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6044248577
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-1. The sample started to lose weight above 780°C, with a total weight loss of 3.2%.
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30
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6044262391
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note
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Electron microscope: LEO 1530, with an additional EDS device (EDAX Pegasus 1200). No impurities, for example, stemming from the reaction container, were found.
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31
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6044232950
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note
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9 crystallizes in the tetragonal space group P4/n, with lattice dimensions of a = 874.83(3), c = 866.46(6) pm (Z = 2). Final residual factors are R1 = 0.0355, wR2 = 0.0899, GOF = 1.246 (all data, 1330 independent reflections, 35 parameters). Further details on the crystal-structure investigation may be obtained from the Fachinformationszentrum Karlsruhe, 76344 Eggenstein-Leopoldshafen, Germany (fax: (+49)7247-808-666; e-mail: crysdata@fiz-karlsruhe.de), on quoting the depository number CSD-413979.
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