Mild hydrothermal synthesis, crystal structure, thermal behavior, spectroscopic and magnetic properties of the (NH4)[Fe(AsO4)1-x (PO4)xF] (x=0.3, 0.6, 0.8) series. Thermal transformation of (NH4)[Fe(AsO4)0.7(PO4) 0.3F]

Journal of Solid State Chemistry

Volumn 182, Issue 4, 2009, Pages 932-941

  Berrocal, Teresa ^a   Mesa, José L ^a   Pizarro, José L ^a   Bazán, Begoña ^a   Lezama, Luis ^a   Arriortua, María I ^a   Rojo, Teófilo ^a  

^a UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

Author keywords

Crystal structure; ESR; IR and UV Vis spectroscopies; Iron(III) arsenates phosphates; Magnetism; Mild hydrothermal synthesis

Indexed keywords

AMMONIUM COMPOUNDS; ANTIFERROMAGNETISM; COMPLEXATION; ELECTROSLAG REMELTING; HYDROTHERMAL SYNTHESIS; IRON COMPOUNDS; MAGNETIC PROPERTIES; NEON; OXYGEN; PHOSPHATES; SINGLE CRYSTALS; SPIN DYNAMICS; THREE DIMENSIONAL;

AIR ATMOSPHERES; ANTIFERRO-MAGNETIC INTERACTIONS; BET SURFACE AREAS; CRYSTALLOGRAPHIC AXES; DIFFUSE REFLECTANCE SPECTRUM; ELECTRONIC MICROSCOPIES; ELECTRONIC TRANSITIONS; ESR; ESR SPECTRUM; EXTERNAL CAVITIES; G VALUES; HIGH SPINS; IR AND UV-VIS SPECTROSCOPIES; LOW TEMPERATURES; MAGNETIC MEASUREMENTS; MILD HYDROTHERMAL CONDITIONS; MILD HYDROTHERMAL SYNTHESIS; OCTAHEDRAL GEOMETRIES; ROOM TEMPERATURES; SPACE GROUPS; SPIN-CANTING; THERMAL BEHAVIORS; THERMAL TRANSFORMATIONS; THREE-DIMENSIONAL FRAMEWORKS; UNIT CELL PARAMETERS; VISIBLE REGIONS;

CRYSTAL STRUCTURE;

EID: 63149098374     PISSN: 00224596     EISSN: 1095726X     Source Type: Journal    
DOI: 10.1016/j.jssc.2009.01.026     Document Type: Article

References (52)

1. Cheetham A.K., Férey G., and Loiseau T. Angew. Chem. Int. Ed. 38 (1999) 3268
2. Davis M.E. Chem. Eur. J. 3 11 (1997) 1745
3. Moore P.B. In: Niagru J., and Moore P.B. (Eds). Crystallochemical Aspects of the Phosphate Minerals (1984), Springer, Berlin
4. Feng S., and Xu R. Acc. Chem. Res. 34 (2001) 239
5. Yu J., and Xu R. Acc. Chem. Res. 36 (2003) 481
6. Williams I.D., Wum M.M., Sung H.H.-Y., Zang X.X., and Yu J. Chem. Commun. (1998) 2463
7. Chem J., Li L., Yang G., and Xu R.R. J. Chem. Soc. Chem. Commun. (1989) 1217
8. Rao C.N.R., Sampathkumaran E.V., Nagarajan R., Paul G., Behera J.N., and Choudhury A. Chem. Mater. 16 (2004) 1441 and references therein
9. Behera J.N., Ayi A.A., and Rao C.N.R. Chem. Commun. (2004) 968 and the references therein
10. Haushalter R.C., Wang Z., Meyer L.M., Dhingra S.S., Thompson M.E., and Zubieta J. Chem. Mater. 6 (1994) 3845
11. Wang S.-L., and Lee Y.-H. Inorg. Chem. 33 (1994) 3845
12. Gagnard F., Resiner C., and Tremel W. Inorg. Chem. 36 (1997) 352
13. Harrison W.T.A., Phillips M.L.F., Chavez A.V., and Nenoff T.M. J. Mater. Chem. 9 (1999) 3087
14. Ekambaram S., and Sevov S.C. Inorg. Chem. 39 (2000) 2405
15. Bazan B., Mesa J.L., Pizarro J.L., Lezama L., Arriortua M.I., and Rojo T. Inorg. Chem. 39 (2000) 6056
16. Bazan B., Mesa J.L., Pizarro J.L., Goñi A., Lezama L., Arriortua M.I., and Rojo T. Inorg. Chem. 40 (2001) 5691
17. Bazan B., Mesa J.L., Pizarro J.L., Arriortua M.I., and Rojo T. Mater. Res. Bull. 38 (2003) 3820
18. Bazan B., Mesa J.L., Pizarro J.L., Lezama L., Garitaonandia J.S., Arriortua M.I., and Rojo T. Solid State Sci. 5 (2003) 1291
19. Bazan B., Mesa J.L., Pizarro J.L., Peña A., Arriortua M.I., and Rojo T. Z. Anorg. Allg. Chem. 631 (2006) 2026
20. Bazan B., Mesa J.L., Pizarro J.L., Lezama L., Peña A., Arriortua M.I., and Rojo T. J. Solid State Chem. 179 (2006) 1485
21. Berrocal T., Mesa J.L., Pizarro J.L., Bazán B., Iglesias M., Aguayo A.T., Arriortua M.I., and Rojo T. Chem. Commun. (2008) 4738
22. Chakrabarti S., and Natarajan S. Angew. Chem. Int. Ed. 11 (2002) 1224
23. Férey G. Chem. Mater. 13 (2001) 3084
24. Estermann M., McCusker L.B., Baerlocher C., Merrouche A., and Kessler H. Nature (1991) 352
25. Loiseau T., and Ferey G. J. Solid Sate Chem. 111 (1994) 309
26. Sassoye C., Loisseau T., Taulelle F., and Ferey G. Chem. Commun. (2000) 943
27. Sassoye C., Marrot J., Loisseau T., and Ferey G. Chem. Mater. 14 (2002) 1340
28. Guillou N., Gao Q., Foster P.M., Chang J.-S., Nogues M., Park S.-E., Ferey G., and Cheetham A.K. Angew. Chem. Int. Ed. 40 (2001) 2831
29. Ferey G. J. Fluorine Chem. 72 (1995) 187
30. Fernandez S., Mesa J.L., Pizarro J.L., Lezama L., Arriortua M.I., Olazcuaga R., and Rojo T. Chem. Mater. 12 (2000) 2092
31. Cavellec M., Riou D., Greneche J.M., and Ferey G. Inorg. Chem. 36 (1977) 2187
32. Luo S.-H., Jiang Y.-C., Wang S.-L., Kao H.-M., and Lii K.-H. Inorg. Chem. 40 (2001) 5381
33. Bazan B., Mesa J.L., Pizarro J.L., Garitaonandia J.S., Arriortua M.I., and Rojo T. Solid State Sci. 5 (2003) 1291
34. Zhang P., Wang Y., Zhu G., Shi Z., Liu Y., Yuan H., and Pang W. J. Solid State Chem. 154 (2000) 368
35. Bazan B., Mesa J.L., Pizarro J.L., Rodríguez-Fernandez J., Sanchez-Marcos J., Roig A., Molins E., Arriortua M.I., and Rojo T. Chem. Mater. 16 (2004) 5249
36. Loisseau T., Calage Y., Lacorre P., and Ferey G. J. Solid State Chem. 111 (1994) 390
37. Hagerman M.E., and Poeppelmeier K.R. Chem. Mater. 7 (1995) 602
38. CRYSALIS, version 171.32.5; Oxford Diffraction Ltd.: Oxford, 2007.
39. Sheldrick, G.M. SHELXL97. Program for the Refinement of Crystal Structures; University of Göttingen: Göttingen, Germany, 1997.
40. E. Dowty, ATOMS, A computer program for displaying atomic structures, shape sotware, 521 Hidden Valley Road, Kingsport, TN, 1993.
41. Zabrodsky H., Peles S., and Avnir D. J. Am. Chem. Soc. 114 (1992) 7843-7851
42. Prinsky M., and Avnir D. Inorg. Chem. 37 (1998) 5575-5582
43. Powder Diffraction File-Inorg and Organic, Files (a) 84-876, (b) 21-410 Pennsylvannia, 1995.
44. Arroyo M.E., Gallardo J.M., and Amador M. Electrochem. Solid State Lett. A 564-A569 (2005) 18
45. Nakamoto K. Infrared and Raman Spectra of Inorganic and Coordination Compounds (1997), Wiley, New York
46. Lever A.B.P. Inorganic Electronic Spectroscopy (1984), Elsevier, Amsterdam
47. Sugano T.Y. J. Phys. Soc. Jpn. 9 (1954) 753
48. Bencini A., and Gatteschi D. EPR of Exchange Coupled Systems (1990), Springer, Berlin/Heidelberg
49. Wijn H.W., Walker L.R., Daris J.L., and Guggenheim H. J. Solid State Commun. 11 (1972) 803
50. Richards P.M., and Salamon M.B. Phys. Rev. B 9 (1974) 32
51. Escuer A., Vicente R., Goher M.A.S., and Mautner F. Inorg. Chem. 34 (1995) 5707
52. Cheung T.T.P., Soos Z.G., Dietz R.E., and Merrit F.R. Phys. Rev. B 17 (1978) 1266