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Volumn 331, Issue 1-2, 2008, Pages 16-24

High resolution NMR for the direct characterisation of complex polyoxyethylated alcohols (CiEj) mixtures

Author keywords

1H and 13C NMR; Alkyl chain distribution; CiEj; Ethoxylate distribution; Polyethoxylated surfactants

Indexed keywords

ALKYLATION; MIXTURES; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYETHYLENE GLYCOLS; POLYETHYLENE OXIDES;

EID: 56549130233     PISSN: 09277757     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.colsurfa.2008.05.007     Document Type: Article
Times cited : (7)

References (28)
  • 2
    • 0026381940 scopus 로고
    • Influence of ethoxylate distribution on interfacial properties of linear and branched ethoxylate surfactants
    • Varadaraj R., Bock J., Geissler P., Zushma S., Brons N., and Colletti T. Influence of ethoxylate distribution on interfacial properties of linear and branched ethoxylate surfactants. J. Colloid Interface Sci. 147 (1991) 396-402
    • (1991) J. Colloid Interface Sci. , vol.147 , pp. 396-402
    • Varadaraj, R.1    Bock, J.2    Geissler, P.3    Zushma, S.4    Brons, N.5    Colletti, T.6
  • 3
    • 0026405087 scopus 로고
    • Effect of hydrocarbon chain branching on interfacial properties of monodisperse ethoxylated alcohol surfactants
    • Varadaraj R., Bock J., Zushma S., Brons N., and Colletti T. Effect of hydrocarbon chain branching on interfacial properties of monodisperse ethoxylated alcohol surfactants. J. Colloid Interface Sci. 147 (1991) 387-395
    • (1991) J. Colloid Interface Sci. , vol.147 , pp. 387-395
    • Varadaraj, R.1    Bock, J.2    Zushma, S.3    Brons, N.4    Colletti, T.5
  • 4
    • 0029884772 scopus 로고    scopus 로고
    • Chromatographic determination of non-ionic aliphatic surfactants of the alcohol polyethoxylate type in the environment
    • A
    • Marcomini A., and Zanette M. Chromatographic determination of non-ionic aliphatic surfactants of the alcohol polyethoxylate type in the environment. J. Chromatogr. 733 (1996) 193-206 A
    • (1996) J. Chromatogr. , vol.733 , pp. 193-206
    • Marcomini, A.1    Zanette, M.2
  • 6
    • 22944456519 scopus 로고    scopus 로고
    • Quantitative assessment of alkyl chain branching in alcohol-based surfactants by nuclear magnetic resonance
    • van Duynhoven J.P.M., Leika A., and van der Hoeven P.C. Quantitative assessment of alkyl chain branching in alcohol-based surfactants by nuclear magnetic resonance. J. Surfactants Deterg. 8 (2005) 73-82
    • (2005) J. Surfactants Deterg. , vol.8 , pp. 73-82
    • van Duynhoven, J.P.M.1    Leika, A.2    van der Hoeven, P.C.3
  • 7
    • 26544432769 scopus 로고
    • Applications of high resolution nuclear magnetic resonance (n.m.r.) spectrometry to the identification and quantitative analysis of nonionic surfactants
    • Flanagan P.W., Greff R.A., and Smith H.F. Applications of high resolution nuclear magnetic resonance (n.m.r.) spectrometry to the identification and quantitative analysis of nonionic surfactants. Anal. Chem. 35 (1963) 1283-1285
    • (1963) Anal. Chem. , vol.35 , pp. 1283-1285
    • Flanagan, P.W.1    Greff, R.A.2    Smith, H.F.3
  • 8
    • 51249175740 scopus 로고
    • Application of carbon-13 NMR to the identification of surfactants in mixture
    • Carminati G., Cavalli L., and Buosi F. Application of carbon-13 NMR to the identification of surfactants in mixture. J. Am. Oil Chem. Soc. 65 (1988) 669-677
    • (1988) J. Am. Oil Chem. Soc. , vol.65 , pp. 669-677
    • Carminati, G.1    Cavalli, L.2    Buosi, F.3
  • 9
    • 0029870584 scopus 로고    scopus 로고
    • Homolog separation of linear alcohol ethoxylates by high-performance liquid chromatography
    • A
    • Lemr K. Homolog separation of linear alcohol ethoxylates by high-performance liquid chromatography. J. Chromatogr. 732 (1996) 299-305 A
    • (1996) J. Chromatogr. , vol.732 , pp. 299-305
    • Lemr, K.1
  • 10
    • 0342470586 scopus 로고    scopus 로고
    • Analysis of polyethoxylated surfactants in microemulsion-oil-water systems
    • Marquez N., Bravo B., Chavez G., Ysambertt F., and Salager J.L. Analysis of polyethoxylated surfactants in microemulsion-oil-water systems. Anal. Chim. Acta 405 (2000) 267-275
    • (2000) Anal. Chim. Acta , vol.405 , pp. 267-275
    • Marquez, N.1    Bravo, B.2    Chavez, G.3    Ysambertt, F.4    Salager, J.L.5
  • 11
    • 0037203872 scopus 로고    scopus 로고
    • Analysis of polyethoxylated surfactants in microemulsion-oil-water systems Part II
    • Marquez N., Bravo B., Chavez G., Ysambertt F., and Salager J.L. Analysis of polyethoxylated surfactants in microemulsion-oil-water systems Part II. Anal. Chim. Acta 452 (2002) 129-141
    • (2002) Anal. Chim. Acta , vol.452 , pp. 129-141
    • Marquez, N.1    Bravo, B.2    Chavez, G.3    Ysambertt, F.4    Salager, J.L.5
  • 12
    • 0037415272 scopus 로고    scopus 로고
    • Analysis of polyethoxylated surfactants in microemulsion-oil-water systems III. Fractionation and partitioning of polyethoxylated alcohol surfactants
    • Marquez N., Bravo B., Ysambertt F., Chavez G., Subero N., and Salager J.L. Analysis of polyethoxylated surfactants in microemulsion-oil-water systems III. Fractionation and partitioning of polyethoxylated alcohol surfactants. Anal. Chim. Acta 477 (2003) 293-303
    • (2003) Anal. Chim. Acta , vol.477 , pp. 293-303
    • Marquez, N.1    Bravo, B.2    Ysambertt, F.3    Chavez, G.4    Subero, N.5    Salager, J.L.6
  • 13
    • 0037199642 scopus 로고    scopus 로고
    • Determination of nonylphenol polyethoxylates in household detergents by high-performance liquid chromatography
    • A
    • Cheng C.-Y., and Ding W.-H. Determination of nonylphenol polyethoxylates in household detergents by high-performance liquid chromatography. J. Chromatogr. 968 (2002) 143-150 A
    • (2002) J. Chromatogr. , vol.968 , pp. 143-150
    • Cheng, C.-Y.1    Ding, W.-H.2
  • 14
    • 0000126301 scopus 로고
    • Determination of nonionic polyethoxylate surfactants in environmental waters by liquid chromatography/electrospray mass spectrometry
    • Crescenzi C., Di Corcia A., Samperi R., and Marcomini A. Determination of nonionic polyethoxylate surfactants in environmental waters by liquid chromatography/electrospray mass spectrometry. Anal. Chem. 67 (1995) 1797-1804
    • (1995) Anal. Chem. , vol.67 , pp. 1797-1804
    • Crescenzi, C.1    Di Corcia, A.2    Samperi, R.3    Marcomini, A.4
  • 15
    • 0345195996 scopus 로고    scopus 로고
    • Investigation of chromatographic behavior of ethoxylated alcohol surfactants in normal-phase and reversed-phase systems using high-performance liquid chromatography-mass spectrometry
    • A
    • Jandera P., Holcapek M., and Theodoridis G. Investigation of chromatographic behavior of ethoxylated alcohol surfactants in normal-phase and reversed-phase systems using high-performance liquid chromatography-mass spectrometry. J. Chromatogr. 813 (1998) 299-311 A
    • (1998) J. Chromatogr. , vol.813 , pp. 299-311
    • Jandera, P.1    Holcapek, M.2    Theodoridis, G.3
  • 16
    • 4744358495 scopus 로고    scopus 로고
    • Increasing UV detection sensitivity in the supercritical fluid chromatographic analysis of alcohol polyethers
    • A
    • Hoffman B.J., Taylor L.T., Rumbelow S., and Pinkston J.D. Increasing UV detection sensitivity in the supercritical fluid chromatographic analysis of alcohol polyethers. J. Chromatogr. 1052 (2004) 161-166 A
    • (2004) J. Chromatogr. , vol.1052 , pp. 161-166
    • Hoffman, B.J.1    Taylor, L.T.2    Rumbelow, S.3    Pinkston, J.D.4
  • 17
    • 0141924425 scopus 로고    scopus 로고
    • Simultaneous quantitative analysis of anionic, cationic, and nonionic surfactants in water by electrospray ionization mass spectrometry with flow injection analysis
    • Barco M., Planas C., Palacios O., Ventura F., Rivera J., and Caixach J. Simultaneous quantitative analysis of anionic, cationic, and nonionic surfactants in water by electrospray ionization mass spectrometry with flow injection analysis. Anal. Chem. 75 (2003) 5129-5136
    • (2003) Anal. Chem. , vol.75 , pp. 5129-5136
    • Barco, M.1    Planas, C.2    Palacios, O.3    Ventura, F.4    Rivera, J.5    Caixach, J.6
  • 18
    • 33646901618 scopus 로고    scopus 로고
    • On the determination of underivatised fatty alcohol ethoxylates by electrospray ionisation-mass spectrometry
    • Bernabe-Zafon V., Simo-Alfonso E.F., and Ramis-Ramos G. On the determination of underivatised fatty alcohol ethoxylates by electrospray ionisation-mass spectrometry. J. Chromatogr. A 1118 (2006) 188
    • (2006) J. Chromatogr. A , vol.1118 , pp. 188
    • Bernabe-Zafon, V.1    Simo-Alfonso, E.F.2    Ramis-Ramos, G.3
  • 19
    • 0029883763 scopus 로고    scopus 로고
    • Capillary gas chromatography of higher alkylpolyoxyethylene glycols with an even number of carbon atoms in the alkyl group. Influence of type of derivatizing agent, alcohol chain length and oxyethylene chain length on the retention indices with a linear temperature increase
    • A
    • Komarek K., Minar J., and Skvarenina S. Capillary gas chromatography of higher alkylpolyoxyethylene glycols with an even number of carbon atoms in the alkyl group. Influence of type of derivatizing agent, alcohol chain length and oxyethylene chain length on the retention indices with a linear temperature increase. J. Chromatogr. 727 (1996) 131-138 A
    • (1996) J. Chromatogr. , vol.727 , pp. 131-138
    • Komarek, K.1    Minar, J.2    Skvarenina, S.3
  • 20
    • 0042426330 scopus 로고    scopus 로고
    • Capillary gas chromatography-mass spectrometry of lower oxyethylenated aliphatic alcohols
    • A
    • Komarek K., Pitthard V., Kostrubanicova E., Skvarenina S., and Hoffmann J. Capillary gas chromatography-mass spectrometry of lower oxyethylenated aliphatic alcohols. J. Chromatogr. 773 (1997) 219-226 A
    • (1997) J. Chromatogr. , vol.773 , pp. 219-226
    • Komarek, K.1    Pitthard, V.2    Kostrubanicova, E.3    Skvarenina, S.4    Hoffmann, J.5
  • 21
    • 0032571542 scopus 로고    scopus 로고
    • Capillary gas chromatography of n-butyl and isobutyl-n-amyl and isoamyl polyethylene glycol ethers and their derivatives
    • A
    • Komarek K., Richter P., and Hoffmann J. Capillary gas chromatography of n-butyl and isobutyl-n-amyl and isoamyl polyethylene glycol ethers and their derivatives. J. Chromatogr. 800 (1998) 305-315 A
    • (1998) J. Chromatogr. , vol.800 , pp. 305-315
    • Komarek, K.1    Richter, P.2    Hoffmann, J.3
  • 22
    • 0031728617 scopus 로고    scopus 로고
    • Determination of non-ionic surfactants of the alcohol polyethoxylate type by means of high temperature gas chromatography and atomic emission detection
    • Asmussen C., and Stan H.-J. Determination of non-ionic surfactants of the alcohol polyethoxylate type by means of high temperature gas chromatography and atomic emission detection. J. High Resolut. Chromatogr. 21 (1998) 597-604
    • (1998) J. High Resolut. Chromatogr. , vol.21 , pp. 597-604
    • Asmussen, C.1    Stan, H.-J.2
  • 23
    • 0030243130 scopus 로고    scopus 로고
    • Analysis of a technical poly(ethylene oxide) by online HPLC/1H-NMR
    • Pasch H., and Hiller W. Analysis of a technical poly(ethylene oxide) by online HPLC/1H-NMR. Macromolecules 29 (1996) 6556-6559
    • (1996) Macromolecules , vol.29 , pp. 6556-6559
    • Pasch, H.1    Hiller, W.2
  • 25
    • 5644269152 scopus 로고    scopus 로고
    • Separation of fatty alcohol polyethoxylates by capillary electrophoresis through easy electroosmotic flow control with a quaternary diammonium salt
    • A
    • Sebastiano R., Citterio A., Righetti P.G., Simo-Alfonso E., and Ramis-Ramos G. Separation of fatty alcohol polyethoxylates by capillary electrophoresis through easy electroosmotic flow control with a quaternary diammonium salt. J. Chromatogr. 1053 (2004) 235-239 A
    • (2004) J. Chromatogr. , vol.1053 , pp. 235-239
    • Sebastiano, R.1    Citterio, A.2    Righetti, P.G.3    Simo-Alfonso, E.4    Ramis-Ramos, G.5
  • 26
    • 0000559579 scopus 로고    scopus 로고
    • Oligomeric separation of ionic and nonionic ethoxylated polymers by Capillary Gel Electrophoresis
    • Wallingford R.A. Oligomeric separation of ionic and nonionic ethoxylated polymers by Capillary Gel Electrophoresis. Anal. Chem. 68 (1996) 2541-2548
    • (1996) Anal. Chem. , vol.68 , pp. 2541-2548
    • Wallingford, R.A.1
  • 27
    • 1842741217 scopus 로고    scopus 로고
    • New modified electrodes for the separate determination of polyoxyethylated nonylphenols
    • Kulapin A.I., Chernova R.K., and Kulapina E.G. New modified electrodes for the separate determination of polyoxyethylated nonylphenols. J. Anal. Chem. 57 (2002) 638-643
    • (2002) J. Anal. Chem. , vol.57 , pp. 638-643
    • Kulapin, A.I.1    Chernova, R.K.2    Kulapina, E.G.3
  • 28
    • 33845222161 scopus 로고    scopus 로고
    • Nonionic surfactant-selective electrode and its application for determination in real solutions
    • Sak-Bosnar M., Madunic-Cacic D., Matesic-Puac R., and Grabaric Z. Nonionic surfactant-selective electrode and its application for determination in real solutions. Anal. Chim. Acta 581 (2007) 355-363
    • (2007) Anal. Chim. Acta , vol.581 , pp. 355-363
    • Sak-Bosnar, M.1    Madunic-Cacic, D.2    Matesic-Puac, R.3    Grabaric, Z.4


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