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54249115126
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-1.
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54249146637
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10
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34547949856
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54249110070
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1-DMAP]≡C15H24N8S 2Zn, Mr=445.95. Monoclinic P2 1/n, a= 11.0951(3, b=13.9392(4, c=13.2449(4) Å, β=97.6854(13)°, V=2030.01(10) Å3, ρcalcd (Z=4)=1.459 Mgm-3, μ= 1.432 mm -1, specimen: 0.07 x 0.18 x 0.63 mm, 2θmax=27.5° λ=0.71073 A°, Nt=14405, N=4572 (Rint=0.042, No=3521, R (I>2σ(I, 0.0357, wR (I>2σI, 0.0639, T=150 K. CCDC 686182 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via
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o=3521, R (I>2σ(I))=0.0357, wR (I>2σ(I)) =0.0639, T=150 K. CCDC 686182 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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13
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54249126661
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54249133623
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The two peaks correspond to anomers of glucose and are consistent with the results of previous solution-phase radio-labeling experiments
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The two peaks correspond to anomers of glucose and are consistent with the results of previous solution-phase radio-labeling experiments.
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16
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84961980477
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18
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54249094849
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The lowest concentration of 1 and 3 observable by the UV detector (254 nm) is 1.0 μm.
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The lowest concentration of 1 and 3 observable by the UV detector (254 nm) is 1.0 μm.
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19
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36749090019
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