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Crystal Growth and Design

Volumn 8, Issue 5, 2008, Pages 1471-1473

Guest control in the self-assembly of H-shaped host to cyclopentanoid (5,43) net

(3) Thakuria, Ranjit a Sarma, Bipul a Nangia, Ashwini a

a UNIVERSITY OF HYDERABAD (India)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 61449172856 PISSN: 15287483 EISSN: 15287505 Source Type: Journal
DOI: 10.1021/cg800089v Document Type: Article

Times cited : (19)

References (22)

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- Crystallographic data: (1a) 0.5·CH3NO 2: C34H32N2O8, M, 596.62 g mol-1, colorless block, size 0.28 × 0.12 × 0.08 mm3, orthorhombic, space group Pbca, a, 14.959(3) Å, b, 9.0758(16) Å, c, 22.131(4) Å, V, 3004.5(10) Å3, Z, 4, μ, 0.095 mm-1, ρcal, 1.319 g cm-3, F000, 1256, T, 298(2) K, 2θmax, 50.0°, 9523 reflections collected, 2647 unique (Rint, 0.0691, GOF, 1.003, R1, 0.0582, wR2, 0.1060, 1525 observed reflections with I > 2σ(I, 208 parameters, 1a) 0.5·CH3NO2: C 34H32N2O8, M, 596.62 g mol -1, colorless needle, size 0.44 × 0.06 × 0.06 mm 3, monoclinic, space group P
- int = 0.0645), GOF = 1.001, R1 = 0.0655, wR2 = 0.1213, 1777 observed reflections with I > 2σ(I), 248 parameters. X-ray reflections on single crystals were collected on Bruker Smart Apex CCD diffractometer using Mo-Kα radiation (λ = 0.71073 Å). SMART was used for collecting frames, indexing reflections, and determining lattice parameters. SAINT was used for integration of reflections intensity and scaling. Friedel pairs were merged. Absorption correction was done in SADABS and SHELX-TL was used for space group determination, structure solution, and least-squares refinements on F2. Structures were solved by the direct methods and non-hydrogen atoms were refined anisotropically. Hydrogen atoms of O-H group were refined from difference Fourier maps and other hydrogen atoms (C-H) were generated geometrically and allowed to ride on the bound heavy atoms. X-Seed was used to prepare figures.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.