Reconciling thermal and structural data from the polymorphic transitions of malonamide

Thermochimica Acta

Volumn 482, Issue 1-2, 2009, Pages 57-61

  Cheung, Eugene Y ^a   Peterson, Matthew L ^a  

^a TransForm Pharmaceuticals   (United States)

Author keywords

Differential scanning calorimetry; Infrared spectroscopy; Phase transitions; Polymorphism; X ray diffraction

Indexed keywords

CALORIMETERS; CALORIMETRY; CHEMICAL STABILITY; CRYSTAL STRUCTURE; CRYSTALLIZATION; DIFFERENTIAL SCANNING CALORIMETRY; DIFFRACTION; GRINDING (COMMINUTION); GRINDING (MACHINING); LASER INTERFEROMETRY; NANOCRYSTALLINE ALLOYS; PHASE TRANSITIONS; POLYMORPHISM; SCANNING; SINGLE CRYSTALS; SPECTROSCOPIC ANALYSIS; SPECTRUM ANALYSIS; THERMOANALYSIS; X RAY ANALYSIS; X RAY DIFFRACTION; X RAY DIFFRACTION ANALYSIS;

CRYSTAL FORMS; MELT CRYSTALLIZATIONS; MONOCLINIC FORMS; ORTHORHOMBIC POLYMORPHS; POLYMORPHIC TRANSITIONS; RECRYSTALLIZATION; SOLID STATES; SOLUTION CRYSTALLIZATIONS; STRUCTURAL DATUMS; TETRAGONAL POLYMORPHS; THERMAL ANALYSIS; X-RAY STRUCTURES;

INFRARED SPECTROSCOPY;

EID: 57649245299     PISSN: 00406031     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.tca.2008.10.019     Document Type: Article

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15. wp = 0.0318 [46 variables, 3324 profile points].
16. wp = 5.81%.
17. wp = 0.0461 [16 variables, 3324 profile points].
18. wp = 0.0366 [16 variables, 3324 profile points].