Reversed-phase high performance liquid chromatographic separation of diastereomers of β-amino alcohols and microwave assisted synthesis of Marfey's reagent, its chiral variants and diastereomers

Journal of Chromatography A

Volumn 1216, Issue 12, 2009, Pages 2592-2596

  Bhushan, Ravi ^a   Kumar, Rajender ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY ROORKEE   (India)

Author keywords

Amino alcohols; Amino acid variants; Indirect chiral separation; Marfey's reagent; Microwave assisted synthesis; Reversed phase high performance liquid chromatography

Indexed keywords

AMINO ACID AMIDES; CHIRAL DERIVATIZING REAGENTS; DIASTEREOMERS; INDIRECT CHIRAL SEPARATION; L-AMINO ACIDS; LIQUID CHROMATOGRAPHIC SEPARATIONS; MARFEY'S REAGENT; MICROWAVE ASSISTED SYNTHESIS; PHOSPHATE BUFFERS; REVERSED-PHASE; REVERSED-PHASE HIGH PERFORMANCE; REVERSED-PHASE HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; TRIFLUOROACETIC ACIDS;

ACETONITRILE; ALCOHOLS; AMIDES; AMINATION; AMINO ACIDS; BINARY MIXTURES; BODY FLUIDS; CHIRALITY; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIQUIDS; MICROWAVE IRRADIATION; ORGANIC ACIDS; SEPARATION; SYNTHESIS (CHEMICAL);

AMINES;

ACETONITRILE; AMIDE; AMINOALCOHOL; BETA AMINO ACID; MARFEY REAGENT; REAGENT; TRIFLUOROACETIC ACID; UNCLASSIFIED DRUG;

ANALYTICAL EQUIPMENT; ARTICLE; CHIRALITY; CONTROLLED STUDY; DERIVATIZATION; DIASTEREOISOMER; ENANTIOMER; MICROWAVE IRRADIATION; PRIORITY JOURNAL; RACEMIC MIXTURE; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SYNTHESIS;

ALANINE; AMINO ALCOHOLS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DINITROBENZENES; HYDROPHOBICITY; LINEAR MODELS; MICROWAVES; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; STEREOISOMERISM;

EID: 60649115204     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.01.045     Document Type: Article

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