Selective synthesis of nanosized TiO2 by hydrothermal route: Characterization, structure property relation, and photochemical application

Journal of Materials Research

Volumn 19, Issue 9, 2004, Pages 2567-2575

  Reddy, K Madhusudan ^a   Guin, Debanjan ^a   Manorama, Sunkara V ^a   Reddy, A Ramachandra ^b  

^a INDIAN INSTITUTE OF CHEMICAL TECHNOLOGY   (India)

^b NATIONAL INSTITUTE OF TECHNOLOGY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

CRYSTALLIZATION; DIFFERENTIAL THERMAL ANALYSIS; HYDROTHERMAL SYNTHESIS; MIXTURES; NANOSTRUCTURED MATERIALS; PARTICLE SIZE ANALYSIS; PHOTOCATALYSIS; PHOTOCHEMICAL REACTIONS; TRANSMISSION ELECTRON MICROSCOPY; ULTRAVIOLET RADIATION; ULTRAVIOLET SPECTROSCOPY; X RAY DIFFRACTION ANALYSIS;

ANATASE; BRUNAUER-EMMETT-TELLER ANALYSIS; RUTILE; SELECTED AREA DIFFRACTION;

TITANIUM DIOXIDE;

EID: 6044239553     PISSN: 08842914     EISSN: None     Source Type: Journal    
DOI: 10.1557/JMR.2004.0335     Document Type: Article

References (39)

1. 2 films. Nature 353, 737 (1991).
2. 2(110)-water ice interface. J. Phys. Chem. B 105, 3856 (2001).
3. Y.C. Yen, T.T. Tseug, and D.A. Chang: Electrical properties of porous titania ceramic humidity sensor. J. Am. Ceram. Soc. 72, 1472 (1989).
4. T. Matsumoto, Y. Murakami and Y. Takasu: Photochromism of titanium oxide gels prepared by the salt-catalytic sol-gel process. Chem. Lett. 49, 348 (2000).
5. R. Asahi, T. Morikawa, T. Ohwaki, K. Aoki, and Y. Taga: Visible light photocatalysis in nitrogen doped titanium oxides. Science 293, 269 (2001).
6. 2 photocatalyst. J. Mol. Catal. 60, 295 (1990).
7. J. Ovenstone and K. Yanagisawa: Hydrothermal synthesis and characterization of strontium doped lanthanum manganite perovskite powders for use as a cathode material in SOFCs. Chem. Mater. 11, 2770 (1999).
8. E.S. Thiele and R.H. French: Light scattering properties of representative, morphological rutile titania nanoparticles using a finite element method. J. Am. Ceram. Soc. 81[3], 469 (1998).
9. T.C. Patton: Pigment Handbook (Wiley, New York, 1973).
10. S.T. Aruna, S. Tirosh, and A.J. Zaban: Nanosize rutile particle synthesis via hydrothermal method without mineralizers. J. Mater. Chem. 10, 2388 (2000).
11. L.H. Edelson and A.M. Glaeser: Role of particle substructure in the sintering of monosized titania. J. Am. Ceram. Soc. 71[4], 225 (1988).
12. A. Chemseddine and T. Mritz: Nanostructuring titania: Control over nanocrystal structure, size, shape, and organization. Eur. J. Inorg. Chem. 2, 235 (1999).
13. 4 hydrolysis. Applied Catal., B: Gen. 26, 207 (2000).
14. H. Cheng, J. Ma, Z. Zhao, and L. Qi: Hydrothermal preparation of uniform nanosized rutile and anatase particles. Chem. Mater. 7, 663 (1995).
15. C.C. Wang and J.Y. Ying: Sol-gel synthesis and hydrothermal processing of anatase and rutile titania nanocrystals. Chem. Mater. 11, 3113 (1999).
16. 2. J. Mater. Chem. 11, 1694 (2001).
17. H. Kominami, J. Kato, S. Murakami, Y. Kera, M. Inoue, and B. Ohtani: Synthesis of titanium(IV) oxide of ultra-high photocatalytic activity: High-temperature hydrolysis of titanium alkoxides with water liberated homogeneously from solvent alcohols. J. Mol. Catal. A 144, 165 (1999).
18. F. Cavani, E. Foresti, F. Parrinello, and F. Triro: Role of the chemistry of solutions of titanium ions in determining the structure of V/Ti/O catalysts. Appl. Catal. 38, 311 (1998).
19. M. Henry, J.P. Jolivet, and J. Livage: In Aqueous Chemistry of Metal Cations, Hydrolysis, Condensation and Complexation, edited by R. Reisfeld and C.K. Jorgensen (Springer-Verlag, Berlin, Germany, 1992), p. 155.
20. L.I. Bekkerman, I.P. Dobrovolskii, and A. Ivakin: Effect of the composition of Ti(IV) solutions and precipitation conditions on the structure of the solid phase. Russ. J. Inorg. Chem. 21, 233 (1976).
21. J. Livage, M. Henry, and C. Sanchez: Sol-gel chemistry of transition metal oxides. Prog. Solid State Chem. 18, 259 (1988).
22. H.P. Klug and L.E. Alexander: In X-ray Diffraction Procedures (Wiley-Interscience, New York, 1974), p. 364.
23. R.A. Spurr and H. Myers: Quantity analysis of anatase-rutile mixture with an x-ray diffractomter. Anal. Chem. 29, 760 (1957).
24. 4. J. Phys. Chem. 103, 3308 (1999).
25. 2O by radiative cooling. Sol. Energy Mater. Sol. Cells 37, 93 (1995).
26. C. Granqvist and T. Eviksson: in Materials for Radiative Cooling to Low Temperatures, edited by C. Granqvist (Pergamon Press, Oxford, U.K., 1991), p. 168.
27. 2) membranes. J. Mater. Chem. 3, 923 (1993).
28. S. Ardizzone, C.L. Bianchi, and B. Vercelli: Structural and morphological features of MgO powders: The key role of the preparative starting compound. J. Mater. Res. 13, 2218 (1998).
29. 2-x nanoparticles. J. Appl. Phys. 87, 1318 (2000).
30. K. Madhusudan Reddy, S.V. Manorama, and A. Ramachandra Reddy: Bandgap studies on anatase titanium dioxide nanoparticles. Mater. Chem. Phys. 78, 239 (2002).
31. Y.W. Zhang, R. Si, C.S. Liao, C.H. Yan, C.X. Xian, and Y. Kou: Facile alcohothermal synthesis, size-dependent ultraviolet absorption and enhanced CO conversion activity of ceria nanocrystals. J. Phys. Chem. B 107, 10159 (2003).
32. Z. Yuhong, W. Ming, X. Gouxing, and Y. Weishen: Preparation and spectroscopic characterization of quantum size titanium dioixde. Chin. J. Internet 2, 17 (2000).
33. B. Ullrich, D.M. Bagnall, H. Sakai, and Y. Segawa: Photoluminescence properties of thin CdS films on glass formed by laser ablation. Solid State Commun. 109, 757 (1999).
34. 2 directly formed as nanometer-sized particles by hydrolysis under hydrothermal conditions. J. Solid State Chem. 170, 39 (2003).
35. J. Ovenstone: Preparation of novel titania photocatalysts with high activity. J. Mater. Sci. 36, 1325 (2001).
36. 2 and its photocatalytic performance. Int. J. Inorg. Mater. 3, 809 (2001).
37. H. Kominami, Y. Ishii, M. Kohno, S. Konishi, Y. Kera, and B. Ohtani: Nanocrystalline brookite-type titanium(IV) oxide photocatalysts prepared by a solvothermal method: Correlation between their physical properties and photocatalytic activities. Catal. Lett. 91, 41 (2003).
38. 2 system:kinetic modelling and reaction mechanism. J. Phys. Chem. B 107, 4296 (2003).
39. R. Chang: Chemistry, 5th ed. (McGraw-Hill, New York, 1994).