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Volumn 71, Issue 9, 2008, Pages 1616-1619

Structures and absolute configurations of sulfate-conjugated triterpenoids including an antifungal chemical defense of the green macroalga Tydemania expeditionis

Author keywords

[No Author keywords available]

Indexed keywords

ANTIFUNGAL AGENT; CYCLOARTA 24 EN 3,29 DIOL 23 DISODIUM SULFATE; CYCLOARTAN 3,23,29 TRIOL 3,29 DISODIUM SULFATE; CYCLOARTAN 3,29 DIOL 23 ONE 3,29 DISODIUM SULFATE; CYCLOARTANE; LANOSTA 8 EN 3,29 DIOL DISODIUM SULFATE; LANOSTANE; NATURAL PRODUCT; SULFATE; TRITERPENOID; UNCLASSIFIED DRUG;

EID: 54149113551     PISSN: 01633864     EISSN: None     Source Type: Journal    
DOI: 10.1021/np800307h     Document Type: Article
Times cited : (20)

References (14)
  • 6
    • 54149102212 scopus 로고    scopus 로고
    • Crystal data for compound 1. C30H48O 9S2Na2·2CH3OH·H 2O, colorless plates (0.28 x 0.21 x 0.11 mm) were recrystallized from MeOH solution, orthorhombic, P212121, a, 7.1495(5) Å, b, 10.4548(7) Å, c, 49.990(3) Å, V, 3736.6(4) Å3, Z, 4, dx, 1.317 g cm-3, F(000, 1584, λ(CuKα) 1.54178 Å, Flack parameter 0.18(5, Data collection was performed on a SMART 1000 CCD; 5594 [R(int) 0.0409] unique reflections were collected to θmax, 65.9°, in which 5110 reflections were observed [F2 > 4σF 2, The crystal structure was resolved by direct methods using SHELXS-97. In the final stage, R, 0.105 and S, 1.094. CCDC no. 686956
    • 2)]. The crystal structure was resolved by direct methods using SHELXS-97. In the final stage, R = 0.105 and S = 1.094. CCDC no. 686956.
  • 10
    • 54149094641 scopus 로고    scopus 로고
    • Crystal data for compound 2. C30H46O 9S2Na2·CH3OH·2H 2O, colorless plates (0.25 x 0.21 x 0.08 mm) were recrystallized from MeOH solution, monoclinic, P21, a, 6.899(1) Å, b, 9.952(1) Å, c, 26.382(3) Å, β, 91.73(1)°, V, 1810.4(4) Å3, Z, 2, dx, 1.331 g cm-3, F(000, 774, λ(Cu Kα) 1.54178 Å, Hack parameter 0.05(3, Data collection was performed on a SMART 1000 CCD; 4376 [R(int, 0.0348] unique reflections were collected to θmax, 66.11°, in which 4069 reflections were observed [F2 > 4σF2, The crystal structure was resolved by direct methods using SHELXS-97. In the final stage, R, 0.061 and S, 1.080. CCDC no. 686957
    • 2)]. The crystal structure was resolved by direct methods using SHELXS-97. In the final stage, R = 0.061 and S = 1.080. CCDC no. 686957.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.