Preparative isolation and purification of acetophenones from the Chinese medicinal plant Cynanchum bungei Decne. by high-speed counter-current chromatography

Separation and Purification Technology

Volumn 64, Issue 2, 2008, Pages 247-252

  Liu, Zhengbo ^a   Sun, Yinshi ^a   Wang, Jianhua ^a   Zhu, Haifang ^a   Zhou, Hongying ^a   Hu, Jiangning ^b   Wang, Jun ^a  

^a SHANDONG AGRICULTURAL UNIVERSITY   (China)

^b Chungnam National University   (South Korea)

Author keywords

Acetophenones; Cynanchum bungei Decne.; High speed counter current chromatography

Indexed keywords

CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ESTERS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; MAGNESIUM PRINTING PLATES; MAGNETIC RESONANCE; MASS SPECTROMETRY; METHANOL; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANIC SOLVENTS; PETROLEUM REFINERIES; PURIFICATION; RESONANCE;

ACETOPHENONES; CHINESE MEDICINAL PLANTS; CRUDE SAMPLES; CYNANCHUM BUNGEI DECNE.; ETHYL ACETATES; HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY; HYDROXYACETOPHENONE; PREPARATIVE ISOLATIONS; SOLVENT SYSTEMS;

LIQUID CHROMATOGRAPHY;

CYNANCHUM;

EID: 56649118853     PISSN: 13835866     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.seppur.2008.10.002     Document Type: Article

References (12)

1. China Pharmacopoeia Committee, Pharmacopoeia of the people's republic of China, 1977, 178.
2. Xu L.C., Zhang H., and Xv C.S. Studies on chemical structure and modern medicament of baishouwu. Chin. Arch. Tradit. Chin. Med. 21 (2003) 1893-1895 1959
3. Gao L.J., Wang J.H., Cui J.H., and Wang H.Z. Studies on immunoregulation of polysaccharides-1a from Radix Cynanchi bungei. China J. Chin. Mater. Med. 30 (2005) 352-355
4. Institute of Material Medica Chinese Academy of Medical Sciences, New edition of ZhongYaoZhi, 1982, 328.
5. Li J., kadota S., kawata Y., Hattor M., Xu G.J., and Namba T. Constituents of the root of Cynanchum bungei Decne. Isolation and structures of new glucosides, bungeiside-A, -B, -C and -D. Chem. Pharm. Bull. 40 (1992) 3133-3137
6. J.J. Zhang, Study on chemical constituents of the Taishanbaishouwu, Master's Thesis, Beijing University of Chinese Medicine, 1997, pp. 31-35.
7. A.Q. Lin, Extraction, isolation and identification of Chemical Constituents from Taishanbaishouwu, Master's Thesis, Shandong Traditional Chinese Medical University, 2005, pp. 8-10.
8. Ito Y. Recent advances in counter-current chromatography. J. Chromatogr. A 538 (1991) 3-25
9. Wang X., Liu J.H., Zhang T.Y., and Ito Y. Rapid simple method for quality control of raw materials of herbs by HSCCC. J. Liq. Chromatogr. Related. Technol. 30 (2007) 2585-2592
10. Li L., Tsao R., Yang R., Liu C.M., Young J.C., and Zhu H.H. Isolation and purification of phenylethanoid glycosides from Cistanche deserticola by high-speed counter-current chromatography. Food Chem. 108 (2008) 702-710
11. Liu Z.L., Yu Y., Shen P.N., Wang J., Wang C.Y., and Shen Y.J. Separation and purification of dl-tetrahydropalmatine from Corydalis yanhusuo by high-speed counter-current chromatography. Sep. Purif. Technol. 58 (2008) 343-346
12. Kohler N., Wray V., and Winterhalter P. Preparative isolation of procyanidins from grape seed extracts by high-speed counter-current chromatography. J. Chromatogr. A 1177 (2008) 114-125