Optimization and validation of a liquid chromatography tandem mass spectrometry (LC/MSn) method for analysis of corticosteroids in bovine liver: Evaluation of Keyhole Limpet β-glucuronidase/sulfatase enzyme extract

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 877, Issue 7, 2009, Pages 635-644

  Croes, K ^a   Goeyens, L ^a,b   Baeyens, W ^a   Van Loco, J ^b   Impens, S ^b,c  

^a VRIJE UNIVERSITEIT BRUSSEL   (Belgium)

^b SCIENTIFIC INSTITUTE OF PUBLIC HEALTH   (Belgium)

^c ODISEE UNIVERSITY COLLEGE   (Belgium)

Author keywords

Bovine liver; Corticosteroids; Keyhole Limpet; Liquid chromatography tandem mass spectrometry; Spectrometry; Validation

Indexed keywords

ACETONITRILE; BLOOD VESSEL PROSTHESES; BODY FLUIDS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ELECTRIC CONDUCTIVITY MEASUREMENT; ENZYMATIC HYDROLYSIS; ENZYMES; ESTERS; ETHERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; HYDROLYSIS; LEAD; LIQUID CHROMATOGRAPHY; LIVER; MASS SPECTROMETERS; MASS SPECTROMETRY; METAL RECOVERY; METHANOL; ORGANIC SOLVENTS; SOLAR RADIATION; SOLVENTS; SPECTROMETERS; SPECTROMETRY; SPECTRUM ANALYSIS;

BOVINE LIVER; CORTICOSTEROIDS; KEYHOLE LIMPET; LIQUID CHROMATOGRAPHY TANDEM MASS SPECTROMETRY; VALIDATION;

EXTRACTION;

ACETIC ACID ETHYL ESTER; ACETONITRILE; ALDOSTERONE; BECLOMETASONE; BETA GLUCURONIDASE; CORTICOSTEROID; DEXAMETHASONE DERIVATIVE; ETHER; FLUOCINOLONE ACETONIDE; FLUOCINONIDE; FLUOROMETHOLONE; HYDROCORTISONE; ISOFLUPREDONE; KEYHOLE LIMPET BETA GLUCURONIDASE; KEYHOLE LIMPET SULFATASE; METHANOL; METHYLPREDNISOLONE; PREDNISOLONE; PREDNISONE; SULFATASE; TRIAMCINOLONE; TRIAMCINOLONE ACETONIDE; UNCLASSIFIED DRUG;

ANIMAL TISSUE; ARTICLE; CALIBRATION; CONTROLLED STUDY; COW; HELIX POMATIA; HYDROLYSIS; LIQUID CHROMATOGRAPHY; NONHUMAN; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; VALIDATION STUDY;

ADRENAL CORTEX HORMONES; ANIMALS; CATTLE; CHROMATOGRAPHY, LIQUID; GASTROPODA; GLUCURONIDASE; HELIX (SNAILS); HYDROLYSIS; LIVER; SULFATASES; TANDEM MASS SPECTROMETRY;

BOVINAE; HELIX POMATIA;

EID: 60449118150     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2009.01.028     Document Type: Article

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