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A weak broad signal centred in the 4-5 ppm region corresponding to water could be eventually observed
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NOTE:, at, overnight
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NOTE: A weak broad signal centred in the 4-5 ppm region corresponding to water could be eventually observed. This can be, at least partly, due to the water frequently present in the DMSO solvent, but in any case, the integrated contents represented around 2-4% in weight and could be minimized by drying the samples in vacuum at 50-70°C overnight.
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This can be, at least partly, due to the water frequently present in the DMSO solvent, but in any case, the integrated contents represented around 2-4% in weight and could be minimized by drying the samples in vacuum
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