ICP-MS and Te Co-precipitation after nickel sulphide fire-assay collection for pd determination in roadside soils

Palladium Emissions in the Environment: Analytical Methods, Environmental Assessment and Health Effects

Volumn , Issue , 2006, Pages 163-172

  Figueiredo, Ana Maria G ^a   Enzweiler, Jacinta ^b   Morcelli Claudia, P R ^a   Sarkis, Jorge ^a  

^a INSTITUTO DE PESQUISAS ENERGÉTICAS E NUCLEARES   (Brazil)

^b UNIVERSITY OF CAMPINAS   (Brazil)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 54349117524     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1007/3-540-29220-9_12     Document Type: Chapter

References (33)

1. Amossé J (1998) Determination of platinum-group elements and gold in geological matrices by inductively coupled plasma-mass spectrometry (ICP-MS) after separation with selenium and tellurium carriers. Geostandards Newsletter -The Journal of Geostandards and Geoanalysis 22: 93-102.
2. Amossé J, Delbos V (2002) Dispersion dans l'environnement routier et urbain de Pt, Pd, et Rh émis par les pots d'échappement catalytiques Étude de la spéciation des elements. Comptes Rendus Chimie 5: 565-570.
3. Asif M, Parry SJ (1989) Elimination of reagent blank problems in the fire assay preconcentration of platinum-group elements and gold with a nickel sulfide bead of less than one gram mass. Analyst 144: 1057-1059.
4. Boisvert R, Bergeron M and Turcotte J (1991) Re-examination od the determination of palladium, platinum and rhodium in rocks by nickel sulphide fire assay followed by graphite furnace atomic absorption measurements. Analytica. Chimica Acta 246: 365-373.
5. Cabral AR, Lehmann B, Kwitko-Ribeiro R, Costa CHC (2002) Palladium and platinum minerals from the Serra Pelada Au-Pd-Pt deposit, Carajas mineral province, northern Brazil. Canadian Mineralogist 40: 1451-1463.
6. Cabri LJ (1992) The Distribution of trace precious metals in minerals and mineral products. Mineralogical Magazine 56: 289-308.
7. Enzweiler J, Potts PJ, Jarvis KE (1995) Determination of platinum, palladium, ruthenium and iridium in geological samples by isotope dilution inductively coupled plasma mass spectrometry using a sodium peroxide fusion and tellurium coprecipitation. Analyst 120: 1391-1396.
8. Figueiredo AMG, Enzweiler J, Sarkis JES, Jorge APS, Shibuya EK (2000) NAA and UV laser ablation ICP-MS for platinum group elements and gold determination in NiS fire assay buttons: A comparison between two methods. Journal of Radioanalytical and Nuclear Chemistry 244(3): 623-625.
9. Frimpong A, Fryer BJ, Longerich HP, Chen Z, and Jackson SE (1995) Recovery of precious metals using nickel sulfide fire assay collection: problems at nanogram per gram concentrations. Analyst 120: 1675-1680.
10. Fritsche J, Meisel T (2004) Determination of anthropogenic input of Ru, Rh, Pd, Re, Os, Ir and Pt in soils along Austrian motorways by isotope dilution ICPMS. Science of the Total Environment 325: 145-154.
11. Gowing CJB, Potts PJ (1991) Evaluation of a rapid technique for the determination of precious metals in geological samples based on a selective aqua regia leach. Analyst 116: 773-779.
12. Horwitz W, Albert R (1995) Precision in analytical measurements: expected values and consequence in geochemical analysis. Fresenius Journal of Analytical Chemistry 35: 507-513.
13. Jackson SE, Fryer BJ, Gosse W, Healey DC, Longerich HP and Strong DF (1990) Determination of the precious metals in geological materials by inductively coupled plasma-mass spectrometry (ICP-MS) with nickel sulphide fire assay collection and tellurium coprecipitation. Chemical Geology 83: 119-132.
14. Jorge APS, Enzweiler J, Shibuya EK, Sarkis JES, Figueiredo AMG (1998) Platinum group elements and gold determination in NiS fire assay buttons by UV laser ablation ICP-MS. Geostandards Newslettter: The Journal of Geostandards and Geoanalysis 22(1): 47-55.
15. Kane JS (1991) Quality control and reference sample databases. Geostandards Newsletter: The Journal of Geostandards and Geoanalysis 15: 32-42.
16. Meisel T, Fellner N, Moser J (2003) A simple procedure for the determination of platinum group elements and rhenium (Ru, Rh, Pd, Re, Os, Ir and Pt) using IDICP- MS with an inexpensive on-line matrix separation in geological and environmental materials. Journal of Analytical Atomic Spectrometry 18: 720-726.
17. Morcelli CPR, Figueiredo AMG (2000) Determination of iridium at sub ng g-1 levels in geological materials by RNAA. Journal of Radioanalytical and Nuclear Chemistry 44: 619-621.
18. Morcelli CPR, Figueiredo AMG, Sarkis JES, Enzweiler J, Kakazu M and Sígolo JB (2005) PGEs and other traffic related elements in roadside soils from São Paulo, Brazil. Science of the Total Environment (in press).
19. Morton O, Puchelt H, Hernández E, Lounejeva E (2001) Traffic-related platinum group elements (PGE) in soils from Mexico City. Journal of Geochemical Exploration 72: 223-227.
20. Oguri K, Shimoda G, Tatsumi Y (1999) Quantitative determination of gold and the platinum-group elements in geological samples using improved NiS fire-assayand tellurium coprecipitation with inductively coupled plasma-mass spectrometry (ICP-MS). Chemical Geology. 157: 189-197.
21. Parry SJ, Sinclair IW, Asif M (1988) in: Geo-Platinum 87, ed. Prichard HM, Potts, PJ, Bowles JFW and Cribb SJ, Elsevier, London, p. 29.
22. Paukert T, Rubeska I (1993) Effects of fusion charge composition on the determination of platinum group elements using collection into a minimized nickel sulphide button. Analytica Chimica Acta 278: 125-136.
23. Pearson DG, Woodland SJ (2000) Solvent extraction anion exchange separation and determination of PGEs Os, Ir, Pt, Pd, Ru and Re-Os isotopes in geological samples by isotope dilution ICP-MS Chemical Geology 165: 87-107.
24. Pennebaker FM, Denton MB (2001) High-precision, simultaneous analysis of Pt, Pd, and Rh in catalytic converter samples by Carius tube dissolution and inductively coupled plasma atomic emission spectroscopy with charge-injection device detection. Applied Spectroscopy 55: 504-509.
25. Potts PJ (1992) A Handbook of Silicate Rock Analysis. Blackie, London, 622 pp.
26. Rauch S, Hemond HF and Peucker-Ehrenbrink B (2004) Source characterisation of atmospheric platinum group element deposition into an ombrotrophic peat bog. Journal of Environmental Monitoring 6: 335-343.
27. Robert RVD, VanWyk E and Palmer R (1971) Concentration of the noble metals by a fire assay technique using NiS as the collector. Report, National Institute for Metallurgy Johannesburg, No. 1371, 15pp.
28. Schafer J, Puchelt H (1998) Platinum group metals (PGM) emitted from automobile catalytic converters and their distribution in roadside soils. Journal of Geochemical Exploration 64: 301-314.
29. Shazali I, Vant'Dack L, Gibjels R (1987) Determination of precious metals in ores and rocks by thermal neutron activation/gama-spectrometry after preconcentration by nickel sulphide fire assay and coprecipitation with tellurium. Analytica Chimica Acta 196: 49-58.
30. Shibuya EK, Sarkis JE, Enzweiler J, Jorge APS, Figueiredo AMG (1998) Determination of platinum group elements and gold in geological materials using an ultraviolet laser ablation high-resolution inductively coupled plasma mass spectrometric technique. Journal of Analytical Atomic Spectrometry 13: 941- 944.
31. Stockman HW (1983) Neutron determination of noble metals in rocks a rapid radiochemical separation based on tellurium copecipitation. Journal of Radioanalytical and Nuclear Chemistry 78(2), 307-317.
32. Wood SA, Middlesworth A (2004) The influence of acetate and oxalate as simple organic ligands on the behavior of palladium in surface environments. The Canadian Mineralogist 42: 411-421.
33. Zischka M, Wegscheider W (2000) Reliability of and measurement uncertainty for the determination of Au, Pd, Pt and Rh by ICP-MS in environmentally relevant samples. In: Anthropogenic Platinum-Group Element Emissions - Their Impact on Man and Environment. Zereini F and Alt F (ed.) Springer-Verlag Berlin Heidelberg, 2000, p. 201-214.