

e HIROSHIMA UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 63149110813 PISSN: 03667022 EISSN: 13480715 Source Type: Journal
DOI: 10.1246/cl.2008.1216 Document Type: Article

Times cited : (22)

References (16)

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- Anal. Calcd for C41H28Cl2FeN4 1.CH2C12: C, 66.96; H, 3.84; N, 7.62, Found: C, 66.14; H, 4.22; N, 7.70, Anal. Calcd for C40H26FeN 4O2 1:C, 73.85; H, 4.03; N, 8.61, Found: C, 72.55; H, 4.56; N, 9.28
- 2 1:C, 73.85; H, 4.03; N, 8.61%. Found: C, 72.55; H, 4.56; N, 9.28%.

10
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- Crystal data for 1-CH2C12 at 123.1 K: C 41 H28Cl2FeN4O2, M r, 735.46, Triclinic, space group P Ī (no. 2, a, 12.201(6, b= 12.550(6, c, 12.985(7) Å, a, 98.064(3)°, β= 116.469(8)°, γ= 110.004(7)°, V, 1568.1(14) Å3, Z, 2, Dcalcd, 1.558gcm 3, μ(MoKα, 0.701cm-1. At 293.1 K: Triclinic, space group PĪ (no. 2, a, 11.988(2, b, 12.631(2, c= 13.462(3)Å, α, 97.96(2)°, 0=117.36(2)°, γ, 108.30(3)°, V, 1619.3(9) Å3, Z, 2, D calcd, 1.508 gcm-3, μ(MoKα, 0.676cm -1. Data collections were performed on a RIGAKU SATURN CCD diffractometer (MoKα, λ, 0.71073 Å) with θ ranges of 2.1 ≦ θ ≦ 27.1
- 2 of 0.1830 for all 5546 reflections. CCDC 282609 & 282610. The obtuse cell choice at 293.1 K is converted from the original acute set (a = 11.988(2), b = 12.631(2), c = 13.289(2) Å, a = 64.94(2)° β = 64.12(2)°, γ = 71.70(2)°) for the easy comparison to the 123.1 K data.

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- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/index.html.
- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journals/chem-lett/index.html.

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