Synthesis of highly regular mesoporous Al-MCM-41 from metakaolin

Applied Clay Science

Volumn 44, Issue 1-2, 2009, Pages 185-188

  Wang, GuangJian ^a,b   Wang, Yuran ^c   Liu, Yiwu ^a   Liu, Zhengwang ^a   Guo, YaJie ^a   Liu, Guangqing ^a   Yang, Zhengxing ^a   Xu, MingXia ^b   Wang, Lei ^a  

^a HUAIBEI NORMAL UNIVERSITY   (China)

^b TIANJIN UNIVERSITY   (China)

^c SHANGHAI JIAO TONG UNIVERSITY   (China)

Author keywords

Al MCM 41; Mesoporous molecular sieves; Metakaolin

Indexed keywords

ADSORPTION; ALUMINA; ALUMINUM; DESORPTION; FOURIER TRANSFORM INFRARED SPECTROSCOPY; FOURIER TRANSFORMS; MOLECULAR SIEVES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SIEVES; SILICA; SPECTROSCOPIC ANALYSIS; SYNTHESIS (CHEMICAL);

AL-MCM-41; ALUMINUM SOURCES; CETYL TRI METHYL AMMONIUM BROMIDES; FOURIER TRANSFORM INFRA-RED SPECTROSCOPIES; HYDROTHERMAL CONDITIONS; IN-SITU SYNTHESIZED; ISOTHERMAL ADSORPTIONS; MAGIC-ANGLE SPINNINGS; MESOPOROUS; MESOPOROUS MOLECULAR SIEVES; METAKAOLIN; NMR SPECTROSCOPIES; POWDER X-RAY DIFFRACTIONS; SEM AND TEM; SI SOURCES; SI/AL RATIOS; STRUCTURE DIRECTING AGENTS; TETRAETHYL ORTHOSILICATE;

MESOPOROUS MATERIALS;

FTIR SPECTROSCOPY; KAOLIN; MINERAL SYNTHESIS; MOLECULAR ANALYSIS; NUCLEAR MAGNETIC RESONANCE; POROUS MEDIUM; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION;

EID: 62349125964     PISSN: 01691317     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.clay.2008.12.002     Document Type: Article

References (12)

1. Corma A., Fornes V., Navarro M.T., and Perezpariente J. Acidity and stability of MCM-41 crystalline aluminosilicates. J. Catal. 148 (1994) 569-574
2. - 1 band. J. Chem. Soc., Chem. Commun. 6 (1993) 557-559
3. Eimer G.A., Pierella L.B., Monti G.A., et al. Preparation and characterization of aluminium-containing MCM-41. Catal. Commun. 4 (2003) 118-123
4. Fang K., Ren J., and Sun Y. Synthesis and characterization of steam-stable AlMCM-41. Mater. Chem. Phys. 90 (2005) 16-21
5. Gregg S.J., and Sing K.S.W. Adsorption Surface Area and Porosity. Second ed. (1982), Academic Press, New York
6. Kang F., Wang Q.Y., and Xiang S.H. Synthesis of mesoporous Al-MCM-41 materials using metakaolin as aluminum source. Mater. Lett. 59 (2005) 1426-1429
7. Kim J.H., Tanabe M., and Niwa M. Characterization and catalytic activity of the Al-MCM-41 prepared by a method of gel equilibrium adjustment. Microporous Mater. 10 (1997) 85
8. Kiseler A.V., and Lygin V.I. Infrared Spectra of Surface Compounds and Adsorbed Substances (1992), Nauka, Moscow (in Russian)
9. Kresge C.T., Leonowicz M.E., Roth W.J., et al. Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism. Nature 359 (1992) 710-712
10. Landau M.V., Varkey S.P., Herskowitz M., et al. Wetting stability of Si-MCM-41 mesoporous material in neutral, acidic and basic aqueous solutions. Microporous Mesoporous Mater. 33 (1999) 149-163
11. Luan Z.H., Cheng C.F., Zhou W.Z., et al. Mesopore molecular sieve MCM-41 containing framework aluminum. J. Phys. Chem. 99 (1995) 1018-1024
12. Pauly T.R., Liu Y., Pinnavaia T.J., et al. Textural mesoporosity and the catalytic activity of mesoporous molecular sieves with wormhole framework structures. J. Am. Chem. Soc. 121 (1999) 8835-8842