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25
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55349128594
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note
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2 = 0.1827 (all data).
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26
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33646901345
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Nsouli N.H., Bassil B.S., Dickman M.H., Kortz U., Keita B., and Nadjo L. Inorg. Chem. 45 (2006) 3858
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Nsouli, N.H.1
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Nadjo, L.6
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27
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55349095511
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note
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-1. Elemental analyses calcd: W, 55.62; Ge, 3.25; Ti, 4.82; K, 6.57. Found: W, 55.13; Ge, 3.19; Ti, 4.66; K, 6.69.
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28
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55349089983
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note
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Synthesis of 2: The synthesis procedure of 2 is similar to that of 1 except that the pH was adjusted to 2. The colorless crystals were collected after one week. (0.17 g, 16.7% yield based on Ge). IR: 962(m), 887(s), 818(s), 750(sh), 637(sh), 537(m) and 468(s) cm-1. Elemental analyses calcd: W, 57.10; Ge, 2.51; Ti, 4.95; K, 4.95; S, 0.37. Found: W, 56.72; Ge, 2.28; Ti, 4.75; K, 5.17; S, 0.30.
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