Three-dimensional chemical analysis with synchrotron tomography at multiple X-ray energies: Brominated aromatic flame retardant and antimony oxide in polystyrene

Chemistry of Materials

Volumn 16, Issue 21, 2004, Pages 4032-4042

  Ham, Kyungmin ^a   Jin, Hua ^a,d   Al Raoush, Riyadh ^a   Xie, Xiaogang ^a   Willson, Clinton S ^a   Byerly, Gary R ^a   Simeral, Larry S ^b   Rivers, Mark L ^c   Kurtz, Richard L ^a   Butler, Leslie G ^a  

^a LOUISIANA STATE UNIVERSITY   (United States)

^b Aylbemarle Corp Proc Devmt Ctr   (United States)

^c UNIVERSITY OF CHICAGO   (United States)

^d Northwestern University   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ALGORITHMS; ANTIMONY COMPOUNDS; ATTENUATION; BINDING ENERGY; CONCENTRATION (PROCESS); DATA ACQUISITION; DIMERS; IMAGE ANALYSIS; MIXTURES; PARTICLE SIZE ANALYSIS; SYNCHROTRONS; SYNTHESIS (CHEMICAL); THREE DIMENSIONAL; X RAY ANALYSIS;

HIGH IMPACT POLYSTYRENE (HIPS); SYNCHROTRON TOMOGRAPHY; X RAY IMAGING; X RAY TOMOGRAPHY;

POLYSTYRENES;

ANTIMONY DERIVATIVE; ANTIMONY OXIDE; FLAME RETARDANT; PHTHALIMIDE DERIVATIVE; POLYSTYRENE; UNCLASSIFIED DRUG;

ALGORITHM; ARTICLE; BINDING AFFINITY; BROMINATION; CHEMICAL ANALYSIS; CONCENTRATION (PARAMETERS); ENERGY; PARTICLE SIZE; QUANTITATIVE ANALYSIS; SYNCHROTRON; X RAY ANALYSIS;

EID: 6044248955     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm0350333     Document Type: Article

References (32)

1. Marschallinger, R. Scanning 1998, 20, 65-73.
2. Jastrow, H.; Vollrath, L. Clin. Anat. 2003, 16, 44-54.
3. Center, P. S. The Visible Human Project at the Pittsburgh Supercomputing Center. http://www.psc.edu/biomed/research/VH/PVB/ (accessed September 2003).
4. Butler, L. G.; Cory, D. G.; Dooley, K. M.; Miller, J. B.; Garroway, A. N. J. Am. Chem. Soc. 1992, 114, 125-135.
5. Barrall, G. A.; Frydman, L.; Chingas, G. C. Science 1992, 255, 714-717.
6. Spanne, P.; Rivers, M. L. Nucl. Instrum. Methods Phys. Res., Sect. B 1987, B24-25, 1063-1067.
7. Flannery, B. P.; Deckman, H. W.; Roberge, W. G.; D'Amico, K. L. Science 1987, 237, 1439-1444.
8. D'Amico, K. L.; Deckman, H. W.; Dunsmuir, J. H.; Flannery, B. P.; Roberge, W. G. Rev. Sci. Instrum. 1989, 60, 1524-1526.
9. Deckman, H. W.; D'Amico, K. L.; Dunsmuir, J. H.; Flannery, B. P.; Gruner, S. M. Adv. X-Ray Anal. 1989, 32, 641-650.
10. Dunsmuir, J. H.; Ferguson, S. R.; D'Amico, K. L. Inst. Phys. Conf. Ser. 1992, 121, 257-264.
11. Spanne, P.; Thovert, J. F.; Jacquin, C. J.; Lindquist, W. B.; Jones, K. W.; Adler, P. M. Phys. Rev. Lett. 1994, 73, 2001-2004.
12. Butler, L. G.; Owens, J. W.; Cartledge, F. K.; Kurtz, R. L.; Byerly, G. R.; Wales, A. J.; Bryant, P. L.; Emery, E. F.; Dowd, B.; Xie, X. G. Environ. Sci. Technol. 2000, 34, 3269-3275.
13. Ellisman, M. H. National Center for Microscopy and Imaging Research: Xvoxtrace Version 2.3. http://ncmir.ucsd.edu/doc/Xvoxtrace.html (accessed June 2003).
14. Lohmann, G. Volumetric Image Analysis; Wiley-Teubner: New York, 1998.
15. Lindquist, W. B.; Lee, S.-M.; Coker, D. A.; Jones, K. W.; Spanne, P. J. Geophys. Res. B 1996, 101, 8297-8310.
16. Oh, W.; Lindquist, W. B. IEEE Pattern Anal. Machine Intelligence 1999, 21, 590-602.
17. Al-Raoush, R. I.; Thompson, K.; Willson, C. S. Soil Sci. Am. J. 2003, 67, 1687-1700.
18. Al-Raoush, R. I.; Willson, C. S. J. Hydrol. 2004, in press.
19. Krill, C. E., III.; Döbrich, K. M.; Michels, D.; Michels, A.; Rau, C.; Weitkamp, T.; Snigirev, A. A.; Birringer, R. Proc. SPIE-Int. Soc. Opt. Eng. 2002, 4503, 205-212.
20. Wan, S. Y.; Ritman, E. L.; Higgins, W. E. 2002, 32, 55-71.
21. Ratnanather, J. T.; Botteron, K. N.; Nishino, T.; Massie, A. B.; Lal, R. M.; Patel, S. G.; Peddi, S.; Todd, R. D.; Miller, M. I. Validating cortical surface analysis of medial prefrontal cortex. In Neuroimage, 2001; Vol. 14, pp 1058-1069.
22. Elmoutaouakkil, A.; Fuchs, G.; Bergounhon, P.; Péres, R.; Peyrin, F. J. Phys. D: Appl. Phys. 2003, 36, A37-43.
23. NIST, NIST XCOM: Photon Cross Sections Database, http://physics.nist.gov/ PhysRefData/Xcom/Text/XCOM.html (accessed June 2003).
24. Litzenburger, A. Polym. Polym, Compos. 2000, 8, 581-592.
25. De Schryver, D.; Landry, S. D.; Reed, J. S. Polym. Degrad. Stab. 1999, 64, 471-477.
26. Simonson, M. Polym. Mater. Sci. Eng. 2000, 83, 90-91.
27. Albemarle, Albemarle Corp. Saytex brochure page, http://www.albemarle. com/saytexbro.htm (accessed June, 2003).
28. Radloff, D.; Spiess, H. W.; Books, J. T.; Dowling, K. C. J. Appl. Polym. Sci. 1996, 60, 715-720.
29. Mrse, A. A.; Lee, Y.; Bryant, P. L.; Fronczek, F. R.; Butler, L. G.; Simeral, L. S. Chem. Mater. 1998, 10, 1291-1300.
30. Harwell, C. R.; Mrse, A. A.; Shelby, A. I.; Butler, L. G.; Hall, R. W. J. Phys. Chem. A 1999, 103, 8088-8092.
31. Rivers, M. L.; Rivers, M. L. Tutorial Introduction to X-ray Computed Microtomography http://www-fp.mcs.anl.gov/xray-cmt/rivers/tutorial.html (accessed June 2003).
32. Chantler, C.; Tran, C.; Barnea, Z.; Paterson, D.; Cookson, D.; Balaic, D. Phys. Rev. A 2001, 64, 062506.