A simple and selective spectrophotometric method for the determination of trace gold in real, environmetal, biological, geological and soil samples using bis (Salicylaldehyde) orthophenylenediamine

Analytical Chemistry Insights

Volumn 2008, Issue 3, 2008, Pages 75-90

  Soomoro, Rubina ^a   Ahmed, M Jamaluddin ^b   Memon, Najma ^a   Khan, Humaira ^a  

^a UNIVERSITY OF SINDH   (Pakistan)

^b UNIVERSITY OF CHITTAGONG   (Bangladesh)

Author keywords

Aqueous and micellar media; Biological and soil samples; BSOPD; Environmental; Gold determination; Spectrophotometry

Indexed keywords

EID: 57049139547     PISSN: None     EISSN: 11773901     Source Type: Journal    
DOI: None     Document Type: Article

References (39)

1. Ahmed, M.J. and Mamun, M.A. 2001. Spectrophotometric determination of lead in industrial, environmental, biological and soil samples using 2,5-dimercapto-1,3,4-thiadiazole. Talanta, 55:43-54.
2. Ahmed, M.J. and Nasir Uddin, M. 2007. A simple spectrophotometric method for the determination of cobalt in industrial, environmental, biological and soil samples using Bis (Salicylaldehyde) orthophenyl-enediamine. Chemosphere, 67:2020-7.
3. Alfonso, G.G. and Gomez Ariza, J.L. 1981. Derivatives of rhodanine as spectrophotometric analytical reagents I. Condensation at C-5 with aromatic pyridine and nonpyridine aldehydes. Microchem. J., 26:574-85.
4. Balcerzak, M., Kosiorek, A. and Swiecicka, E. 2006. Morin as a spectrophotometric reagent for gold. J. Anal. Chem., 61:119-23.
5. Chen, Z., Huang, Z., Chen, J., Chen, J., Yin, J., Su, Q. and Yang, G. 2006. Spectrophotometric determination of gold in water and ore with 2-Carboxyl-1-Naphthalthiorhodanine. Anal. Lett., 39:579-87.
6. El-Zawawy, F.M., El-Shahat, M.F. and Mohamed, A.A. 1995. Spectrophotometric determination of silver and gold with 5-(2,4-dihydroxyben zylidene)rhodanine and cationic surfactants. Analyst., 120:549-54.
7. Fujita, Y., Mori, I. and Matsuo, T. 1999. Spectrophotometric determination of gold(III) by an association complex formation between gold-thiamine and phloxine. Anal. Sci., 15:1009-12.
8. Gangadharappa, M., Reddy, P.R., Reddy, V.R. and Reddy, S. 2004. Direct spectrophotometric determination of gold(III) using 2′-aminoacetophenone isonicotinoyl hydrazone (2-AAINH). J. Indian Chem. Soc., 81:525-7.
9. Gao, X.Y., Hu, Q.F., Yang, G.Y. and Jia-yuan, Y. 2005. Study on solid phase extraction and spectrophotometric determination of gold with p-sulfobenzylidene-thiorhodanine. Fenxi. Shiyanshi., 24:67-70.
10. Ghazy, S.E., El-shazly, R.M., El-Shasri, M.S., Al-Hazmi, GAA. and El-Asmy, A.A. 2006. Spectrophotometric determination of cooper(II) in natural waters, vitamins and certified steel scrap samples using acetophenone-chlorophenylthiosemicarbazone. J. Iranian Chemical Society, 3(2):140-50.
11. Gowda, H.S., Gowda, A.T. and Made Gowda, N.M. 1984. Spectrophotometric determination of microamounts of gold(III) with propericiazine. Microchem. J., 30:259-65.
12. Hu, Q., Chen, X., Yang, X., Huang, Z., Chen, J. and Yang, G. 2006. Solid phase extraction and spectrophotometric determination of Au (III) with 5-(2-Hydroxy-5-nitrophenylazo)- thiorhodanine. Anal. Sci., 22:627-30.
13. Jackson, M.L. 1965. Soil Chemical Analysis, Prentice Hall, Englewood Cliffs, NJ. 272.
14. Juvonen, R., Lakomaa, T. and Soikkeli, L. 2002. Determination of gold and the platinum group elements in geological samples by ICP-MS after nickel sulphide fire assay: difficulties encountered with different types of geological samples. Talanta, 58:595-603.
15. Kavanoz, M., Gulce, H. and Yildiz, A. 2004. Anodic Stripping voltammetric determination of gold on a polyvinylferrocene coated glassy carbon electrode. Turk J. Chem., 28:287-97.
16. Khan, H., Ahmed, M.J. and Bhanger, M.I. 2007. A rapid spectrophotometric method for the determination of trace level lead using 1,5-Diphenylthiocarbazone in the presence of aqueous micellar solution. Anal. Sci., 23(2):193-9.
17. Koh, T., Okazaki, T. and Ichikawa, M. 1986. Spectrophotometric determination of gold(III) by formation of dicyanoaurate(I) and its solvent extraction with methylene blue. Anal. Sci., 2:249-53.
18. Matouskova, E., Mcova, I.N. and Suk, V. 1980. The spectrophotometric determination of gold with bromopyrogallol red. Microchem. J., 25:403-9.
19. Medved, J., Bujdos, M., Mats, P., Matus, P. and Kubova, J. 2004. Determination of trace amounts of gold in acid-attacked environmental samples by atomic absorption spectrometry with electro thermal atomization after preconcentration. Anal. Bioanal. Chem., 379:60-5.
20. Melwanki, M.B., Masti, S.P. and Seetharamappa, J. 2002. Determination of trace amounts of gold(III) using ethopropazine hydrochloride and isothipendyl hydrochloride: spectrophotometric study. Turk J. Chem., 26:17-22.
21. Mirza, M.Y. 1980. Studies on the extraction of platinum metals with tri-iso-octylamine from hydrochloric and hydrobromic acid separation and determination of gold, palladium and platinum. Talanta, 27:101-6.
22. Mitra, S. 2003. Sample Preparation Techniques in Analytical Chemistry. Wiley-Interscience, New Jersey. 14.
23. Nat., A., Ene, A. and Lupu, R. 2004. Rapid determination of goLd in Romanian auriferous aLLuviaL sands,concentrates and rocks by 14 MeV NAA. J. Radional. Nucl. chem., 261:179-88.
24. Ojeda, C.B., Torres, A.G., Rojas, F.S. and Pavon, JMC. 1987. Fluorimetric determination of trace amounts gallium in biological tissues. Analyst., 112:1499-501.
25. Ortuno, J.A., Perez-Ruiz, T., Sanchez-Pedreno, C. and Buendia, P.M. 1984. 1,2,4,6-Tetraphenylpyridinium perchlorate as a reagent for ion-association complex formation and its use for the spectrophotometric determination of gold. Microchem. J., 30:71-8.
26. Pal, A. 1999. Photoinitiated gold sol generation in aqueous Triton X-100 and its analytical application for spectrophotometric determination of gold. Talanta, 46:583-87.
27. Pal, B. and Chowdhury, B. 1984. Triazene-N.-oxides as new type of fluorimetric reagents. Part I: trace determination of zirconium at the nanogram level, Mikrochim. Acta., 83:121-31.
28. Parker, G.A. 1983. Analytical Chemistry of Molybdenum. Springer-Vergal, Berline.
29. Patell, K.S. and Lieser, K. 1986. Extraction and spectrophotometric determination of gold (III) by use of amides and amidines. Anal. Chem., 58:1547-51.
30. Pramauro, E., Prevot, A.B., Pelizzetti, E., Marchelli, R., Dossena, A. and Biancardi, A. 1992. Quantitative removal of uranyl ions from aqueous solutions using micellar-enhanced ultrafiltration. Anal. Chim. Acta., 264(2):303-10.
31. Pyrzynska, K. 2005. Recent developments in the determination of gold by atomic absorption spectrometry technique. Spectrochemica. Acta., Part(B. 60):1316-22.
32. Salam, M.A. and Chowdhury, D.A. 1997. Preparation and characterization of shiff-base reagents. Bull. Pure Appl. Chem., 16C:45-9.
33. Sandell, E.B. 1965. Colorimetric Determination of Traces of Metals, Interscience, New York. 269.
34. Stahr, H.M. 1991. Analytical Methods in Toxicology, third ed. John Wiley and sons, New York. 75.
35. Tani, H., Kamidate, T. and Walanabe, H. 1998. Aqueous micellar two-phase system for protein separation. Anal. Sci., 14:875-9.
36. Wu, Y., Jiang, Z., Hu, B. and Duan, J. 2004. Electro thermal vaporization inductively coupled plasma atomic emission spectrometry for the determination of gold, palladium, and platinum using chelating resinYPA4 as both extractant and chemical modifier. Talanta, 63:585-292.
37. Yoe, J.A. and Jones, A.L. 1944. Stability constant of coordination compounds. Ind. Eng. Chem. Anal. Ed., 16:11.
38. Zaijun, L., Jiaomai, P. and Jian, T. 2003. Highly sensitive and selective spectrophotometric method for determination of trace gold in geological samples with 5-(2-hydroxy-5-nitrophenylazo)- rhodanine. Anal. Bioanal. Chem., 375:408-41.
39. Zhao, J., Li, J., Hung, Z., Huang, Z., Wei, Q., Chen, J. and Yang, G. 2006. Study on the solid phase extraction and spectrophotometric determination of gold in water and ore with 5-(p-aminobenzylidene)-thiorhodanine. Indian J. Chem., 45A:1651-5.