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58749092887
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note
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2 = 0.1356, for 2874 unique reflections and 232 parameters, S = 1.090. Structural data for 1 and 2 were collected on a Bruker Smart Apex CCD with graphitemonochromated Mo Ka radiation. Their structures were solved by direct methods and refined with the fullmatrix least-squares technique using the SHELXS-97 and SHELXL-97 programs [24]. CCDC: 1, 705021.
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25
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58749102806
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note
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2 = 0.1364, for 2839 unique reflections and 208 parameters, S = 1.138. The lattice water molecules occupy the 1D channel and are disorder between two positions, in a ratio of 0.6-0.4, their positions and composition could not be accurately determined because of their high structural disorder, but were confirmed by EA and TG. CCDC: 2, 705022.
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