Synthesis of MCM-22 zeolites of different Si/Al ratio and their structural, morphological and textural characterisation

Microporous and Mesoporous Materials

Volumn 118, Issue 1-3, 2009, Pages 1-10

  Delitala, C ^a   Alba, M D ^b   Becerro, A I ^b   Delpiano, D ^c   Meloni, D ^c   Musu, E ^c   Ferino, I ^c  

^a Saras Ricerche e Tecnologie SpA   (Italy)

^b INSTITUTO DE CIENCIA DE MATERIALES DE SEVILLA   (Spain)

^c UNIVERSITY OF CAGLIARI   (Italy)

Author keywords

MCM 22; NMR; Structure; Texture; XRD

Indexed keywords

ADSORPTION; ALUMINUM; CRYSTAL STRUCTURE; DIFFRACTION; MAGNETIC RESONANCE; MICROPOROSITY; NUCLEAR MAGNETIC RESONANCE; PHYSISORPTION; SCANNING; SCANNING ELECTRON MICROSCOPY; SILICATE MINERALS; TEXTURES; X RAY ANALYSIS; X RAY DIFFRACTION; X RAY DIFFRACTION ANALYSIS; ZEOLITES;

AL-IONS; CHARACTERISATION; CRYSTALLISED SAMPLES; CRYSTALLOGRAPHIC SITES; DEGREE OF CRYSTALLINITY; DIFFRACTION DATUMS; FERRIERITE; IN DEPENDENCES; MAGIC ANGLE SPINNING NUCLEAR MAGNETIC RESONANCES; MAS-NMR; MCM-22; MICROPOROUS; NMR; POROUS STRUCTURES; SI/AL RATIOS; SINUSOIDAL CHANNELS; STRUCTURE; SUPERCAGES; SYNTHESIS OF; ULTRAMICROPORE VOLUMES; X-RAY DIFFRACTIONS; XRD; ZEOLITE FRAMEWORKS;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 57749200741     PISSN: 13871811     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.micromeso.2008.07.047     Document Type: Article

References (40)

1. M.K. Rubin, P. Chu, Mobil Oil Corporation, US Patent 4,954,325, 1990.
2. Leonowicz M.E., Lawton J.A., Lawton S.L., and Rubin M.K. Science 264 (1994) 1910
3. Ravishankar R., Bhattarcharya D., Jacob N.E., and Sivasanker S. Micropor. Mesopor. Mater. 4 (1995) 83
4. Corma A. Micropor. Mesopor. Mater. 21 (1998) 487
5. Wu P., Komatsu T., and Yashima T. Micropor. Mesopor. Mater. 22 (1998) 343
6. Corma A., Corell C., Pérez-Pariente J., Guil J.M., Guil-López R., Nicolopoulos S., Gonzalez-Calbet J., and Vallet-Regi M. Zeolites 16 (1996) 7
7. Wendelbo R., Roque-Malherbe R., and Corma A. Micropor. Mater. 10 (1997) 231
8. Frache A., Cadoni M., Bisio C., and Marchese L. Langmuir 18 (2002) 6875
9. O. Ducreux, E. Jolimaitre, Institut Francais du Petrole, US Patent 935,658, 2004.
10. Rungsirisakun R., Nanok T., Probst M., and Limtrakul J. J. Mol. Struct. 756 (2005) 39
11. J. Denayer, R. Ocakoglu, G. Baron, Vrije Universiteit Brussel, International Patent WO/2005/016857, 2005.
12. Denayer J.F.M., Ocakoglu R.A., Thybaut J., Marin G., Jacobs P., Martens J., and Baron G.V. J. Phys. Chem. B 110 (2006) 8551
13. Wang S., Li H., and Xu L. J. Colloid Interface Sci. 295 (2006) 71
14. Delitala C., Cadoni E., Delpiano D., Meloni D., Melis S., and Ferino I. Micropor. Mesopor. Mater. 110 (2008) 197
15. Corma A., Corell C., and Pérez-Pariente J. Zeolites 15 (1995) 2
16. Unverricht S., Hunger M., Ernst S., Karge H.G., and Weitkamp J. Stud. Surf. Sci. Catal. 84 (1994) 37
17. Ravishankar R., Sen T., Ramaswamy V., Soni H.S., Ganapathy S., and Sivasanker S. Stud. Surf. Sci. Catal. 84 (1994) 331
18. Guray I., Warzywoda J., Bac N., and Sacco A. Micropor. Mesopor. Mater. 31 (1999) 241
19. Cheng M., Tan D., Liu X., Han X., Bao X., and Lin L. Micropor. Mesopor. Mater. 42 (2001) 307
20. Vuono D., Pasqua L., Testa F., Aiello R., Fonseca A., Koranyi T.I., and Nagy J.B. Micropor. Mesopor. Mater. 97 (2006) 78
21. D. Meloni, Ph.D. Thesis, Université de Poitiers, 2000.
22. Mochida I., Educhi S., Hironaka M., Nagao S., Sakanishi K., and Whitehurst D.D. Zeolites 18 (1997) 142
23. Grunnberg B., Emmler T., Gedat E., Shenderovich J., Findenegg G.H., Limbach H.H., and Buntkowsky G. Chem. A Eur. J. 10 (2004) 5689
24. Xie X., Stazawa M., Kunimori K., and Hayashi S. Micropor. Mesopor. Mater. 39 (2000) 25
25. Engelhardt G., and Michel D. High Resolution Solid State NMR of Silicates and Zeolites (1987), Wiley, New York
26. Pfeifer H. J. Chem. Soc. Faraday Trans. 1 84 (1988) 3777-3783
27. Hunger M., Ernst S., and Weitkamp J. Zeolites 15 (1995) 188-192
28. Heeribout L., Dorémieux-Morin C., Nogier J.P., Vincent R., and Fraissard J. Micropor. Mesopor. Mater. 24 (1998) 101
29. Mastikhin V., Noscov A.V., Treskikh V.V., Zamaraev K.I., and Wachs I.E. J. Phys. Chem. 98 (1994) 13621
30. Semmer-Herlédan V., Heeribout L., Batamack P., Dorémieux-Morin C., Fraissard J., Gola A., and Benazzi E. Micropor. Mesopor. Mater. 34 (2000) 157
31. Hannus I., Konya Z., Nagy J.B., Lentz P., and Kiricsi I. Appl. Catal. B: Environ. 17 (1998) 157
32. Chen T.H., Wanters B.H., and Grobet P.J. Eur. J. Inorg. Chem. 2 (2000) 281
33. Kolodziejski W., Zicovich-Wilson C., Corell C., Pérez-Pariente J., and Corma A. J. Phys. Chem. 99 (1995) 7002
34. Lawton S.L., Fung A.S., Kennedy G.J., Alemany L.B., Chang C.D., Hatzikos G.H., Lissy D.N., Rubin M.K., Timken H.K.C., Steuernagel S., and Woessner D.E. J. Phys. Chem. 100 (1996) 3788
35. Kennedy G.J., Lawton S.L., Fung A.S., Rubin M.K., and Steuernagel S. Catal. Today 49 (1999) 385
36. Wang Y., Zhou D., Yang G., Liu X., Ma D., Liang D.B., and Bao X. Chem. Phys. Lett. 388 (2004) 363
37. Camblor M.A., Corell C., Corma A., Díaz-Cabañas M.J., Nicolopoulos S., González-Calbet J.M., and Vallet-Regi M. Chem. Mater. 8 (1996) 2415
38. Engelhardt G., and Radeglia R. Chem. Phys. Lett. 108 (1984) 271
39. Rouquerol F., Rouquerol J., and Sing K. Adsorption by Powders and Porous Solids. Principles Methodology and Applications (1999), Academic Press, London (and literature therein)
40. Breck D.W. Zeolite Molecular Sieves (1974), John Wiley, New York p. 636