Effects of cooling rate and solution concentration on solution crystallization of L-glutamic acid in an oscillatory baffled crystallizer

Crystal Growth and Design

Volumn 8, Issue 8, 2008, Pages 2875-2881

  Ni, Xiongwei ^a   Liao, Anting ^a  

^a HERIOT WATT UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61549123333     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg7012039     Document Type: Article

References (34)

1. Hennessy, A.; Neville, A.; Roberts, K. J. In-situ SAXS/WAXS and turbidity studies of the structure and composition of multi-homologous n-alkane waxes crystallised in the absence and presence of flow improving additive species. Cryst. Growth Des. 2004, 4, 1069-1078.
2. 3+) in nearly perfect single crystals of potassium dihydrogen phosphate (KDP) as examined by X-ray standing waves, X-ray absorption spectroscopy and molecular modelling. Chem. Mater. 2005, 17, 4053-4061.
3. Borissova, A.; Dashova, Z.; Lai, X.; Roberts, K. J. Examination of the semi-batch crystallisation of benzophenone from saturated methanol solution via aqueous anti-solvent drowning-out as monitored in-process using ATR FTIR spectroscopy. Cryst. Growth Des. 2004, 4, 1053-1060.
4. Yu, Z.; Chow, P. S.; Tan, R. B. H. Application of attenuated total reflectance-Fourier transform infrared (ATR-FTIR) technique in the monitoring and control of anti-solvent crystallization. Ind. Eng. Chem. Res. 2006, 45 (1), 438-444.
5. Mougin, P.; Wilkinson, D.; Roberts, K. J. In situ ultrasonic attenuation spectroscopic study of the dynamic evolution of particle size during solution-phase crystallization of urea. Cryst. Growth Des. 2003, 3, 67-72.
6. Rousseau, R. W.; Barthe, S. In Using FBRM Measurements, Fines Destruction and Varying Cooling Rates to Control Paracetamol CSD in a Batch Cooling Crystallizer; The 2005 Annual Meeting of AIChE, Cincinnati, 2005.
7. Chew, J. W.; Shan, A. C. P.; B.H., R. T. Automated in-line technique using FBRM to achieve consistent product quality in cooling crystallization. Cryst. Growth Des. 2007, 7 (8), 1416-1422.
8. Lu, J.; Chow, P. S.; Carpenter, K. Phase transitions in lysozyme solutions characterized by differential scanning calorimetry. Prog. Cryst. Growth Charact. Mater. 2003, 46 (3), 105-129.
9. Braatz, R. D.; Hasebe, S. In Particle Size and Shape Control in Crystallization Processes; Chemical Process Control-CPC 6, Tucson, Arizona, USA, 2001; Tucson, Arizona, USA, 2001.
10. Jealous, A. C.; Johnson, H. F. Power requirements for pulse generation in pulse columns. Ind. Eng. Chem. 1955, 47, 1159-1166.
11. Nyvlt, J. Kinetics of Nucleation in Solution. J. Cryst. Growth 1968, 3 (4), 377-383.
12. Nyvlt, J.; Rychly, R.; Gottfried, J.; Wurzelova, J. Metastable Zone-Width of Some Aqueous Solution. J. Cryst. Growth 1970, 6, 151-162.
13. Liang, J. K. Process Scale Dependence of Batch Crystallisation L-Glutamic Acid from Aqueous Solution in Relation to Reactor Internals, Reactant Mixing and Process Conditions; Heriot-Watt University: Edinburgh, 2002.
14. Liang, K.; G., W.; Wikinson, D.; Ford, L. J.; Roberts, K. J.; Wood, W. M. L. An Examination into the effect of stirrer material and agitation rate on the nucleation of L-glutamic acid batch crystallized from supersaturated aqueous solutions. Cryst. Growth Des. 2004, 4 (5), 1039-1044.
15. Smith, L. A.; Roberts, K. J.; Machin, D.; McLeod, G. An examination of the solution phase and nucleation properties of sodium, potassium and rubidium dodecyl sulphastes. J. Cryst. Growth 2001, 226, 158-167.
16. Karel, M.; Nyvlt, J.; Chianese, A. Crystallization of pentaerythritol I. Solubility, density and metastable zone width. Collect. Czech. Chem. Commun. 1994, 59, 1261-1269.
17. Lee, J. H.; Kim, J. H.; Zhu, I. H.; Zhan, X. B.; Lee, J. W.; Shin, D. H.; Kim, S. K. Optimisation of conditions for the production of pullulan and high molecular weight pullulan by Aureobasidium pullulans. Biotechnol. Lett. 2001, 23, 817-820.
18. Gron, H.; Mougin, P.; Thomas, A.; White, G.; Wilkinson, D. Dynamic in-process examination of particle size and crystallographic form under defined conditions of reactant supersaturation as associated with the batch crystallisation of monosodium glutamate from aqueous solution. Ind. Eng. Chem. Res. 2003, 42, 4888-4898.
19. Gerson, A. R.; Roberts, K. J.; Sherwood, J. N. An instrument for the examination of nucleation form solution and its application to the study of precipitation from diesel fuels and solution of n-alkanes. Power Technol. 1991, 65, 243-249.
20. Garside, J.; Mersmann, A.; Nyvlt, J. In Measurement of Crystal Growth and Nucleation Rate; IChemE: UK, 2002; pp 156-169.
21. Cheon, Y. H. K.; Kim, S.-H. A study on crystallization kinetics of pentaerythritol in a batch cooling crystallizer. Chem. Eng. Sci. 2005, 60, 4791-4802.
22. Mullin, J. W., Crystallisation; Butterworth-Heinnemann: Oxford, UK, 1993.
23. Martini, S., Herrera, M. L., and Hartel, R. W. Effect of Cooling Rate on Nucleation Behaviour of Milk Fat-Sunflower Oil Blends J. Agric. Food Chem. 2001, 43, 3223-3229.
24. Rielly, C. Power Numbers for Impellers; 2006.
25. Wood, W. M. L. Crystal Science Techniques in the Manufacture of Chiral Compounds; John Wiley and Sons Ltd.: New York, 1997.
26. Burton, W. K.; Cabrera, N.; Frank, F. C. The Growth of Crystals and the Equilibrium Structure of Their Surface. Phil. Transact. 1951, A243, 299-358.
27. Kitamura, M. In Situ Observation of Growth Process of a-L-Glutamic Acid with Atomic Force Microscopy. J. Colloid Interface Sci. 2000, 224, 311-316.
28. Cashell, C.; Corcoran, D.; Hodnett, B. K. Secondary nucleation of the β-polymorph of the L-glutamic acid on the surface of α-form crystals. Chem. Commun. 2003, 3, 374-375.
29. Kitamura, M. Polymorphism in the crystallisation of L-glutamic acid. J. Cryst. Growth 1989, 96, 541-546.
30. Ono, T.; Kramer, H. J. M.; ter Horst, J. H.; Jansens, P. J. Process modeling of the polymorphic transformation of L-glutamic acid. Cryst. Growth Des. 2004, 4 (6), 1161-1167.
31. Ostwald, W. Studien uber die bilding und umwandlung fester korpe. Zeitshright fur Physikalische Chemie; In Wolde, P. R., Frenkel, D. 1999. Homogeneous nucleation and the Ostwald step rule 1897, 22, 289-330.
32. Wolde, P. R.; Frenkel, D. Homogeneous nucleation and the ostwald step rule. Phys. Chem. Chem. Phys. 1999, 1, 2191-2196.
33. Garside, J.; Davey, R. J. Secondary contact nucleation: kinetics, growth and scale-up. Chem. Eng. Commun. 1980, 4, 393-424.
34. Kitamura, M. Controlling factor of polymorphism in crystallization process. J. Cryst. Growth 2002, 237-239, 2205-2214.