SCOPUS 정보 검색 플랫폼

Volumn , Issue 17, 2008, Pages 2689-2691

α-Arylation of aryl ketones: Expanding the scope of the Truce-Smiles rearrangement

Author keywords

Arylation; Indole; Ketone; Rearrangement; Truce Smiles

Indexed keywords

2 (1H INDOL 2 YL)PHENOL; KETONE DERIVATIVE; PHENOL DERIVATIVE; UNCLASSIFIED DRUG;

ALPHA ARYLATION; ARTICLE; ARYLATION; CHEMICAL STRUCTURE; REACTION ANALYSIS; SYNTHESIS; TRUCE SMILES REARRANGEMENT;

EID: 55549106494 PISSN: 09365214 EISSN: None Source Type: Journal
DOI: 10.1055/s-0028-1083523 Document Type: Article

Times cited : (29)

References (10)

1
- 55549133125
- UK
- New Address: T. J. Snape, School of Pharmacy, Maudland Building, University of Central Lancashire, Preston, PR1 2HE, UK.
- Snape, School of Pharmacy, Maudland Building, University of Central Lancashire, Preston, PR1
- New Address, T.J.¹

2
- 0000585779
- Millard, A.; Rathke, M. J. Am. Chem. Soc. 1977, 99, 4833.
- (1977) J. Am. Chem. Soc , vol.99 , pp. 4833
- Millard, A.¹ Rathke, M.²

3
- 15744377645
- Bella, M.; Kobbelgaard, S.; Jørgensen, K. J. Am. Chem. Soc. 2005, 127, 3670.
- (2005) J. Am. Chem. Soc , vol.127 , pp. 3670
- Bella, M.¹ Kobbelgaard, S.² Jørgensen, K.³

4
- 0037366605
- Horton, D.; Bourne, G.; Smythe, M. Chem. Rev. 2003,103, 893.
- (2003) Chem. Rev , vol.103 , pp. 893
- Horton, D.¹ Bourne, G.² Smythe, M.³

5
- 3042582144
- Mitchell, L.; Barvian, N. Tetrahedron Lett. 2004, 45, 5669.
- (2004) Tetrahedron Lett , vol.45 , pp. 5669
- Mitchell, L.¹ Barvian, N.²

6
- 0343496824
- Erickson, W.; McKennon, M. Tetrahedron Lett. 2000, 41, 4541.
- (2000) Tetrahedron Lett , vol.41 , pp. 4541
- Erickson, W.¹ McKennon, M.²

7
- 54449097480
- in press; DOI:10.1039/ B808960D
- Snape, T. Chem. Soc. Rev. 2008, in press; DOI:10.1039/ B808960D.
- (2008) Chem. Soc. Rev
- Snape, T.¹

9
- 0000141869
- Bordwell, F.; Cornforth, F. J. Org. Chem. 1978, 43, 1763.
- (1978) J. Org. Chem , vol.43 , pp. 1763
- Bordwell, F.¹ Cornforth, F.²

10
- 55549133461
- Synthesis of 18 1-(2-Hydroxyphenyl)-2-(2-nitrophenyl)ethanone (5,105 mg, 0.41 mmol) was dissolved in MeOH (4.1 mL, Then, Pd/C (10 mg, 10 wt, was added, and the flask evacuated and backfilled with hydrogen (3 cycles, The reaction was then stirred under an atmosphere of hydrogen for 18 h. The reaction was filtered through Celite and eluted with MeOH (10 mL) and the solvent removed in vacuo. The crude product was purified by column chromatography On silica gel (10% EtOAc in PE) to give the title compound as a pale yellow solid (62 mg, 72, Rf, 0.39 (30% EtOAc in PE, mp 170-172 °C (EtOAc-PE, IR: nmax 3500 (OH, 3425 (NH) cm -1. 1H NMR (300 MHz, CDCl3, d, 9.22 (1 H, br s, 7.70 (1 H, dd, J, 1.6, 7.8 Hz, Ar, 7.66 (1 H, d, J, 7.8 Hz, Ar, 7.42 (1 H, d, J, 8.1 Hz, Ar, 7,26-7.11 (3 H, m, Ar, 7.04(1 H, td, J, 1.1,7.6Hz, Ar, 6.91 1 H, dd, J, 0.9, 8.1 Hz, Ar, 6.87
- +]: 210.0919; found: 210.0920.

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