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Volumn 20, Issue 5, 2009, Pages 554-556

The new synthesis of sesquiterpenoids 10-bromo-α-chamigrene

Author keywords

10 Bromo chamigrene; Carbonyl coupling; Halogenated sesquiterpenoids; Synthesis

Indexed keywords

EID: 62849094912 PISSN: 10018417 EISSN: None Source Type: Journal
DOI: 10.1016/j.cclet.2009.01.029 Document Type: Article

Times cited : (5)

References (18)

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- Spectral data of compound 5: 1H NMR (CDCl3-TMS, 400 MHz, δppm, 1.68, s, 6H, CH3)2C{double bond, long}CH, 5.12 (m, 1H, CH{double bond, long}C, 2.05 (m, 2H, CH2CH{double bond, long, 2.05 (t, 2H, CH2C(CH3){double bond, long, 1.60 (S, 3H,CH3C(CH2){double bond, long, 2.29 (t, 4H, CH2)2C{double bond, long, 1.27 (t, 4H, CH2CO)2, 3.96 (s, 4H, CH2O)2, 13C NMR CDCl3-TMS, 400 MHz, δppm, 17.83, 27.38, 25.98, 18.47, 34.56, 26.93, 27.21, 36.23, 35.96, 64.47, 109.29, 124.58, 126.26, 130.33, 131.72
- 3-TMS, 400 MHz, δppm): 17.83, 27.38, 25.98, 18.47, 34.56, 26.93, 27.21, 36.23, 35.96, 64.47, 109.29, 124.58, 126.26, 130.33, 131.72.

11
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18
- 62849122804
- Spectral data of 10-bromo-α-chamigrene: 1H NMR (CDCl3-TMS, 400 MHz, δppm, 1.68, s, 3H, CH3C(C){double bond, long}CH, 1.60 (t, 3H, CH3C(CH2){double bond, long, 1.66, d, 6H, CH3)2CHBr, 2.79 (m, 2H, CH2CHBr, 2.31 (t, 2H, CH2(C)CH{double bond, long, 2.07 (t, 2H, CH2C{double bond, long, 2.02 (t, 2H, CH2CH2, 5.84 (t, 1H, CH{double bond, long}C (CH3, 4.29 (d, 1H, CH{double bond, long}C (CH3, 3.39 (m, 1H, CHBr, 13C NMR (CDCl3-TMS, 400 MHz, δppm, 12.40, 19.87, 21.23, 25.97, 28.32, 28.41, 31.09, 35.56, 44.04, 58.84, 66.54, 124.09, 125.86, 129.10, 130.24. C15H23Br, m/z 283, 285 (M, 1, 203 (42, 135 (22, 119 (33, 109 (100, 95 65
- +), 203 (42), 135 (22), 119 (33), 109 (100), 95 (65).

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