Determination of sulphur in uranium matrix by total reflection X-ray fluorescence spectrometry

Spectrochimica Acta - Part B Atomic Spectroscopy

Volumn 63, Issue 12, 2008, Pages 1395-1398

  Dhara, Sangita ^a   Misra, N L ^a   Aggarwal, S K ^a  

^a BHABHA ATOMIC RESEARCH CENTRE   (India)

Author keywords

Solvent extraction; Sulphur; Total reflection X ray fluorescence spectrometry; Trace element; Uranium

Indexed keywords

ELECTROMAGNETIC WAVE REFLECTION; FLUORESCENCE; FLUORESCENCE SPECTROSCOPY; SODIUM SULFATE; SOLVENT EXTRACTION; SPECTROMETRY; SULFUR; TRACE ELEMENTS; TRICHLOROETHYLENE; URANIUM; URANIUM COMPOUNDS; X RAYS;

CALIBRATION SOLUTIONS; CONCENTRATION LEVELS; EXCITATION SOURCES; TOTAL REFLECTION X-RAY FLUORESCENCE SPECTROMETRIES; TRACE DETERMINATION; TRACE-LEVEL DETERMINATION; TRI-N-BUTYL PHOSPHATE; URANYL NITRATE SOLUTION;

CHEMICALS REMOVAL (WATER TREATMENT);

EID: 59349109191     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.sab.2008.10.033     Document Type: Article

References (13)

1. Sayi Y.S., Shankaran P.S., Yadav C.S., Chhapru G.C., Ramakumar K.L., and Venugopal V. Determination of total sulphur by vacuum combustion extraction-quadruple mass spectrometry (VCE-QMS). Proc. Natl. Acad. Sci. India 72 (A) (2002) 241-248
2. 2 fuel pellets for heavy water reactors, BARC Newsletter, Founder's day special issue October-2001 (http://www.barc.ernet.in/publications/nl/).
3. Singh Mudher K.D., Krishnan K., Khandekar R.R., Yadav M.B., Jayadevan N.C., and Sood D.D. Rubidium uranium trisulphate: a new chemical assay standard for uranium. J. Radioanal. Nucl. Chem. 240 (1999) 183-191
4. Vallet V., and Grenthe I. On the structure and relative stability of uranyl (VI) sulphate complexes in solution. C.R. Chimie 10 (2007) 905-915
5. 4. J. Solid State Chem. 45 (1982) 235-240
6. Sayi Y.S., Shankaran P.S., Yadav C.S., and Chhapru G.C. Determination of total sulphur in inorganic compounds-an overview. Indian J. Chem. Technol. 10 (2003) 373-381
7. Klockenkämper R. Total reflection X-ray fluorescence analysis. Chemical Analysis vol. 140 (1996), John Wiley & Sons, New York
8. Haarich M., Knöchel A., and Salow H. Einsatz der totalreflexions-röntgenfluoreszenzanalyse in der analytik von nuklearen wiederaufarbeitungsanlagen. Spectrochim. Acta Part B 44 (1989) 543-549
9. Klockenkämper R., and von Bohlen A. Total-reflection X-ray fluorescence moving towards nanoanalysis: a survey. Spectrochim. Acta Part B 56 (2001) 2005-2018
10. Misra N.L., Singh Mudher K.D., Adya V.C., Rajeswari B., and Venugopal V. Determination of trace elements in uranium oxide by Total reflection X-ray fluorescence spectrometry. Spectrochim. Acta Part B 60 (2005) 834-840
11. Misra N.L., Dhara S., and Singh Mudher K.D. Uranium determination in seawater by total reflection X-ray fluorescence. Spectrochim. Acta Part B 61 (2006) 1166-1169
12. Alsecz A., Osán J., Kurunczi S., Alföldy B., Várhegyi A., and Török S. Analytical performance of different X-ray spectroscopic techniques for the environmental monitoring of the recultivated uranium mine site. Spectrochim. Acta Part B 62 (2007) 769-776
13. Dhara S., Misra N.L., Mudher K.D.S., and Aggarwal S.K. Bulk determination of uranium and thorium in presence of each other by total reflection X-ray fluorescence spectrometry. Spectrochim. Acta Part B 62 (2007) 82-85