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60649084983
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note
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2 (4.9 mg, 5 mol %), toluene (3 mL) and alkynes (0.2 mmol) under atmosphere at room temperature. After stirring for 2 h, 60 μL of water was added, and the reaction mixture was continued to be stirred under atmosphere at reflux for 12 h. After the completion of the reaction, as monitored by TLC, the solvent was evaporated under reduced pressure and the residue was purified by flash column chromatography on a silica gel to give the product.
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