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33749986681
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For a meso-hydroxyporphyrin, see: Esdaile, L. J.; Senge, M. O.; Arnold, D. P. Chem. Commun. 2006, 4192.
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For a meso-hydroxyporphyrin, see: Esdaile, L. J.; Senge, M. O.; Arnold, D. P. Chem. Commun. 2006, 4192.
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3
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0015935467
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(a) Stolzenberg, A. M.; Spreer, L. O.; Holm, R. H. J. Am. Chem. Soc. 1980, 102, 364.
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57149092495
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(c) Song, J.; Jang, S. Y.; Yamaguchi, S.; Sanker, J.; Hiroto, S.; Aratani, N.; Shin, J.-Y.; Easwaramoorthi, S.; Kim, K. S.; Kim, D.; Shinokubo, H.; Osuka, A. Angew. Chem., Int. Ed. 2008, 47, 6007.
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0000948772
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For related dimerization of oxophlorins, see: a
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14
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57149104481
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The crystaltographic data of 3a: C127H 147N8O4Cl9, M, 2168.58, triclinic, space group P1 (No. 2, a, 14.333(2, b, 16.550(3, c, 27.977(5) Å, α, 93.212(3, β, 103.856(3, γ, 110.975(3)°, V, 5942.3(17) Å3, Z, 2, T, 90(2) K, ρcalcd, 1.212 g/cm, R1, 0.0937 (I > 2σ(I, wR2, 0.3056 (all data, GOF, 1.047. 3b: C 127H143N9O4Ni2Cl 4, M, 2110.96, triclinic, space group P1 (No. 2, a, 13.188(5, b, 14.388(5, c, 16.656(7) Å, α, 66.993(12, β, 86.554(14, γ, 78.472(12)°, V, 2849.9(19) Å3 Z, 1, T, 123 K, ρcalcd, 1.230 g/cm, R1, 0.0860 7 > 2
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2 = 0.2661 (all data), GOF = 1.029.
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