Experimental characterization and population balance modeling of the polymorph transformation of L-glutamic acid

Crystal Growth and Design

Volumn 9, Issue 1, 2009, Pages 243-252

  Cornell, Jeroen ^a   Lindenberg, Christian ^a   Mazzotti, Marco ^a  

^a ETH ZURICH   (Switzerland)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61649097086     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg800387a     Document Type: Article

References (33)

1. Scholl, J.; Lindenberg, C.; Vicum, L.; Brozio, J.; Mazzotti, M. Precipitation of alpha L-glutamic acid: determination of growth kinetics. Faraday Discuss. 2007, 136, 247-264.
2. Lindenberg, C.; Mazzotti, M. J. Cryst. Growth, submitted.
3. Hilflker, R., Polymorphism: In the Pharmaceutical Industry, 1st ed.; Wiley-VCH: Weinheim, Germany, 2006.
4. Bernstein, J.; Davey, R. J.; Henck, J. O. Concomitant polymorphs. Angew. Chem., Int. Ed. 1999, 38 (23), 3441-3461.
5. Scholl, J.; Bonalumi, D.; Vicum, L.; Mazzotti, M.; Muller, M. In situ monitoring and modeling of the solvent-mediated polymorphic transformation of L-glutamic acid. Cryst. Growth Des. 2006, 6 (4), 881-891.
6. Qu, H. Y.; Louhi-Kultanen, M.; Rantanen, J.; Kallas, J. Solvent-mediated phase transformation kinetics of an anhydrate/hydrate system. Cryst. Growth Des. 2006, 6 (9), 2053-2060.
7. Borissova, A.; Jammoal, Y.; Javed, K. H.; Lai, X.; Mahmud, T.; Penchev, R.; Roberts, K. J.; Wood, W. Modeling the precipitation of L-glutamic acid via acidification of monosodium glutantate. Cryst. Growth Des. 2005, 5 (3), 845-854.
8. Ono, T.; Kramer, H. J. M.; ter Horst, J. H.; Jansens, P. J. Process modeling of the polymorphic transformation of L-glutamic acid. Cryst. Growth Des. 2004, 4 (6), 1161-1167.
9. Caillet, A.; Sheibat-Othman, N.; Fevotte, G. Crystallization of monohydrate citric acid. 2. Modeling through population balance equations. Cryst. Growth Des. 2007, 7 (10), 2088-2095.
10. Aaltonen, J.; Kogermann, K.; Strachan, C. J.; Rantanen, J. In-line monitoring of solid-state transitions during fluidisation. Chem. Eng. Sci. 2007, 62 (1-2), 408-415.
11. Strachan, C. J.; Rades, T.; Gordon, K. C.; Rantanen, J. Raman spectroscopy for quantitative analysis of pharmaceutical solids. J. Pharm. Pharmacol. 2007, 59 (2), 179-192.
12. Santos, J. C.; Reis, M. M.; Machado, R. A. F.; Bolzan, A.; Sayer, C.; Giudici, R.; Araujo, P. H. H. Online monitoring of suspension polymerization reactions using Raman spectroscopy. Ind. Eng. Chem. Res. 2004, 43 (23), 7282-7289.
13. Reis, M. M.; Araujo, P. H. H.; Sayer, C.; Giudici, R. In situ near-infrared spectroscopy for simultaneous monitoring of multiple process variables in emulsion copolymerization. Ind. Eng. Chem. Res. 2004, 43 (23), 7243-7250.
14. Fevotte, G.; Alexandre, C.; Nida, S. O. A population balance model of the solution-mediated phase transition of citric acid. AIChE J. 2007, 53 (10), 2578-2589.
15. Cornel, J.; Lindenberg, C.; Mazzotti, M. Quantitative application of in situ ATR-FTIR and Raman spectroscopy in crystallization processes. Ind. Eng. Chem. Res. 2008, 47 (14), 4870-4882.
16. Scholl, J.; Vicum, L.; Muller, M.; Mazzotti, M. Precipitation of L-glutamic acid: Determination of nucleation kinetics. Chem. Eng. Technol. 2006, 29 (2), 257-264.
17. Sakata, Y. Studies on the polymorphism of L-glutamic acid. Part II. Measurement of solubilities. Agric. Biol. Chem. 1961, 25 (11), 835-837.
18. Kitamura, M. Crystallization Behavior and Transformation Kinetics of L-Histidine Polymorphs. J. Chem. Eng. Jpn. 1993, 26 (3), 303-307.
19. Worlitschek, J.; Hocker, T.; Mazzotti, M. Restoration of PSD from chord length distribution data using the method of projections onto convex sets. Part. Part. Syst. Charact. 2005, 22 (2), 81-98.
20. Kempkes, M.; Eggers, J.; Mazzotti, M. Measurement of particle size and shape by FBRM and in situ microscopy. Chem. Eng. Sci. 2008, 63 (19), 4656-4675.
21. Mersmann, A., Crystallization Technology Handbook, 2nd ed.; Marcel Dekker: New York, 2001.
22. Lindenberg, C.; Schöll, J.; Vicum, L.; Brozio, J.; Mazzotti, M. L-glutamic acid precipitation: agglomeration effects. Cryst. Growth Des. 2008, 8(1), 224-237.
23. Garside, J.; Davey, R. J. Secondary Contact Nucleation - Kinetics, Growth and Scale-Up. Chem. Eng. Commun. 1980, 4 (4-5), 393-424.
24. Kraume, M., Mischen und Rühren, 1st ed.; Wiley-VCH: Weinheim, Germany, 2003.
25. Kitamura, M.; Ishizu, T. Growth kinetics and morphological change of polymorphs of L-glutamic acid. J. Cryst. Growth 2000, 209 (1), 138-145.
26. Davey, R. J.; Cardew, P. T.; McEwan, D.; Sadler, D. E. Rate Controlling Processes in Solvent-Mediated Phase-Transformations. J. Cryst. Growth 1986, 79 (1-3), 648-653.
27. Kumar, S.; Ramkrishna, D., III. Nucleation, growth and aggregation of particles. Chem. Eng. Sci. 1997, 52 (24), 4659-4679.
28. Beck, J. V.; Arnold, K. J., Parameter Estimation in Engineering and Science, 1st ed.; John Wiley & Sons: New York, 1977.
29. Cardew, P. T.; Davey, R. J. The Kinetics of Solvent-Mediated Phase-Transformations. Proc. R. Soc. London, Ser. A 1985, 398 (1815), 415-428.
30. Ferrari, E. S.; Davey, R. J. Solution-mediated transformation of alpha to beta L-glutamic acid: Rate enhancement due to secondary nucleation. Cryst Growth Des. 2004, 4 (5), 1061-1068.
31. Cashell, C.; Sutton, D.; Corcoran, D.; Hodnett, B. K. Inclusion of the stable form of a polymorph within crystals of its metastable form. Cryst. Growth Des. 2003, 3 (6), 869-872.
32. Lacmann, R.; Herden, A.; Mayer, C. Kinetics of nucleation and crystal growth. Chem. Eng. Technol. 1999, 22 (4), 279-289.
33. Teychené, S.; Biscans, P. Nucleation Kinetics of Polymorphs: Induction Period and Interfacial Energy Measurements. Cryst Growth Des. 2008, 8(4), 1133-1139.