메뉴 건너뛰기




Volumn 27, Issue 1, 2009, Pages 13-15

Synthesis and absolute configuration of the diynediol from Psathyrella scobinacea

Author keywords

Absolute configuration; Diol; Diyne; Natural product

Indexed keywords


EID: 58649090253     PISSN: 1001604X     EISSN: None     Source Type: Journal    
DOI: 10.1002/cjoc.200990005     Document Type: Article
Times cited : (4)

References (11)
  • 11
    • 58649102131 scopus 로고    scopus 로고
    • Data for 16 (colorless oil, α]D28 +22.6 (c 0.25, EtOH, 1H NMR (CDCl3, 300 MHz) δ: 4.15 (d, J=6.5 Hz, 1H, 3.85 (dq, J=6.5, 6.3 Hz, 1H, 2.64 (br s, 1H, 2.53 (br s, 1H, 2.22 (s, 1H, 1.29 (d, J=6.3 Hz, 3H, 13C NMR (CDCl3, 100 MHz) δ: 74.5, 70.8, 70.5, 68.8, 67.6, 67.1, 18.4; FT-IR (film) ν: 3381, 3291, 2978, 2918, 2228, 2064, 1455, 1398, 1261, 1125, 1031, 918 cm-1; EI-MS m/z, 124 (0.68, 86 (33, 49 (57, 45 (100, EI-HRMS calcd for C7H8O 2 (M, 124.0524, found 124.0523. Data for 17 (white solid, m.p. 64-65°C, α]D28 +28.2 (c 0.7, EtOH, 1H NMR (CDCl3, 400 MHz) δ: 4.35 (d, J=3.5 Hz, 1H, 3.93 (dq, J=3.5, 6.4 Hz, 1H, 3.21 (br s, 1H, 2.55 (br s, 1H, 2.20 (s, 1H, 1.28 d, J=6.4 Hz, 3H, 13C
    • +) 124.0524, found 124.0525.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.