Absolute configuration and crystal packing for three chiral drugs prone to spontaneous resolution: Guaifenesin, methocarbamol and mephenesin

Journal of Molecular Structure

Volumn 920, Issue 1-3, 2009, Pages 377-382

  Bredikhin, Alexander A ^a   Gubaidullin, Aidar T ^a   Bredikhina, Zemfira A ^a   Krivolapov, Dmitry B ^a   Pashagin, Alexander V ^a   Litvinov, Igor A ^a  

^a A E ARBUZOV INSTITUTE OF ORGANIC AND PHYSICAL CHEMISTRY   (Russian Federation)

Author keywords

Chiral drugs; Conglomerates; Crystal packing; Molecular structure; Spontaneous resolution

Indexed keywords

ENANTIOMERS; MOLECULAR STRUCTURE;

ABSOLUTE CONFIGURATIONS; CHIRAL DRUGS; CONGLOMERATES; CRYSTAL PACKING; ENANTIOPURE; GUAIFENESIN; PARAMETER METHODS; SPONTANEOUS RESOLUTION; X-RAY ANALYSIS;

CRYSTAL STRUCTURE;

EID: 59749087833     PISSN: 00222860     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.molstruc.2008.11.037     Document Type: Article

References (22)

1. Kinbara K., and Saigo K. Top. Stereochem. 23 (2003) 207
2. Fogassy E., Nogradi M., Kozma D., Egri G., Palovics E., and Kiss V. Org. Biomol. Chem. 4 (2006) 3011
3. Coquerel G. Enantiomer 3 (2000) 481
4. Custelcean R., and Ward M.D. Cryst. Growth Des. 5 (2005) 2277
5. Pasteur L. Ann. Chim. Phys. 24 (1848) 442
6. Perez-Garcia L., and Amabilino D.B. Chem. Soc. Rev. 36 (2007) 941
7. Jacques J., Collet A., and Wilen S.H. Enantiomers, Racemates and Resolutions (1994), Krieger Publishing Company, Malabar, Florida, USA
8. Bredikhin A.A., Bredikhina Z.A., Lazarev S.N., and Savel'ev D.V. Mendeleev Commun. 13 (2003) 104
9. Bredikhina Z.A., Novikova V.G., Zakharychev D.V., and Bredikhin A.A. Tetrahedron: Asymmetry 17 (2006) 3015
10. Bredikhin A.A., Bredikhina Z.A., Zakharychev D.V., and Pashagin A.V. Tetrahedron: Asymmetry 18 (2007) 1239
11. Bredikhin A.A., Bredikhina Z.A., Novikova V.G., Pashagin A.V., Zakharychev D.V., and Gubaidullin A.T. Chirality 20 (2008) 1092
12. In: O'Neil M.J. (Ed). The Merck Index. 14th ed. (2006), Merck and Co., Inc., Whitehouse Station, NJ, USA ((a) 4555, (b) 5980, (c) 5850)
13. G.M. Sheldrick, SADABS, Program for Empirical X-ray Absorption Correction, Bruker-Nonius, 2004.
14. G.M. Sheldrick, SHELXTL v.6.12, Structure Determination Software Suite, Bruker AXS, Madison, Wisconsin, USA, 2000.
15. Farrugia L.J. J. Appl. Crystallogr. 32 (1999) 837-838
16. Flack H.D. Acta Crystallogr. Sect. A 39 (1983) 876
17. Flack H.D., and Bernardinelli G. J. Appl. Crystallogr. 33 (2000) 1143
18. APEX2 (version 2.1), SAINTPlus. Data Reduction and Correction Program, (version 7.31A), Bruker Advansed X-ray Solutions, BrukerAXS Inc., Madison, Wisconsin, USA, 2006.
19. Spek A.L. Acta Crystallogr. Sect. A 46 (1990) 3440
20. Wang Y., Li M., Liu L., Zhou L., and Wang J. Acta Crystallogr. Sect. E: Struct. Rep. Online 61 (2005) 1999
21. Kaduk J.A. Powder Diffr. 19 (2004) 127
22. Luo X., Pietrobon R., Curtis L.H., and Hey L.A. Spine 29 (2004) E531