SCOPUS 정보 검색 플랫폼

Synlett

Volumn , Issue 5, 2009, Pages 0828-0832

An easy one-pot synthesis of tetrasubstituted 3-alkynylpyrroles via multicomponent coupling reaction

(3) Chen, Xueming a Hou, Lei a Li, Xingshu a

a SUN YAT SEN UNIVERSITY (China)

Author keywords

Multicomponent reactions; Pyrroles; Tetrasubstituted 3 alkynylpyrroles

Indexed keywords

EID: 62349104845 PISSN: 09365214 EISSN: 14372096 Source Type: Journal
DOI: 10.1055/s-0028-1087952 Document Type: Article

Times cited : (20)

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- General Procedure for the Preparation of Imines To a round-bottomed flask containing the amine (10 mmol) in toluene (20 mL) was added anhyd Na2SO4 (50 mmol, The mixture was stirred, and then ethyl glyoxalate (12 mmol) was added slowly. After the reaction was completed (about 1 h, monitored by TLC, Na2SO4 was removed by filtration, and toluene was distilled under reduced pressure to yield the crude imine (95% yield, which was used for the next step without purification. General Procedure for the Preparation of Pyrrole Derivatives To a flask containing phenylacetylene (6 mmol, a 1.2 M solution of Me2Zn in toluene (6 mmol) was added at r.t. The resulting solution was stirred for 1 h, and then the imine (1 mmol) in toluene (1 mL) was added at the same temperature. The reaction mixture was stirred for 5 h. After the reaction was completed (monitored by TLC, it was quenched by addition of H2O 5 mL, The mix
- +]: 347.1679; found: 347.1680.

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