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Crystal Growth and Design

Volumn 8, Issue 11, 2008, Pages 3902-3904

A new "opened-cube" (H2O)10 cluster and undulated water chain in porous metal-organic frameworks

(5) Wang, Li Yan a Yang, Yuan a Liu, Kui a Li, Bao Long a Zhang, Yong a

a SOOCHOW UNIVERSITY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61549105584 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg800484k Document Type: Article

Times cited : (118)

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- Preparation of 1 and 2: A solution of H4btec (0.026 g, 0.1 mmol) in 10 mL of H2O was adjusted to approximately pH 6 with dilute Et3N solution. Then btb (0.058 g, 0.3 mmol) in 10 mL of CH 3OH was added. This mixture was added to one side of the H-shape tube, and Cd(NO3)·3H2O (0.062 g, 0.2 mmol) in 20 mL of water was added to the other side of the H-shape tube. Colorless crystals of 1 were obtained in 65% yield (0.081 g) after one month. Anal. Calcd. For C34H58Cd 2N18O18: C, 33.15; H, 4.75; N, 20.47. Found: C, 33.04; H, 4.68; N, 20.36, 2 was prepared as for 1 by using H 2phth instead of H4btec. The reaction reagents were H 2phth (0.033 g, 0.2 mmol, btb (0.019 g, 0.1 mmol) and Cd(NO 3) 3H2O (0.062 g, 0.2 mmol, Colorless crystals of 2 were obtained in 52% yield 0.046 g, Anal. Ca
- 15.50: C, 32.74; H, 4.01; N 9.55. Found: C, 32.67; H, 3.94; N, 9.51 (%).

44
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- Crystal data for 1: C34H58Cd2N 18O18, Mr, 1231.78, monoclinic, space group P21/c, a, 12.6665(16, b, 18.196(2, c, 10.9031(14) Å, β, 103.115(3)°, V, 2447.4(5) Å3, Z, 2, Dc, 1.672 g cm -3, μ, 0.958 mm-1, 4455 [R(int, 0.0503] unique reflections, 4028 data with I > 2σ(I, 353 parameters, R1, 0.0405, wR2, 0.0941, S, 1.089. 2: C24H35Cd2N6O15.50, Mr, 880.38, monoclinic, space group P2 1/c, a, 14.5197(14, b, 11.0769(10, c, 21.106(2) A, β, 107.720(2)°, V, 3233.5(6) Å3, Z, 4, Dc, 1.808 g.cm-3, μ, 1.395 mm-1,5891 [Rint, 0.0254
- 2 = 0.0615, S = 1.072.

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