LC-MS and LC-PDA vs. phytochemical analysis of Colchicum brachyphyllum

Pharmazie

Volumn 63, Issue 12, 2008, Pages 860-865

  Alali, Feras Q ^a   Tahboub, Y R ^a   Al Daraysih, I S ^a   El Elimat, T ^a  

^a JORDAN UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Jordan)

Author keywords

[No Author keywords available]

Indexed keywords

2,3 DINORDEMECOLCINE; 3 NORCOLCHICINE; 3 NORDEMECOLCINE; ALKALOID DERIVATIVE; ANDROBIPHENYLINE; APIGENIN; BETA LUMICOLCHICINE; COLCHICINE; CORNIGERINE; DEMECOLCINE; DEMECOLCINONE; UNCLASSIFIED DRUG; DYES, REAGENTS, INDICATORS, MARKERS AND BUFFERS;

ARTICLE; CHEMICAL ANALYSIS; COLCHICUM; COLCHICUM BRACHYPHYLLUM; DRUG STRUCTURE; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; NONHUMAN; PHYTOCHEMISTRY; RELIABILITY; VALIDITY; CHEMISTRY; FLOWER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PLANT LEAF; PLANT SEED; PLANT STEM; THIN LAYER CHROMATOGRAPHY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, THIN LAYER; COLCHICUM; FLOWERS; INDICATORS AND REAGENTS; MASS SPECTROMETRY; PLANT LEAVES; PLANT STEMS; SEEDS;

EID: 61449100467     PISSN: 00317144     EISSN: None     Source Type: Journal    
DOI: 10.1691/ph.2008.8639     Document Type: Article

References (30)

1. Ackermann B, Regg B, Colombo L, Stella S, Coutant J (1996) Rapid analysis of antibiotic-containing mixtures from fermentation broths by using liquid chromatography-Electrospray ionization-mass spectrometry and matrix-assisted laser desorption ionization-time-of-flight-mass spectrometry. J Am Soc Mass Spectrum 7: 1227-1237.
2. Alali F, El-Alali A (2005) LC-MS analysis of corms of Colchicum hierosolymitanum (Colchcaceae). Acta Pharma Turc 47: 143-150.
3. Alali F, Gharaibeh A, Ghawanmeh A, Tawaha K, Oberlies N (2008) Colchicinoids from Colchicum crocifolium Boiss.: A case study in dereplication strategies for (-)-colchicine and related analogs using LC-MS and LCPDA techniques. Phytochem Analysis 19: DOI: 10.1002/pca.1060.
4. Alali F, Ma'aya'h AS, Alkofahi A, Qandil A, Li C, Burgess JP, Wani MC, Oberlies NH (2006) A New colchicinoid from Colchicum tauri, an unexplored meadow saffron native to Jordan. Nat Prod Commun 1: 95-99.
5. Alali FQ, El-Elimat T, Li C, Qandil A, Alkofahi A, K Tawaha K, Burgess JP, Nakanishi Y, Kroll DJ, Navarro HA, III JOF, Wani MC, Oberlies NH (2005) New colchicinoids from a native Jordanian meadow saffron, Colchicum brachyphyllum: Isolation of the first naturally occurring dextrorotatory colchicinoid. J Nat Prod 68: 173-178.
6. Alvi K, Peterson J, Hofmann B (1995) Rapid identification of elaiophylin and geldanamycin in Streptomyces fermentation broths using CPC coupled with a photodiode array detector and LC-MS methodologies. J Ind Microbiol 15: 80-84.
7. Carmona M, Zalacain A, Sanchez AM, Novella JL, Alonso GL (2006) Crocetin esters, picrocrocin and its related compounds present in Crocus sativus stigmas and Gardenia jasminoides fruits. Tentative identification of seven new compounds by LC-ESI-MS. J Agr Food Chem 54: 973-979.
8. Chommadov B, Yusupov M, Sadykov A (1990) Photochemical isomers of tropolone alkaloids. Chem Nat Compd 26: 113-128.
9. Constant H, Beecher C (1995) A method for the dereplication of natural product extracts using electrospray HPLC/MS. Nat Prod Lett 6: 193-196.
10. Cordell GA, Shin YG (1999) Finding the needle in the haystack. The dereplication of natural product extracts. Pure Appl Chem 71: 1089-1094.
11. Freyer A, Zarga MA, Firdous S, Guinaudeau H, Shamma M (1987) Five new alkaloids from Colchicum ritchii. J Nat Prod 50: 684-689.
12. Ghisalberti E (1993) Detection and isolation of bioactive natural products. In: Colegate S, Molyneux R (ed.) Detection, isolation and structural determination. CRC Press, Inc, p. 9-57.
13. Hostettmann K, Wolfender J, Terreaux C (2001) Modern screening techniques for plant extracts. Pharm Biol 39: 18-32.
14. Jin M, Yang Y, Su B, Ren Q (2006) Rapid quantification and characterization of soya saponins by high-performance liquid chromatography coupled with electrospray mass spectrometry. J Chromatogr A 1108: 31-37.
15. Kingston D (1996) Natural products as pharmaceuticals and sources for lead structures. In: Meyer P (ed.) The practice of Medicinal Chemistry. Academic Press Limited, p. 101-116.
16. Liau B, Jong T, Lee M, Chen S (2007) LC-APCI-MS method for detection and analysis of tryptanthrin, indigo, and indirubin in Daqingye and Banlangen. J Pharm Biomed Anal 43: 346-335.
17. Liu A, Guo H, Ye M, Lin Y, Sun J, Xu M, Guo D (2007) Detection, characterization and identification of phenolic acids in Danshen using high-performance liquid chromatography with diode array detection and electrospray ionization mass spectrometry. J Chromatogr A 1161: 170-182.
18. Nielsen K, Smedsgaard J (2003) Fungal metabolite screening: database of 474 mycotoxins and fungal metabolites for dereplication by standardised liquid chromatography-UV-mass spectrometry methodology. J Chromatogr A 1002: 111-136.
19. Niessen WMA (1999) State-of-the-art in liquid chromatography-mass spectrometry. J Chromatogr A 856: 179-197.
20. O'Neil MJ, Smith A, Heckelman PE (2001) The Merck Index, Merck Research Laboratories, Division of Merck and Co., Inc., White House Station, NJ, p. 432.
21. Petsalo A, Jalonen J, Tolonen A (2006) Identification of flavonoids of Rhodiola rosea by liquid chromatography-tandem mass spectrometry. J Chromatogr A 1112: 224-231.
22. Rosso A, Zuccaro S (1998) Determination of alkaloids from the colchicine family by reversed-phase high-performance liquid chromatography. J Chromatogr A 825: 96-101.
23. Sarker S, Nahar L (2005) Hyphenated techniques. In: Sarker S, Latif Z, Gray AI (ed.) Natural Products Isolation. HUMANA Press, Totowa, New Jersey, p. 233-268.
24. Schultze AE, Roth RA (1993) Fibrinolytic activity in blood and lungs of rats treated with Monocrotaline pyrrole. Toxicol Appl Pharmacol 121: 129-137.
25. Sedlock D, Sun H, Smith W, Kawaoka K, Gillum A, Cooper R (1992) J Ind Microbiol 9: 45-52.
26. Smelcerovic A, Verma V, Spiteller M, Ahmad SM, Puri SC, Qazi GN (2006) Phytochemical analysis and genetic characterization of six Hypericum species from Serbia. Phytochemistry 67: 171-177.
27. Su Q, Rowley K, Balazs NDH (2002) Carotenoids: Separation methods applicable to biological samples. J Chromatogr B 781: 393-418.
28. Sun L, Rezaei KA, Temelli F, Ooraikul B (2002) Supercritical fluid extraction of alkylamides from Echinacea angustifolia. J Agr Food Chem 50: 3947-3953.
29. Tsao R, Yang R (2003) Optimization of a new mobile phase to know the complex and real polyphenolic composition: Towards a total phenolic index using high-performance liquid chromatography. J Chromatogr A 1018: 29-40.
30. Wolfender J, Queiroz EF, Hostettmann K (2006) The importance of hyphenated techniques in discovery of new lead compounds from nature. Exp Op Drug Discov 1: 237-260.