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61549132538
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-1): v 3450m (O-H), 1629s (C=O), 1599s (C=N).
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-1): v 3450m (O-H), 1629s (C=O), 1599s (C=N).
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27
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61549132846
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Crystal data for 1 (C18H21MnN 2O6, Mt, 416.31, triclinic, space group P1̄, a, 9.1082(18, b, 10.184(2, c, 11.642(2) Å, α, 65.43(3, β, 81.75(3, γ, 69.72(3)°, V, 921.3(3) Å3, Z, 2, p calcd, 1.501 g cm-3, μ(MoKα, 0.754 mm-1, R1, 0.0665, wR2, 0.1246 (all data, T, 293 K. Crystal data for 2 (C17H 17MnN2O5, Mt, 384.27, monoclinic, space group P21/c, a, 10.550(2, b, 8.5260(17, c, 18.152(4) Å, β, 97.26(3)°, V, 1619.7(6) Å3, Z, 4, pcalcd, 1.576 g cm -3, μ(MoKα, 0.847 mm-1, R1, 0.0256, wR2, 0.0729 all data
-
-1, R1 = 0.0256, wR2 = 0.0729 (all data), T = 293 K.
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30
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32544448395
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Rodriguez, V.8
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