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57849112662
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note
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-1 for the azide group. Caution! Azide complexes are potentially explosive. Only a small amount of the materials should be prepared and handled with care.
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37
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57849166164
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note
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2 = 0.0870 [I > 2σ(I)]. Suitable single crystals of compound 1 was mounted on a Brucker SMART APEX CCD diffractometer equipped with a graphite-monochromated Mo Kα radiation source (λ = 0.71073 Å) at 298 K. All absorption corrections were performed with SADABS program. All the structures were solved by direct methods and refined with full-matrix least-squares and expanded using Fourier techniques. The non-hydrogen atoms were refined anisotropically. Hydrogen atoms were placed in the calculate positions. All calculations were performed using SHELXTL-97 program.
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