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Volumn 50, Issue 15, 2009, Pages 1714-1716

Rhodium-copper-TBAF-catalyzed hydroarylation of alkynes with aryl Trimethoxysilanes

Author keywords

[No Author keywords available]

Indexed keywords

ALKYNE DERIVATIVE; COPPER; COPPER ACETATE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; RHODIUM; SILANE DERIVATIVE; TETRABUTYLAMMONIUM; TETRABUTYLAMMONIUM FLUORIDE; UNCLASSIFIED DRUG;

EID: 60649084427     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tetlet.2009.01.130     Document Type: Article
Times cited : (15)

References (30)
  • 18
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    • For review on the organozinc reagents, see:
    • For review on the organozinc reagents, see:. Knochel P., Almena Perea J.J., and Jones P. Tetrahedron 54 (1998) 8275
    • (1998) Tetrahedron , vol.54 , pp. 8275
    • Knochel, P.1    Almena Perea, J.J.2    Jones, P.3
  • 19
    • 14344266665 scopus 로고    scopus 로고
    • de Mejijere A., and Diederich F. (Eds), Wiley-VCH, Weinheim
    • Mitchell T.N. In: de Mejijere A., and Diederich F. (Eds). Metal-Catalyzed Cross-Coupling Reactions Vol. 1 (2004), Wiley-VCH, Weinheim 125-162
    • (2004) Metal-Catalyzed Cross-Coupling Reactions , vol.1 , pp. 125-162
    • Mitchell, T.N.1
  • 27
    • 0000604304 scopus 로고    scopus 로고
    • The rhodium-catalyzed regioselective hydroarylation reaction of 2-(2-phenylethynyl)pyridine with arylboronic acids, see:
    • The rhodium-catalyzed regioselective hydroarylation reaction of 2-(2-phenylethynyl)pyridine with arylboronic acids, see:. Lautens M., and Yoshida M. Org. Lett. 4 (2002) 123
    • (2002) Org. Lett. , vol.4 , pp. 123
    • Lautens, M.1    Yoshida, M.2
  • 29
    • 0000796405 scopus 로고    scopus 로고
    • Organosilanols have been reported to be reactive towards transmetallation with palladium, see:
    • Organosilanols have been reported to be reactive towards transmetallation with palladium, see:. Oi S., Honma Y., and Inoue Y. Org. Lett. 4 (2002) 667
    • (2002) Org. Lett. , vol.4 , pp. 667
    • Oi, S.1    Honma, Y.2    Inoue, Y.3
  • 30
    • 60649084983 scopus 로고    scopus 로고
    • note
    • 2 (4.9 mg, 5 mol %), toluene (3 mL) and alkynes (0.2 mmol) under atmosphere at room temperature. After stirring for 2 h, 60 μL of water was added, and the reaction mixture was continued to be stirred under atmosphere at reflux for 12 h. After the completion of the reaction, as monitored by TLC, the solvent was evaporated under reduced pressure and the residue was purified by flash column chromatography on a silica gel to give the product.


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