1,2-Hydroboration of alkyn-1-yldichlorosilanes using triethylborane

Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences

Volumn 63, Issue 11, 2008, Pages 1267-1275

  Wrackmeyer, Bernd ^a   Khan, Ezzat ^a   Milius, Wolfgang ^a  

^a UNIVERSITY OF BAYREUTH   (Germany)

Author keywords

9 BBN; Alkenes; Alkynes; Hydroboration; NMR; Silanes; Triethylborane

Indexed keywords

HYDROCARBONS; NUCLEAR MAGNETIC RESONANCE; OLEFINS; REAGENTS; SILANES; SINGLE CRYSTALS;

29SI NMR; 9-BBN; ALKYNES; ETHYL GROUPS; HYDROBORATION; HYDROGEN TRANSFER; SINGLE CRYSTAL X-RAY DIFFRACTION; TRIETHYLBORANE;

CRYSTAL STRUCTURE;

EID: 57749093136     PISSN: 09320776     EISSN: None     Source Type: Journal    
DOI: 10.1515/znb-2008-1105     Document Type: Article

References (37)

1. A. Stock, F. Zeidler, Ber. Deutsch. Chem. Ges. 1921, 54B, 531.
2. a) L. Rosenblum, J. Am. Chem. Soc. 1955, 77, 5016;
3. b) R. Köster, Liebigs Ann. Chem. 1958, 618, 31;
4. c) E. C. Ashby, J. Am. Chem. Soc. 1959, 81, 4791;
5. d) P. F. Winternitz, A. A. Carotti, J. Am. Chem. Soc. 1960, 82, 2430.
6. R. Köster, G. Benedikt, W. Larbig, K. Reinert, G. Rotermund, Angew. Chem. 1963, 75, 1079.
7. R. Köster, W. Larbig, G. W. Rotermund, Liebigs Ann. Chem. 1965, 682, 21.
8. R. Köster, in Houben-Weyl, Methoden der Organischen Chemie (Ed.: R. Köster), Vol. 13/3c, Thieme, Stuttgart, 1984, p. 217.
9. E. Abuin, J. Grotewold, E. A. Lissi, M. C. Vara, J. Chem. Soc. B, 1968, 1044.
10. B. Wrackmeyer, Coord. Chem. Rev. 1995, 145, 125.
11. a) B. Wrackmeyer, J. Chem. Soc., Chem. Commun. 1988, 1624;
12. b) R. Köster, G. Seidel, B. Wrackmeyer, Chem. Ber. 1989, 122, 1825.
13. a) R. Köster, G. Seidel, J. Süß, B. Wrackmeyer, Chem. Ber. 1993, 126, 1107;
14. b) R. Köster, G. Seidel, I. Klopp, C. Krüger, G. Kehr, J. Süß, B. Wrackmeyer, Chem. Ber. 1993, 126, 1385.
15. a) B. Wrackmeyer, J. Süß, Main Group. Met. Chem. 1996, 19, 39;
16. b) B. Wrackmeyer, H. E. Maisel, W. Milius, Chem. Ber. / Recueil 1997, 130, 1349;
17. c) B. Wrackmeyer, J. Süß, Z. Naturforsch. 2002, 57b, 741.
18. B. Wrackmeyer, K. Shahid, S. Ali, Appl. Organomet. Chem. 2005, 19, 377.
19. B. Wrackmeyer, K. Shahid, S. Ali, Z. Naturforsch. 2005, 60b, 590.
20. B. Wrackmeyer, E. Khan, S. Bayer, K. Shahid, Z. Naturforsch. 2007, 62b, 1174.
21. a) W. E. Davidsohn, M. C. Henry, Chem. Rev. 1967, 67, 73;
22. nd ed.) Elsevier, Amsterdam, 1988;
23. c) L. Brandsma, Synthesis of Acetylenes, Allenes, Cumulenes-Methods and Techniques, Elsevier, Amsterdam, 2004.
24. B. Wrackmeyer, Progr. NMR Spectrosc. 1979, 12, 227.
25. B. Wrackmeyer, E. Khan, R. Kempe Z. Naturforsch. 2007, 62b, 75.
26. P. H. M. Budzelaar, G. Talarico, Structure and Bonding 2003, 105, 141.
27. E. Iglesia, D. G. Barton, S. L. Soled, S. Miseo, J. E. Baumgartner, W. E. Gates, G. A. Fuentes, G. D. Meitzner, Studies in Surface Science and Catalysis 1996, 101, 533.
28. B. Wrackmeyer, W. Milius, M. H. Bhatti, S. Ali, J. Organomet. Chem. 2003, 669, 72.
29. a) G. A. Morris, R. Freeman, J. Am. Chem. Soc. 1979, 101, 760;
30. b) G. A. Morris, J. Am. Chem. Soc. 1980, 102, 428;
31. c) G. A. Morris, J. Magn. Reson. 1980, 41, 185;
32. d) D. P. Burum, R. R. Ernst, J. Magn. Reson. 1980, 39, 163.
33. B. Wrackmeyer, O. L. Tok, Yu. N. Bubnov, Angew. Chem. 1999, 111, 214;
34. Angew. Chem. Int. Ed. 1999, 38, 124;
35. b) B. Wrackmeyer, O. L. Tok, Magn. Reson. Chem. 2002, 40, 406;
36. c) B. Wrackmeyer, W. Milius, O. L. Tok, Chem. Eur. J. 2003, 9, 4732.
37. G. M. Sheldrick, Acta Crystallogr. Sect. A 2008, A64, 112.