On-line monitoring of composite nanoparticles synthesized in a pre-industrial laser pyrolysis reactor using Laser-Induced Breakdown Spectroscopy

Spectrochimica Acta - Part B Atomic Spectroscopy

Volumn 63, Issue 10, 2008, Pages 1183-1190

  Amodeo, Tanguy ^a   Dutouquet, Christophe ^a   Tenegal, François ^b   Guizard, Benoît ^b   Maskrot, Hicham ^b   Le Bihan, Olivier ^a   Fréjafon, Emeric ^a  

^a INSTITUT NATIONAL DE L ENVIRONNEMENT INDUSTRIEL ET DES RISQUES INERIS   (France)

^b SRMA   (France)

Author keywords

Composite nanoparticles; Laser pyrolysis; LIBS; On line monitoring; Process control

Indexed keywords

ATOMIC EMISSION SPECTROSCOPY; COMPOSITE MATERIALS; LASER INDUCED BREAKDOWN SPECTROSCOPY; LASER PRODUCED PLASMAS; MONITORING; NANOPARTICLES; OPTIMIZATION; PROCESS CONTROL; PROCESS MONITORING; PYROLYSIS; SILICON CARBIDE; STOICHIOMETRY; SYNTHESIS (CHEMICAL); VOLTAGE MEASUREMENT;

COMPOSITE NANOPARTICLES; LASER PYROLYSIS; LASERINDUCED BREAKDOWN SPECTROSCOPY (LIBS); LIBS; ON-LINE MONITORING SYSTEM; ONLINE MONITORING; REAL TIME MONITORING SYSTEM; REAL-TIME PROCESS MONITORING;

ARGON LASERS;

EID: 55549101236     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.sab.2008.09.005     Document Type: Article

References (28)

1. Cannon W.R., Danforth S.C., Haggerty J.S., and Marra R.A. Sinterable ceramic powders from laser-driven reactions: II, powder characteristics and process variables. J. Am. Ceram. Soc. 65 (1982) 330-335
2. Fichet P., Mauchien P., and Moulin C. Determination of impurities in uranium and plutonium dioxides by Laser-Induced Breakdown Spectroscopy. Appl. Spectrosc. 53 (1999) 1111-1117
3. Fichet P., Mauchien P., Wagner J.F., and Moulin C. Quantitative elemental determination in water and oil by Laser-Induced Breakdown Spectroscopy. Anal. Chim. Acta 429 (2001) 269-278
4. Dudragne L., Adam Ph., and Amouroux J. Time-resolved Laser-Induced Breakdown Spectroscopy: application for qualitative and quantitative detection of fluorine, chlorine, sulfur and carbon in air. Appl. Spectrosc. 52 (1998) 1321-1327
5. Cremers D.A., and Radziemski L.J. Detection of chlorine and fluorine in air by Laser-Induced Breakdown Spectroscopy. Anal. Chem. 55 (1983) 1252-1256
6. Hahn D.W., and Lunden M.M. Detection and analysis of aerosol particles by Laser-Induced Breakdown Spectroscopy. Aerosol Sci. Technol. 33 (2000) 30-48
7. Radziemski L.J., Loree T.R., Cremers D.A., and Hoffman N.M. Time-resolved laser-induced breakdown spectrometry of aerosols. Anal. Chem. 55 (1983) 1246-1252
8. Noll R., Bette H., Brysch A., Krausharr M., Mönch I., Peter L., and Sturm V. Laser-induced breakdown spectrometry - applications for production control and quality assurance in the steel industry. Spectrochim. Acta Part B 56 (2001) 637-649
9. Gruber J., Heitz J., Strasser H., Bäuerle D., and Ramaseder N. Rapid in-situ analysis of liquid steel by Laser-Induced Breakdown Spectroscopy. Spectrochim. Acta Part B 56 (2001) 685-693
10. Whitehouse A.I., Young J., Botheroyd I.M., Lawson S., Evans C.P., and Wright J. Remote materials analysis of nuclear power station steam generator tubes by Laser-Induced Breakdown Spectroscopy. Spectrochim. Acta Part B 56 (2001) 821-830
11. Hahn D.W., Flower W.L., and Hencken K.R. Discrete particle detection and metal emissions monitoring using Laser-Induced Breakdown Spectroscopy. Appl. Spectrosc. 51 (1997) 1836-1844
12. Neuhauser R.E., Panne U., Niessner R., and Wilbring P. On-line monitoring of chromium aerosols in industrial exhaust streams by laser-induced plasma spectroscopy (LIPS). J. Anal. Chem. 364 (1999) 720-726
13. Cheng M.-D. Field measurement comparison of aerosol metals using aerosol beam focused laser-induced plasma spectrometer and reference methods. Talanta 61 (2003) 127-137
14. Buckley S.G., Johnsen H.A., Hencken K.R., and Hahn D.W. Implementation of Laser-Induced Breakdown Spectroscopy as a continuous emission monitor for toxic metals. Waste Manage. 20 (2000) 455-462
15. Carranza J.E., Fisher B.T., Yoder G.D., and Hahn D.W. On-line analysis of ambient air aerosols using Laser-Induced Breakdown Spectroscopy. Spectrochim. Acta Part B 56 (2001) 851-864
16. Lithgow G.A., Robinson A.L., and Buckley S.G. Ambient measurements of metal-containing PM2.5 in an urban environment using Laser-Induced Breakdown Spectroscopy. Atmos. Environ. 38 (2004) 3319-3328
17. Cauchetier M., Croix O., Luce M., Michon M., Paris J., and Tistchenko S. Laser synthesis of ultrafine powders. Ceram. Int. 13 (1987) 13-17
18. http://physics.nist.gov/PhysRefData/ASD/lines_form.html.
19. Griem H.R. Principles of Plasma Spectroscopy (1997), Cambridge University Press
20. Miziolek A.W., Palleschi V., and Schechter I. Laser-Induced Breakdown Spectroscopy (2006), Cambridge University Press
21. Konjevic N., and Wiese W.L. Experimental stark widths and shifts for spectral lines of neutral and ionized atoms. J. Phys. Chem. Ref. Data 19 (1990) 1307-1385
22. Wiese W.L., Kelleher D.E., and Paquette D.R. Detailed study of the Stark broadening of Balmer lines in a high-density plasma. Phys. Rev. A At. Mol. Opt. Phy. 6 (1972) 1132-1153
23. Cremers D.A., and Radziemski L.J. Handbook of Laser-Induced Breakdown Spectroscopy (2006), Wiley
24. Carranza J.E., and Hahn D.W. Assessment of the upper particle size limit for quantitative analysis of aerosols using Laser-Induced Breakdown Spectroscopy. Anal. Chem. 74 (2002) 5450-5454
25. Hohreiter V., and Hahn D.W. Calibration effects for Laser-Induced Breakdown Spectroscopy of gaseous sample streams: analyte response of gas-phase species versus solid-phase species. Anal. Chem. 77 (2005) 1118-1124
26. Carranza J.E., and Hahn D.W. Plasma volume considerations for analysis of gaseous and aerosol samples using Laser-Induced Breakdown Spectroscopy. J. Anal. At. Spectrom. 17 (2002) 1534-1539
27. Hermann J., Boulmer-Leborgne C., and Hong D. Diagnostics of the early phase of an ultraviolet laser-induced plasma by spectral line analysis considering self-absorption. J. Appl. Phys. 83 (1998) 691-696
28. Hermann J., and Dutouquet C. Local thermal equilibrium plasma modeling for analyses of gas-phase reactions during reactive-laser ablation. J. Appl. Phys. 91 (2002) 10188-10193