A transient permeation-based method for composite zeolite membranes characterization

AIChE Journal

Volumn 54, Issue 10, 2008, Pages 2527-2538

  Courthial, L ^a   Baudot, A ^a   Tayakout Fayolle, M ^a   Jallut, C ^b  

^a IFP ENERGIES NOUVELLES   (France)

^b UNIVERSITÉ LYON 1   (France)

Author keywords

Dynamic modeling; Mass transfer; Membrane; Transient techniques; Zeolite

Indexed keywords

BUTANE; COMPOSITE MEMBRANES; DIFFUSION; DYNAMIC MODELS; EQUILIBRIUM CONSTANTS; ISOMERS; MASS TRANSFER; MEMBRANES; NONDESTRUCTIVE EXAMINATION; TRANSPORT PROPERTIES; ZEOLITES;

ADSORPTION EQUILIBRIUM CONSTANTS; EXPERIMENTAL APPROACHES; NONDESTRUCTIVE CHARACTERIZATION; SYNTHESIS PROCEDURE; THERMODYNAMIC AND TRANSPORT PROPERTIES; TRANSIENT PERMEATION; TRANSIENT TECHNIQUES; TRANSPORT PHENOMENA;

PERMEATION;

EID: 54949125275     PISSN: 00011541     EISSN: 15475905     Source Type: Journal    
DOI: 10.1002/aic.11580     Document Type: Article

References (57)

1. Jallut C, Thomas G, Touré Y, Diard JP. Estimation de paramètres physico-chimiques et problèmes inverses. In: Corriou JP, editor. Automatique Et Procédés Chimiques. Paris; Hermes Science, 2001:51-99.
2. Gembarovic J, Vozar L, Majernik V. Using the least square method for data reduction in the flash method. Int J Heat Mass Transfer. 1990;33:1563-1565.
3. Roetzel W, Luo X, Xuan Y. Measurement of heat transfer coefficient and axial dispersion coefficient using temperature oscillations. Exp Therm Fluid Sci. 1993;7:345-353.
4. Ros S, Jallut C, Grillot JM, Amblard M. A transient-state technique for the heat transfer coefficient measurement in a corrugated plate heat exchanger channel based on frequency response and residence time distribution. Int J Heat Mass Transfer. 1995;38:1317-1325.
5. Hufton JR, Danner RP. Chromatographic study of alkanes in silicalite: equilibrium properties. AIChE J. 1993;39:954-961.
6. Hufton JR, Danner RP. Chromatographic study of alkanes in silicalite: transport properties. AIChE J. 1993;39:962-974.
7. Jolimaitre E, Tayakout-Fayolle M, Jallut C, Ragil K. Determination of mass transfer and thermodynamic properties of branched paraffins in silicalite by inverse chromatography technique. Ind Eng Chem Res. 2001;40:914-926.
8. Vonmeien OF, Biscaia EC, Nobrega R. Polymer-solute diffusion and equilibrium parameters by inverse gas chromatography. AIChE J. 1997;43:2932-2943.
9. Fujasova M, Linek V, Moucha T. Mass transfer correlations for multiple-impeller gas-liquid contactors. Analysis of the effect of axial dispersion in gas and liquid phases on 'local' kLa values measured by the dynamic pressure method in individual stages of the vessel. Chem Eng Sci. 2007;62:1650-1669.
10. Navarro-Laboulais J, Cardona SC, Torregrosa JI, Abad A, Lopez F. Structural identifiability analysis of the dynamic gas-liquid film model. AIChE J. 2006;52:2851-2863.
11. Perrin S, Chaudourne S, Jallut C, Lieto J. Transient state techniques for mass transfer characterization of a gas-liquid packed column. Chem Eng Sci. 2002;57:3335-3345.
12. Gleaves JT, Yablonskii GS, Phanawadee P, Schuurman Y. TAP-2: an interrogative kinetics approach. Appl Catal A. 1997;160:55-88.
13. Delgado JA, Nijhuis TA, Kapteijn F, Moulijn JA. Determination of adsorption and diffusion parameters in zeolites through a structured approach. Chem Eng Sci. 2004;59:2477-2487.
14. Berthier F, Diard JP, Montella C, Pronzato L, Walter E. Choice of experimental method induced by structural properties of mechanisms. J Electroanal Chem. 1995;399:1-6.
15. Kruczek B, Frisch HL, Chapanian R. Analytical solution for the effective time lag of a membrane in a permeate tube collector in which Knudsen flow regime exists. J Membr Sci. 2005;256:57-63.
16. Taveira P, Mendes A, Costa C. On the determination of diffusivity and sorption coefficients using different time-lag models. J Membr Sci. 2003;221:123-133.
17. Sanchez J. Gijiu CL, Hynek V, Muntean O, Julbe A. The application of transient time-lag method for the diffusion coefficient estimation on zeolite composite membranes. Sep Purif Technol. 2001;25:467-474.
18. Bennett KH, Cook KD, Falconer JL, Noble RD. Time-dependent permeance of gas mixtures through zeolite membranes. Anal Chem. 1999;71:1016-1020.
19. Gardner TQ, Falconer JL, Noble RD. Adsorption and diffusion properties of zeolite membranes by transient permeation. Desalination. 2002;149:435-440.
20. Walter E, Pronzato L. Identification of Parametric Models from Experimental Data. Berlin: Springer, 1997.
21. Couenne F, Jallut C, Tayakout-Fayolle M. On minimal representation of heterogeneous mass transfer for simulation and parameter estimation: application to breakthrough curves exploitation. Comput Chem Eng. 2005;30:42-53.
22. Tayakout-Fayolle M, Jolimaitre E, Jallut C. Consequence of structural identifiability properties on state-model formulation for linear inverse chromatography. Chem Eng Sci. 2000;55:2945-2956.
23. Gardner TQ, Flores AI, Noble RD, Falconer JL. Transient measurements of adsorption and diffusion in H-ZSM-5 membranes. AIChE J. 2002;48:1155-1167.
24. Gardner TQ, Lee JB, Noble RD, Falconer JL. Adsorption and diffusion properties of butanes in ZSM-5 zeolite membranes. Ind Eng Chem Res. 2002;41:4094-4105.
25. Chau C, Sicard M, Le Dred R. Membrane zéolithique de faible épaisseur, sa préparation et son utilisation en séparation. Eur. Pat. EP 1, 369,166 A1, 2003.
26. Chau C, Prevost I, Dalmon JA, Miachon S. Process for preparing supported zeolitic membranes by temperature-controlled crystallisation. U.S. Pat. 6,582,495 B2, 2003.
27. Chau C, Prevost I, Dalmon JA, Miachon S. Procédé de préparation de membranes zéolithiques supportées par cristallisation contrôlées en température. Eur. Pat. EP 1, 230,972 B1, 2006.
28. Wicke E, Kallenbach R. Die Oberflächendiffusion von kohlendioxyd in aktiven kohlen. Kolloid Z. 1941;97:135-151.
29. Amost D, Schneider P. Dynamic transport of multicomponent mixtures of gases in porous solids. Chem Eng J Biochem Eng J. 1995;57:91-99.
30. Biswasa J, Do DD, Greenfield PF, Smith JM. Evaluation of bidisperse transport properties of a reforming catalyst using a diffusion cell T. Theoretical development. Appl Catal. 1987;32: 217-234.
31. Biswasa J, Do DD, Greenfield PF, Smith JM. Evaluation of bidisperse transport properties of a reforming catalyst using a diffusion cell II. Experimental study. Appl Catal. 1987;32:235-247.
32. Burghardt A, Smith JM. Dynamic response of a single catalyst pellet. Chem Eng Sci. 1979;34:267-273.
33. Do DD, Smith JM. Transient response of diffusion cell containing a porous solid. Chem Eng Sci. 1984;39:1689-1699.
34. Dogu G, Smith JM. Rate parameters from dynamic experiments with single catalyst pellets. Chem Eng Sci. 1976;31;123-I35.
35. Bakker WJW, Kapteijn F, Poppe J, Moulijn JA. Permeation characteristics of a metal-supported silicalite-1 zeolite membrane. J. Membr Sci. 1996;117:57-78.
36. Sun MS, Talu O, Shah DB. Diffusion measurements through embedded zeolite cristal. AIChE J. 1996;42:3001-3007.
37. Courthial L, Baudot A, Jolimaitre E, Tayakout-Fayolle M, Jallut C. Moments method applied to the in-situ characterisation of normal butane mass transfer in MFT zeolite membranes. Desalination. 2006;193:215-223.
38. Tayakout-Fayolle M, Jallut C, Lefevre F, Dalmon JA. Application of transient methods to measurements of mass transfer parameters in zeolitic membranes. ECCE1, First European Congress on Chemical Engineering, Florence, Italy, May 4-7, 1997, Vol. 2, 1209-1212.
39. Poling BP, Prausnitz JM, O'Connel JP. The Properties of Gases and Liquids, 5th ed. Boston: McGraw-Hill, 2001.
40. Aris R. On the dispersion of a solute in a fluid flowing through a tube. Proc R Soc Lond A. 1956;235:67-77.
41. Ciavarella P, Moueddeb H, Miachon S, Fiaty K, Dalmon JA. Experimental study and numerical simulation of hydrogen/isobutane permeation and separation using MFI-zeolite membrane reactor. Catal Today, 2000;56:253-264.
42. Vasenkov S, Karger J. Evidence for the existence of intracistalline transport barriers in MFI-type zeolites: a model constituency check using MC simulations. Microporous Mesoporous Mater. 2002;55:139-145.
43. Bakker WJW, Van den Broeke UP, Kapteijn F, Moulijn JA. Temperature dependence of one-component permeation through a silicalite-1 membrane. AIChE J. 1997;43:2203-2214.
44. Ghosh UK, Upadhyay SN. Mass transfer to newtonian and non-newtonian fluids in short annuli. AIChE J. 1985;31:1721-1724.
45. Grober H, Erk S, Tate GE. Fundamentals of Heat Transfer. New York: McGraw-Hill, 1961.
46. Kapteijn F, Bakker WJW, Zheng G, Moulijn JA. Temperature- and occupancy-dependent diffusion of n-butane through a silicalite-1 membrane. Microporous Mater. 1994;3:227-234.
47. Zhu W, Van de Graaf JM, Van den Broeke LJP, Kapteijn F, Moulijn JA. TEOM: a unique technique for measuring adsorption properties. Light alkanes in silicalite-1. Ind Eng Chem Res. 1998;37: 1934-1942.
48. Pascual P, Ungerer P, Tavitian B, Boutin A. Development of a transferable guest-host force field for adsorption of hydrocarbons in zeolites. II. Prediction of alkenes adsorption and alkane/alkene selectivity in silicalite. J Phys Chem B. 2004;108:393-398.
49. Shen D, Rees LVC. Adsorption and diffusion on n-butane and 2-butyne in silicalite-1. Zeolites. 1991;11:684-689.
50. Ferreira AFP, Mittelmeijer-Hazeleger MC, Bliek A. Adsorption and differential heats of adsorption of normal and iso-butane on zeolite MFI. Microporous Mesoporous Mater. 2006;91:47-52.
51. Krishna R, Baur R. Analytic solution of the Maxwell-Stefan equations for multicomponent permeation across a zeolite membrane. Chem Eng J. 2004;97:37-45.
52. Heink W, Karger J, Pfeifer H, Datema K, Nowak AK. High-temperatured pulse field gradient nuclear magnetic resonance self-diffusion measurements of alkanes in MFI-type zeolites. J Chem Soc Faraday Trans. 1992;88:2505-3809.
53. Millot B, Méthivier A, Jobic H, Moueddeb H, Dalmon JA. Permeation of linear and branched alkanes in ZSM-5 supported membranes. Microporous Mesoporous Mater. 2000;38:85-95.
54. Hayhurst DT, Paravar AR. Diffusion of C1 to C5 normal paraffins in silicalite. Zeolites. 1988;8:27-29.
55. Jiang M, Eic M, Miachon S, Dalmon JA, Kocirik M. Diffusion of n-butane, isobutane and ethane in a MFI-zeolite membrane investigated by gas permeation and ZLC measurements. Sep Purif Technol. 2001;25:287-295.
56. Keizer K, Burggraaf AJ, Vroon ZAEP, Verweij H. Two component permeation through thin zeolite MFI membranes. J Membr Sci. 1998; 147:159-172.
57. Millot B, Méthivier A, Jobic H, Moueddeb H, Bee M. Diffusion of isobutane in ZSM-5 zeolite: a comparison of quasi-elastic neutron scattering and supported membrane results. J Phys Chem B. 1999; 103:1096-1101.