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1H NMR spectroscopy. The disappearance of the resonances arising from the aldehyde protons in 2 or m-tolualdehyde (δ = 9.9-10.1) and the simultaneous appearance of resonances arising from the imine protons in 3 or 4 (δ = 8.4-8.5) were monitored. Concentration vs time profiles were constructed by deconvolution of these resonances.
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1H NMR spectroscopy. The disappearance of the resonances arising from the aldehyde protons in 2 or m-tolualdehyde (δ = 9.9-10.1) and the simultaneous appearance of resonances arising from the imine protons in 3 or 4 (δ = 8.4-8.5) were monitored. Concentration vs time profiles were constructed by deconvolution of these resonances.
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