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-1): 3300-3100s, br, O-H; 2968m, 2902m, C-H; 1670s, 1624s, 1361m, COO; 1311m, O-H; 1232w, 1213w, 1053s, C-O; 931s, C-H.
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int = 0.0444. R1 = 0.0322 for 697 observations of I ≥ 2σ(I), wR2 = 0.0923 for all data, GOF = 1.082. CCDC 694325. The atomic coordinates for this structure have been deposited with the Cambridge Crystallographic Data Centre. The coordinates can be obtained, upon request, from the Director, Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, U.K.
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