A commonly used spin label: S-(2,2,5,5-tetra-methyl-1-oxyl- Δ3-pyrrolin-3-ylmeth-yl) methane-thio-sulfonate

Acta Crystallographica Section C: Crystal Structure Communications

Volumn 64, Issue 11, 2008, Pages

  Zielke, Vitali ^a   Eickmeier, Henning ^a   Hideg, Kalman ^b   Reuter, Hans ^a   Steinhoff, Heinz Jürgen ^a  

^a UNIVERSITY OF OSNABRÜCK   (Germany)

^b UNIVERSITY OF PÉCS   (Hungary)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMIC PHYSICS; ATOMS; COLUMNS (STRUCTURAL); HYDROCARBONS; METHANE; SPIN DYNAMICS; STEREOCHEMISTRY;

ASYMMETRIC UNITS; BOND LENGTHS AND ANGLES; C ATOMS; DOUBLE BONDS; METHYL GROUPS; PLANAR CHIRALITIES; SIDE CHAINS; SOLID STATES; SPIN LABELS; TITLE COMPOUNDS;

CRYSTAL STRUCTURE;

MESYLIC ACID DERIVATIVE; METHANETHIOSULFONATE; PYRROLE DERIVATIVE; PYRROLINE;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; CRYSTALLIZATION; CRYSTALLOGRAPHY; METHODOLOGY; SPIN LABELING; SYNTHESIS;

CRYSTALLIZATION; CRYSTALLOGRAPHY; MESYLATES; MODELS, MOLECULAR; MOLECULAR CONFORMATION; PYRROLES; SPIN LABELS;

TETRA;

EID: 55749115794     PISSN: 01082701     EISSN: 01082701     Source Type: Journal    
DOI: 10.1107/S0108270108032113     Document Type: Article

References (29)

1. Allen, F. H., Kennard, O., Watson, D. O., Brammer, L., Orpen, A. O. & Taylor, R. (1987). J. Chem. Soc. Perkin Trans 2, pp. S1-19.
2. Altenbach, C., Marti, T., Khorana, H. G. & Hubbell, W. L. (1990). Science, 248, 1088-1092.
3. Balog, M., Abé, C., Kalai, T., Steinhoff, H.-J., Jeko, J. & Hideg, K. (2007). Synthesis, pp. 1663-1670.
4. Balog, M., Kalai, T., Jekö, J., Berente, Z., Steinhoff, H.-J., Engelhard, M. & Hideg, K. (2003). Tetrahedron Lett. 44, 9213-9217.
5. Balog, M., Kalai, T., Jekö, J., Steinhoff, H.-J., Engelhard, M. & Hideg, K. (2004). Synlett, 14, 2591-2593.
6. Beier, C. & Steinhoff, H. I (2006). Biophys. J. 91, 2647-2664.
7. Berliner, L. J., Grunwald, J., Hankovszky, H. O. & Hideg, K. (1982). Anal. Biochem. 119, 450-455.
8. Boeyens, J. C. A. & Kruger, G. J. (1970). Acta Cryst. B26, 668-672.
9. Bordignon, E. & Steinhoff, H. J. (2007). Biological Magnetic Resonance, Vol. 27, ESR Spectroscopy in Membrane Biophysics, edited by M. A. Hemminga & L. J. Berliner, pp. 129-164. Berlin: Springer.
10. Brandenburg, K. (1999). DIAMOND. Version 2.1c. Crystal Impact GbR, Bonn, Germany.
11. Bruker (2004). SADABS and SMART. Bruker AXS Inc., Madison, Wisconsin, USA.
12. Bruker (2007). SAINT. Version 7.34A. Bruker AXS Inc., Madison, Wisconsin, USA.
13. Budil, D. E., Sale, K. L., Khairy, K. A. & Fajer, P. G. (2006). J. Phys. Chem. A, 110, 3703-3713.
14. DeSensi, S. C., Rangel, D. P., Beth, A. H., Lybrand, T. P. & Hustedt, E. J. (2008). Biophys. J. 94, 3798-3809.
15. Dickman, M. H. & Doedens, R. J. (1983). Inorg. Chem. 22, 1591-1594.
16. Duskova, J., Labsky, J., Hasek, J. & Cisarova, I. (2001). Acta Cryst. E57, 085-086.
17. Fegy, K., Sanz, N., Luneau, D., Belorizky, E. & Rey, P. (1998). Inorg. Chem. 37, 4518-4523.
18. Hirel, C., Vostrikova, K. E., Pécaut, J., Ovcharcnko, V. I. & Rey, P. (2001). Chem. Eur. J. 7, 2007-2014.
19. Hubbell, W. L., Mchaourab, H. S., Altenbach, C. & Lietzow, M. A. (1996). Structure, 4, 779-783.
20. Niermann, N., Degefa, T. H., Walder, L., Zielke, V, Steinhoff, H. J., Onsgaard, J. & Speller, S. (2006). Phys. Rev. B, 74, 235424.
21. Osiecki, J. H. & Ullman, E. F. (1968). J. Am. Chem. Soc. 90, 1078-1079.
22. Papoutsakis, D., Kirby, J. P., Jackson, J. E. & Nocera, D. G. (1999). Chem. Eur. J. 5, 1474-1480.
23. Porter, L. C. & Doedens, R. J. (1984). Acta Cryst. C40, 1814-1817.
24. Sezer, D., Freed, J. H. & Roux, B. (2008a). J. Phys. Chem. B, 112, 5755-5767.
25. Sezer, D., Freed, J. H. & Roux, B. (2008b). J. Chem. Phys. 128, 165106.
26. Sheldrick, G. M. (2008). Acta Cryst. A64, 112-122.
27. Steinhoff, H.-J., Mollaaghababa, R., Altenbach, C., Hideg, K., Krebs, M., Khorana, H. G. & Hubbell, W. L. (1994). Science, 266, 105-122.
28. Turley, J. W. & Boer, F. P. (1972). Acta Cryst. B28, 1641-1644.
29. Wiley, D. W., Calabrese, J. C., Harlow, R. L. & Miller, J. S. (1991). Angew. Chem. Int. Ed. 30, 450-452.