Determination of fluoroquinolones in aquaculture products by ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)

Food Additives and Contaminants - Part A Chemistry, Analysis, Control, Exposure and Risk Assessment

Volumn 26, Issue 1, 2009, Pages 39-46

  Pearce, J N ^a   Burns, B G ^a   van de Riet, J M ^a   Casey, M D ^a   Potter, R A ^a  

^a CANADIAN FOOD INSPECTION AGENCY   (Canada)

Author keywords

Aquacultured products; Ciprofloxacin; Danofloxacin, enrofloxacin; Fluoroquinolones; Multiresidue method; Sarafloxacin; Ultra performance liquid chromatography tandem mass spectrometry (UPLC MS MS)

Indexed keywords

ANTIINFECTIVE AGENT; DRUG RESIDUE; QUINOLONE DERIVATIVE; ACETONITRILE; AMMONIUM HYDROXIDE; CIPROFLOXACIN; DANOFLOXACIN; DICHLOROMETHANE; ENROFLOXACIN; FORMIC ACID; HEXANE; NORDIFLOXACIN; QUINOLINE DERIVED ANTIINFECTIVE AGENT; WATER;

ANALYSIS; ANIMAL; AQUACULTURE; CHEMISTRY; FOOD ANALYSIS; FOOD CONTAMINATION; LIQUID CHROMATOGRAPHY; METABOLISM; PENAEIDAE; PROCEDURES; SALMON; SEA FOOD; TANDEM MASS SPECTROMETRY; TILAPIA; ANALYTICAL ERROR; ANIMAL TISSUE; ARTICLE; CENTRIFUGATION; CONTROLLED STUDY; DIET SUPPLEMENTATION; DILUTION; NONHUMAN; PRIORITY JOURNAL; RELIABILITY; REVERSED PHASE LIQUID CHROMATOGRAPHY; SAMPLING; SHRIMP; SOLID PHASE EXTRACTION;

ANIMALS; ANTI-BACTERIAL AGENTS; AQUACULTURE; CHROMATOGRAPHY, LIQUID; DRUG RESIDUES; FLUOROQUINOLONES; FOOD ANALYSIS; FOOD CONTAMINATION; PENAEIDAE; SALMON; SEAFOOD; TANDEM MASS SPECTROMETRY; TILAPIA;

DECAPODA (CRUSTACEA); MESOPENAEUS TROPICALIS; TILAPIA;

EID: 58949091553     PISSN: 19440049     EISSN: 19440057     Source Type: Journal    
DOI: 10.1080/02652030802189757     Document Type: Article

References (20)

1. AOAC. 2000. “ AOAC official methods of analysis ”. In. Method 937-07 Fish and marine products–treatment and sample preparation procedure, 17th Edn, Gaithersburg, MD:AOAC International. sect. 35.1.01
2. Bethem, R, Boison, JO, Gale, J, Heller, D, Lehotay, S, Loo, J, Musser, S, Price, P, and Stein, S. 2003. Establishing the fitness for purpose of mass spectrometric methods. J Am Soc Mass Spectrom, 14:528–541.
3. Canadian Food Inspection Agency. 2005. “ Fish products standards and methods manual ”. In Approved theraputants for aquaculture use, Ottawa, ON(Canada):Canadian Food Inspection Agency. Appendix No. 1 2005
4. Dufresne, G, and Fouquet, A. 2007. Multiresidue determination of quinolone and fluoroquinolone antibiotics in fish and shrimp by liquid chromatography/tandem mass spectrometry. J AOAC Int, 90:604–612.
5. EURACHEM guide. The fitness for purpose of analytical methods:a laboratory guide to method validation and related topics. Eurachem Working Group Report, December 1998, EURACHEM. 1998
6. European Communities Commission Decision (ECCD). 2002. Implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Off J Eur Comm, L221:8–36.
7. Kowalczuk, D, Hopkala, H, and Gumieniczek, A. 2003. Application of solid-phase extraction of fluoroquinolone derivatives from a biological matrix to their biodetermination by liquid chromatography. J Liq Chromatog Relat Tech, 26:1731–1741.
8. McNabb, P, Selwood, AI, and Holland, PT. 2005. Multiresidue method for determination of algal toxins in shellfish:single-laboratory validation and interlaboratory study. J AOAC Int, 88:761–772.
9. Pecorelli, I, Galarini, R, Bibi, R, Floridi, AL, Casciarri, E, and Floridi, A. 2003. Simultaneous determination of 13 quinolones from feeds using accelerated solvent extraction and liquid chromatography. Anal Chimica Acta, 483:81–89.
10. Roybal, JE, Pfenning, AP, Turnipseed, SB, Walker, CC, and Hurlbut, JA. 1997. Determination of four fluoroquinolones in milk by liquid chromatography. J AOAC Int, 80:982–987.
11. Roybal, JE, Walker, CC, Pfenning, AP, Turnipseed, SB, Storey, JM, Gonzales, SA, and Hurlbut, JA. 2003. Concurrent determination of four fluoroquinolones in catfish, shrimp and salmon by LC with fluorescence detection. J AOAC Int, 85:1293–1301.
12. Samanidou, VF, Demetriou, CE, and Papadoyannis, IN. 2003. Direct determination of four fluoroquinolones; enozacin, norfloxacin, ofloxacin and ciprofloxacin, in pharmaceuticals and blood serum by HPLC. Anal Bioannal Chem, 375:623–629.
13. Schneider, MJ, Darwish, AM, and Freeman, DW. 2007. Simultaneous multiresidue determination of tetracyclines and fluoroquinolones in catfish muscle using high performance liquid chromatography with fluorescence detection. Anal Chemica Acta., 586:269–274.
14. Schneider, MJ, and Donoghue, DJ. 2003. Multiresidue determination of fluoroquinolone antibiotics in eggs using liquid chromatography-fluorescence-mass spectrometry. Anal Chimica Acta, 483:39–49.
15. Steffenak, I, Hormazabal, V, and Yndestad, M. 1991. A rapid assay for the determination of sarafloxacin (A-55620) in fish by high performance liquid chromatography. J Liq Chrom, 14:1983–1989.
16. Tittlemier, SA, Van de Riet, JM, Burns, G, Potter, R, Murphy, C, Rourke, W, Pearce, H, and Dufresne, G. 2007. Analysis of veterinary drug residues in fish and shrimp composites collected during the Canadian Total Diet Study, 1993–2004. Food Add. Contam, 24:14–20.
17. Toussaint, B, Bordin, G, Janosi, A, and Rodriguez, AR. 2002. Validation of a liquid chromatography-tandem mass spectrometry method for the simultaneous quantification of 11 fluoroquinolone antibiotics in swine kidney. J Chromatog A, 976:195–206.
18. Turnipseed, SB, Roybal, JE, and Pfenning, AP. 2006. Confirmation of fluoroquinolone residues in salmon and shrimp tissue by LC/MS:evaluation of single quadrapole and ion trap instruments. USFDA Lab Informat Bull, 4298:1–20.
19. US Food and Drug Administration. 2005. Guidance for industry:mass spectrometry for confirmation of the identity of animal drug residues, Washington, DC:US Food and Drug Administration. [cited 2005 Jan 20]. Available from:http://www.fda.gov/cvm/guidance/guide118.doc/
20. van de Riet, JM, Murphy, CJ, Pearce, JN, Potter, RA, and Burns, BG. 2005. Determination of malachite green and leucomalachite green in a variety of aquacultured products by liquid chromatography with tandem mass spectrometry detection. J AOAC Int, 88:744–749.